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1. 发明授权

US6106802A Stable synthetic material and method for preparing same 失效
标题翻译：稳定的合成材料及其制备方法
公开(公告)号：US6106802A
公开(公告)日：2000-08-22
申请号：US24069
申请日：1998-02-17
申请人： Juan Lujano , Jose Carrazza , Norma Valencia de Zapata
发明人： Juan Lujano , Jose Carrazza , Norma Valencia de Zapata
IPC分类号： B01J23/44 , B01J20/02 , B01J20/28 , B01J23/46 , B01J35/10 , C01B33/158 , C01B33/46 , C01B37/00 , C01B37/02 , C01B39/00 , B01J21/06
CPC分类号： C01B37/02 , B01J20/02 , B01J20/06 , B01J20/103 , B01J20/3204 , B01J20/3236 , B01J29/0308 , B01J29/0325 , B01J29/041 , B01J35/002 , B01J35/10 , B01J35/1061 , B01J29/0316 , B01J29/0341
摘要： A composition of matter is provided including an inorganic porous material having wall portions defining mesopore-sized channels having a mean diameter of between about 15 .ANG. and about 100 .ANG. and a narrow diameter distribution of less than or equal to about 30 .ANG., the material having a void volume from the mesopore-sized channels of at least about 0.1 cc/g and a surface area of at least about 500 m.sup.2 /g and having a number of hydroxyl groups of at least about 1.5 mmol of hydroxyl groups per gram of material, and exhibiting thermal and hydrothermal stability at temperatures up to about 500.degree. C. Catalytic materials incorporating aluminum and other active metals, as well as a process for preparing the composition, are also disclosed.
摘要翻译：提供了一种物质组合物，其包括无机多孔材料，所述无机多孔材料具有限定中孔尺寸的通道的壁部分，其平均直径为约15至约100，窄直径分布小于或等于约30，所述材料具有来自中孔尺寸的通道的空隙体积为至少约0.1cc / g，表面积为至少约500m 2 / g，并且每克材料具有至少约1.5mmol羟基数量的羟基，并且在高达约500℃的温度下表现出热和水热稳定性。还公开了掺入铝和其它活性金属的催化材料以及制备该组合物的方法。

2. 发明授权

US06485702B1 Stable synthetic material and method for preparing same 有权
标题翻译：稳定的合成材料及其制备方法
公开(公告)号：US06485702B1
公开(公告)日：2002-11-26
申请号：US09568521
申请日：2000-05-09
申请人： Juan Lujano , Jose Carrazza , Norma Valencia de Zapata
发明人： Juan Lujano , Jose Carrazza , Norma Valencia de Zapata
IPC分类号： C01B3326
CPC分类号： C01B37/02 , B01J20/02 , B01J20/06 , B01J20/103 , B01J20/3204 , B01J20/3236 , B01J29/0308 , B01J29/0316 , B01J29/0325 , B01J29/0341 , B01J29/041 , B01J35/002 , B01J35/10 , B01J35/1061
摘要： A composition of matter is provided including an inorganic porous material having wall portions defining mesopore-sized channels having a mean diameter of between about 15 Å and about 100 Å and a narrow diameter distribution of less than or equal to about 30 Å, the material having a void volume from the mesopore-sized channels of at least about 0.1 cc/g and a surface area of at least about 500 m2/g and having a number of hydroxyl groups of at least about 1.5 mmol of hydroxyl groups per gram of material, and exhibiting thermal and hydrothermal stability at temperatures up to about 500° C. Catalytic materials incorporating aluminum and other active metals, as well as a process for preparing the composition, are also disclosed.
摘要翻译：提供了一种物质组合物，其包括无机多孔材料，所述无机多孔材料具有限定中孔尺寸的通道的壁部分，其平均直径在大约和大约之间，并且窄直径分布小于或等于约，其具有来自中孔尺寸的通道的空隙体积为至少约0.1cc / g，表面积为至少约500m 2 / g，并且每克材料具有至少约1.5mmol羟基数量的羟基，并且在高达约500℃的温度下表现出热和水热稳定性。还公开了掺入铝和其它活性金属的催化材料以及制备该组合物的方法。

