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1. 发明授权

US09805851B2 Grain-oriented electrical steel sheet and method of producing the same 有权
公开(公告)号：US09805851B2
公开(公告)日：2017-10-31
申请号：US14352904
申请日：2012-10-16
申请人： JFE STEEL CORPORATION
发明人： Makoto Watanabe , Yukihiro Shingaki , Toshito Takamiya , Tomoyuki Okubo
IPC分类号： H01F1/147 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/12 , C22C38/16 , C22C38/34 , C22C38/60 , C21D8/02 , C21D8/12 , C21D9/46 , H01F1/16 , C22C38/00 , C22C38/08 , C23C22/33 , C23C22/74
CPC分类号： H01F1/14775 , C21D8/0263 , C21D8/1222 , C21D8/1233 , C21D8/1272 , C21D9/46 , C22C38/001 , C22C38/008 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/08 , C22C38/12 , C22C38/16 , C22C38/34 , C22C38/60 , C23C22/33 , C23C22/74 , H01F1/16
摘要： In a method of producing a grain-oriented electrical steel sheet by hot rolling a steel slab comprising C: 0.001˜0.10 mass %, Si: 1.0˜5.0 mass %, Mn: 0.01˜1.0 mass %, one or two of S and Se: 0.01˜0.05 mass % in total, sol. Al: 0.003˜0.050 mass % and N: 0.001˜0.020 mass %, cold rolling, subjecting to primary recrystallization annealing, applying an annealing separator and finally subjecting to final annealing, the primary recrystallization annealing is conducted so as to control a heating rate S1 between 500 and 600° C. to not less than 100° C./s and a heating rate S2 between 600 and 700° C. to not less than 30° C./s but not more than 0.6×S1, and as a main ingredient of the annealing separator is used MgO having an expected value μ(A) of citric acid activity distribution of 3.5˜3.8, a cumulative frequency F of 25˜45% when an activity A is not less than 4.0.

2. 发明申请

US20160333227A1 METHOD FOR PRODUCING METAL CONTAINING COMPOSITE AND METAL CONTAINING COMPOSITE FORMED BY ADHESION 有权
标题翻译：用于生产含金属复合材料的方法和通过粘合形成的含金属复合材料
公开(公告)号：US20160333227A1
公开(公告)日：2016-11-17
申请号：US15153670
申请日：2016-05-12
申请人： ANDOH-Corporation limited partnership company
发明人： Naoki ANDOH
IPC分类号： C09J7/02
CPC分类号： B32B7/12 , B29C65/00 , B29C65/02 , B29C65/4835 , B29C65/526 , B29C65/8215 , B29C65/8253 , B29C66/0222 , B29C66/02245 , B29C66/0242 , B29C66/112 , B29C66/114 , B29C66/1142 , B29C66/30322 , B29C66/43 , B29C66/43421 , B29C66/43441 , B29C66/71 , B29C66/7212 , B29C66/72141 , B29C66/73161 , B29C66/73751 , B29C66/73755 , B29C66/7394 , B29C66/742 , B29C66/7422 , B29C66/7428 , B29C66/74281 , B29C66/74283 , B29C66/919 , C09J5/06 , C09J163/00 , C23C22/05 , C23C22/33 , C23C22/57 , C23C22/63 , C23C22/64 , C23F1/18 , C23F1/20 , C23F1/28 , C23F1/40 , C23G1/00 , C23G1/125 , C23G1/22 , B29K2307/04 , B29K2063/00
摘要： An adhesive (B) of solvent containing adhesive as a suspension of low viscosity is prepared by adding a solvent MIBK to a one-part epoxy adhesive of a dicyandiamide-curable type (A). Metal shaped articles (M1 to M5) as adherends are prepared each of which, through various surface treatment, has specific surface configuration of roughened face and/or ultrafine irregularities and the surface is entirely covered with a thin layer of ceramics such as a metal oxide or metal phosphate. The specified face of each metal shaped article (M1 to M5) is painted with the solvent containing adhesive (B). The faces painted with the adhesive of two metal shaped articles (M1 to M5) are caused to abut each other, the articles are heated to cure the one-epoxy adhesive to accomplish adhesion. With one of the adherends replaced by a CFRP shaped article (P2), a composite of a metal and CFRP can be formed.
摘要翻译：通过将溶剂MIBK加入到双氰胺可固化型（A）的一部分环氧粘合剂中来制备粘合剂（B）作为低粘度悬浮液的粘合剂。制备作为被粘物的金属制品（M1至M5），其各自通过各种表面处理具有粗糙面和/或超细不规则性的比表面构造，并且表面完全被诸如金属氧化物的陶瓷薄层或金属磷酸盐。每个金属制品（M1至M5）的指定表面涂上含溶剂的粘合剂（B）。使用两个金属制品（M1至M5）的粘合剂涂上的表面彼此邻接，将制品加热固化单环氧树脂粘合剂以实现粘合。通过用CFRP成型制品（P2）代替的被粘物之一，可以形成金属和CFRP的复合物。

3. 发明申请

US20130302600A1 DRY-IN-PLACE CORROSION-RESISTANT COATING FOR ZINC OR ZINC-ALLOY COATED SUBSTRATES 审中-公开
标题翻译：用于锌或锌合金涂层基材的耐腐蚀涂层
公开(公告)号：US20130302600A1
公开(公告)日：2013-11-14
申请号：US13947012
申请日：2013-07-19
申请人： Eco-Green Coatings, L.L.C.
发明人： William D. KRIPPES , Theodore JAROSZ , Mike SERAFINI , William CAPIZZANO
IPC分类号： C09D5/08
CPC分类号： C09D5/08 , C23C22/12 , C23C22/33 , C23C2222/10 , Y10T428/12535 , Y10T428/273
摘要： A process for making a corrosion-resistant metal component. The process having the steps of: combining water, at least one zinc phosphate compound and at least one chromium compound, being chromium (III) or chromium (IV) compounds, to form a first solution; separately combining at least one silicate compound with water to form a second solution; combining the first solution with the second solution such as to form a mixed aqueous solution; optionally combining the mixed aqueous solution with at least one acrylic resin to form a coating mixture; and, applying the coating mixture to a metal substrate having a zinc or zinc-alloy surface to form a coating on the metal substrate, the coating providing chemical resistance for at least 150 hours in accordance with ASTM B117 standards where the zinc or zinc-alloy coating of the metal substrate has a weight of 0.04 oz/ft2 (12.20 g/m2).
摘要翻译：一种制造耐腐蚀金属组分的方法。该方法具有以下步骤：将水，至少一种磷酸锌化合物和至少一种铬化合物，作为铬（III）或铬（IV）化合物组合以形成第一溶液; 分别将至少一种硅酸盐化合物与水混合以形成第二溶液; 将第一溶液与第二溶液组合以形成混合水溶液; 任选地将混合的水溶液与至少一种丙烯酸树脂混合以形成涂料混合物; 并且将涂料混合物施加到具有锌或锌合金表面的金属基材上以在金属基材上形成涂层，该涂层根据ASTM B117标准提供耐化学性至少150小时，其中锌或锌合金金属基材的涂层重量为0.04盎司/平方英尺（12.20克/平方米）。

4. 发明授权

US08119222B2 Pre-coated metal sheet for slot-in drive cases 有权
标题翻译：预涂金属板，用于插入式驱动器箱
公开(公告)号：US08119222B2
公开(公告)日：2012-02-21
申请号：US11602512
申请日：2006-11-20
申请人： Takehiro Ozawa , Masatsugu Saito
发明人： Takehiro Ozawa , Masatsugu Saito
IPC分类号： B32B15/08 , B32B15/082 , B32B15/09 , B32B15/092 , B32B27/00 , B32B27/30 , B32B27/36 , B32B27/38 , D06N7/04 , D06N7/00 , G11B5/62 , G11B17/00
CPC分类号： B05D5/08 , B05D5/02 , C08L77/00 , C09D5/00 , C09D7/65 , C23C22/33 , C23C28/00 , Y10T428/24372 , Y10T428/24405 , Y10T428/25 , Y10T428/265 , Y10T428/269 , Y10T428/31529 , Y10T428/31605 , Y10T428/31678
摘要： A pre-coated metal sheet for slot-in drive cases which has a metal sheet; chemical conversion coatings formed on both sides of the metal sheet; and a coating film formed on one of the chemical conversion coatings and containing at least one base resin selected from a polyester-series resin, an epoxy-series resin and an acrylic-series resin, at least one resin beads selected from nylon-series resin beads, fluorine-series resin beads and urethane-series resin beads, and at least one lubricant a3 selected from carnauba wax, polyethylene wax and microcrystalline wax. The coating film has a surface having an arithmetical mean deviation of the assessed profile Ra of 0.3 to 4.5 μm and a mean width of the profile elements, RSm, of 105 to 280 μm, and the ratio of mean particle diameter of the resin beads to coating film layer thickness of the coating film is in the range of 2.0 to 3.0.
摘要翻译：一种用于插入式驱动器壳体的预涂金属片，其具有金属片; 化学转化涂层形成在金属板的两面; 以及形成在所述化学转化涂层之一上并且含有选自聚酯类树脂，环氧类树脂和丙烯酸系树脂中的至少一种基础树脂的涂膜，至少一种选自尼龙系树脂珠粒，氟系树脂珠和氨基甲酸酯系树脂珠，以及选自巴西棕榈蜡，聚乙烯蜡和微晶蜡中的至少一种润滑剂a3。涂膜的表面具有评估的轮廓Ra的计算平均偏差为0.3〜4.5μm，轮廓元素的平均宽度RSm为105〜280μm，树脂珠粒的平均粒径与涂膜的涂膜层厚度在2.0〜3.0的范围内。

5. 发明授权

US06656294B1 Method of reducing elution of lead in lead-containing copper alloy, and drinking water service fittings made of lead-containing copper alloy 有权
公开(公告)号：US06656294B1
公开(公告)日：2003-12-02
申请号：US09586608
申请日：2000-06-02
申请人： Masashi Kawamoto , Akira Gotou , Mituo Imamoto
发明人： Masashi Kawamoto , Akira Gotou , Mituo Imamoto
IPC分类号： C23C2200
CPC分类号： E03B7/006 , C23C22/24 , C23C22/33 , C23F1/00 , C25D5/14 , C25D5/34 , Y10T29/4943
摘要： It is an object of the present invention to provide a processing method for preventing elution of lead in a lead-containing copper alloy to prevent lead from eluting from a faucet metal, etc. made of a lead-containing copper alloy, and a drinking water service fitting made of a lead-containing copper alloy in which elution of lead has been prevented. By forming a chromate film on the surface of a lead-containing copper alloy material, it is possible to reduce elution of the lead left in a limited amount on the surface. A drinking water service fitting made of a lead-containing copper alloy is immersed in an alkaline etching solution in a pre-processing step for a nickel chromium plating step to selectively remove lead on the surface of the lead-containing copper alloy material and is then activated in a solution such as sulfuric acid and hydrochloric acid. Nickel plating is subsequently effected, and then chromium plating is effected in a sargent chromium or chromium fluoride bath, and a chromate film may be formed by immersing the drinking water service fitting in a chromate solution.

6. 发明申请

US20020155314A1 Surface-treated steel sheet and production method therefor 失效
标题翻译：表面处理钢板及其制造方法
公开(公告)号：US20020155314A1
公开(公告)日：2002-10-24
申请号：US10024297
申请日：2001-12-17
发明人： Takafumi Yamaji , Kenji Morita , Akira Matsuzaki , Masaaki Yamashita , Etsuo Hamada
IPC分类号： B32B015/00
CPC分类号： C23C28/3225 , C23C2/26 , C23C22/33 , C23C22/73 , C23C22/83 , C23C26/00 , C23C28/00 , C23C28/345 , Y10S428/925 , Y10T428/12535 , Y10T428/12549 , Y10T428/12569 , Y10T428/12583 , Y10T428/12611 , Y10T428/12792 , Y10T428/12799
摘要： A surface-treated steel sheet includes a steel sheet, an AlnullZn-base alloy plating layer formed on the steel sheet, a chemical conversion film provided on the alloy plating layer, and a concentric layer of a Cr compound that is formed on the alloy plating layer of the chemical conversion film. The surface-treated steel sheet may include a steel sheet, an zinc-base plating layer formed on the steel sheet, and a film that contains chromium and calcium and that is formed on the zinc-base plating layer.
摘要翻译：表面处理钢板包括钢板，形成在钢板上的Al-Zn基合金镀层，设置在合金镀层上的化学转化膜，以及形成在钢板上的Cr化合物的同心层化学转化膜的合金镀层。表面处理钢板可以包括钢板，形成在钢板上的锌基镀层，以及含有铬和钙并形成在锌基镀层上的膜。

7. 发明授权

US06461741B1 Grain-oriented electromagnetic steel sheet with excellent coating properties and process for its manufacture 有权
标题翻译：晶粒取向的电磁钢板具有优良的涂层性能及其制造工艺
公开(公告)号：US06461741B1
公开(公告)日：2002-10-08
申请号：US09661003
申请日：2000-09-13
申请人： Kazutoshi Takeda , Shuichi Yamazaki , Hideyuki Kobayashi , Hiroyasu Fujii
发明人： Kazutoshi Takeda , Shuichi Yamazaki , Hideyuki Kobayashi , Hiroyasu Fujii
IPC分类号： B32B1504
CPC分类号： C23C28/044 , C04B28/346 , C04B2111/00525 , C21D8/1283 , C21D8/1288 , C23C22/08 , C23C22/33 , C23C22/74 , H01F1/14783 , H01F1/18 , Y10S428/90 , Y10S428/928 , Y10T428/12993 , Y10T428/32 , C04B14/06 , C04B14/307 , C04B40/0263 , C04B41/5006 , C04B41/0072
摘要： A high permeability grain-oriented electromagnetic steel sheet with a higher tension-imparting effect and more excellent cohesion and magnetic properties compared to the prior art, which also maintains sufficient corrosion resistance to withstand practical use; the grain-oriented electromagnetic steel sheet has on its surface an insulation coating comprising a first layer composed mainly of a divalent or trivalent metal hydrogen phosphate salt and silica, and a second layer composed mainly of aluminum borate and leaving a surface roughness of 0.1 &mgr;m-0.35 &mgr;m in terms of Ra (center like average roughness).
摘要翻译：与现有技术相比，具有更高的张力赋予效果和更优异的内聚力和磁特性的高磁导率晶粒取向电磁钢板，其也保持足够的耐腐蚀性以抵抗实际应用; 晶粒取向电磁钢板表面具有包含主要由二价或三价金属磷酸氢盐和二氧化硅组成的第一层的绝缘层，以及主要由硼酸铝组成的第二层，表面粗糙度为0.1μm- 以Ra计为0.35μm（中心像平均粗糙度）。

8. 发明授权

US06461449B1 Conversion coating zinciferous surfaces to resist blackening and white rust 失效
标题翻译：转化涂层含锌表面，防止黑化和白锈
公开(公告)号：US06461449B1
公开(公告)日：2002-10-08
申请号：US09529197
申请日：2000-04-07
申请人： Yuzuru Matsubara , Akira Kato
发明人： Yuzuru Matsubara , Akira Kato
IPC分类号： C23C2230
CPC分类号： C23C22/33
摘要： Metal surfaces, particularly the zinciferous surfaces of zinc-coated steel, can be given a chromate conversion coating that is superior in terms of blackening resistance and white rust resistance by drying into place on the surfaces a layer of a treatment liquid that contains water, hexavalent chromium atoms, trivalent chromium cations, nitrate ions and one or more types of metal ions selected from the group consisting of Ni, Co, Zn and Al, the molar ratio of the total of these metal ions to nitrate ions being in the range from 0.05 to 1.0, the molar ratio of trivalent chromium ions to hexavalent chromium atoms being in the range of 0.11:1.0 to 1.0:1.0, and the molar ratio of nitrate ions to total chromium atoms being in the range of 2.1 to 5.5. Preferably, the coating formed has a chromium content of 10 to 100 mg/m2.
摘要翻译：金属表面，特别是镀锌钢板的镀锌表面，可以得到铬酸盐转化膜，其耐黑变性和耐白锈锈性优于表面上一层含有水，六价铬的处理液铬原子，三价铬阳离子，硝酸根离子和选自Ni，Co，Zn和Al的一种或多种金属离子，这些金属离子与硝酸根离子的总摩尔比在0.05以下至1.0，三价铬离子与六价铬原子的摩尔比在0.11:1.0至1.0:1.0的范围内，硝酸根离子与总铬原子的摩尔比在2.1至5.5的范围内。优选地，形成的涂层的铬含量为10〜100mg / m 2。

9. 发明授权

US06329067B2 Chromating solution and chromated metal sheet 失效
标题翻译：铬酸盐溶液和铬酸盐金属片
公开(公告)号：US06329067B2
公开(公告)日：2001-12-11
申请号：US09752469
申请日：2001-01-03
申请人： Yukio Uchida , Hirofumi Taketsu , Shinya Furukawa
发明人： Yukio Uchida , Hirofumi Taketsu , Shinya Furukawa
IPC分类号： B32B1504
CPC分类号： C23C22/33 , C23C22/30 , Y10T428/31678
摘要： In a chromating solution comprising a water-soluble chromium compound and a reducing agent and in which hexavalent chromium ions produced by dissolution of the water-soluble chromium compound have been partly reduced with the reducing agent to trivalent chromium ions, an oxycarboxylic acid compound is used as the reducing agent. This chromating solution causes neither gelation nor sedimentation of the solution even when hexavalent chromium ions are reduced to trivalent chromium ions at a reduction percentage of more than 50%. The chromating solution and a chromate film formed on a steel sheet may also contain an organic resin, phosphoric acid or a phosphoric acid compound, or a silica sol.
摘要翻译：在包含水溶性铬化合物和还原剂的铬酸盐溶液中，通过还原剂将三价铬离子部分还原，其中通过溶解水溶性铬化合物产生的六价铬离子被使用，使用羟基羧酸化合物作为还原剂。即使当六价铬离子以大于50％的还原率还原成三价铬离子时，该铬酸盐溶液也不会引起溶液的凝胶化和沉淀。形成在钢板上的铬酸盐溶液和铬酸盐膜也可以含有有机树脂，磷酸或磷酸化合物或二氧化硅溶胶。

10. 发明授权

US5320737A Treatment to reduce solder plating whisker formation 失效
标题翻译：处理以减少焊料电镀晶须的形成
公开(公告)号：US5320737A
公开(公告)日：1994-06-14
申请号：US391754
申请日：1989-08-10
申请人： Chung-Yao Chao , Julius Fister
发明人： Chung-Yao Chao , Julius Fister
IPC分类号： C23C22/24 , C23C22/33 , C23G1/10 , C25D3/60 , C25D5/34 , H05K3/34
CPC分类号： H05K3/3473 , C23C22/24 , C23C22/33 , C23G1/103 , C25D3/60 , C25D5/34 , H05K2203/0392 , H05K2203/0723
摘要： The formation of whiskers during tin or tin-lead solder electroplating of a copper base alloy substrate in a methane sulfonate solder plating bath is inhibited by passivating the surface of the substrate prior to electroplating. Preferred passivating solutions include an aqueous solution of sodium dichromate and phosphoric acid, and an aqueous solution of chromic acid and phosphoric acid. Passivation is preferably followed by treatment with a basic solution having a pH of at least 8.
摘要翻译：铜基合金基板在甲烷磺酸盐焊料镀液中的锡或锡铅焊料电镀期间形成晶须在电镀之前钝化基板的表面被抑制。优选的钝化溶液包括重铬酸钠和磷酸的水溶液和铬酸和磷酸的水溶液。优选通过用pH至少为8的碱性溶液处理钝化。

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