3. 发明授权

US06410477B1 Hydrogenation catalyst of carbon monoxide and method of manufacturing hydrogenation product 失效
标题翻译：一氧化碳氢化催化剂及氢化产物的制造方法
公开(公告)号：US06410477B1
公开(公告)日：2002-06-25
申请号：US09657905
申请日：2000-09-08
申请人： Yasuo Ohtsuka , Muneyoshi Yamada , Ye Wang
发明人： Yasuo Ohtsuka , Muneyoshi Yamada , Ye Wang
IPC分类号： B01J2108
CPC分类号： B01J23/75 , B01J21/08 , B01J23/40 , B01J23/462 , B01J23/74 , B01J29/0316 , B01J35/10 , B01J35/1061 , C10G2/33
摘要： Provided is a hydrogenation catalyst of carbon monoxide, which is suited to the manufacture of a hydrogenation product containing target components (e.g., gasoline fuel oil components or diesel fuel oil components) at high selectivity from a gas mixture of hydrogen and carbon monoxide. This hydrogenation catalyst of carbon monoxide has a structure in which a transition metal is carried by a porous material in which 90% or more of all pores are fine pores each having a diameter of 1 to 50 nm.
摘要翻译：本发明提供一种一氧化碳的氢化催化剂，其适用于从氢气和一氧化碳的气体混合物以高选择性制备含有目标组分（例如汽油燃料油组分或柴油燃料油组分）的氢化产物。这种一氧化碳氢化催化剂具有这样的结构，其中过渡金属由多孔材料承载，其中所有孔的90％或更多是具有1至50nm直径的细孔。

4. 发明申请

US20050187410A1 Mesoporous material and use thereof for the selective oxidation of organic compounds 审中-公开
公开(公告)号：US20050187410A1
公开(公告)日：2005-08-25
申请号：US11108452
申请日：2005-04-18
申请人： Zhiping Shan , Thomas Maschmeyer , Jacobus Jansen
发明人： Zhiping Shan , Thomas Maschmeyer , Jacobus Jansen
IPC分类号： B01J21/06 , B01J21/08 , B01J21/12 , B01J23/26 , B01J23/38 , B01J23/44 , B01J23/50 , B01J23/52 , B01J29/00 , B01J29/03 , B01J29/04 , B01J29/08 , B01J29/40 , B01J29/70 , B01J29/80 , B01J29/87 , B01J29/88 , B01J29/89 , B01J35/00 , B01J35/04 , B01J35/10 , B01J37/00 , B01J37/02 , B01J37/03 , B01J37/08 , B01J37/10 , C01B13/36 , C01B33/12 , C01B37/00 , C01B37/02 , C07B61/00 , C07C2/66 , C07C45/46 , C07D301/06 , C07D301/08 , C07D301/10 , C07D303/04 , C10G2/00 , C10G11/04 , C10G11/05 , C10G27/04 , C10G29/20 , C10G45/00 , C10G45/04 , C10G45/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/08 , C10G50/00 , C07C249/08
CPC分类号： B01J29/89 , B01J21/06 , B01J21/063 , B01J21/12 , B01J23/26 , B01J23/38 , B01J23/44 , B01J23/50 , B01J23/52 , B01J29/005 , B01J29/0308 , B01J29/0316 , B01J29/04 , B01J29/042 , B01J29/046 , B01J29/084 , B01J29/40 , B01J29/70 , B01J29/7007 , B01J29/80 , B01J29/87 , B01J29/88 , B01J35/002 , B01J35/1023 , B01J35/1042 , B01J35/1061 , B01J35/1085 , B01J37/0018 , B01J37/033 , B01J37/10 , B01J2229/32 , B01J2229/36 , B01J2229/42 , B01J2229/62 , B82Y30/00 , C01B13/366 , C01B33/126 , C01B37/005 , C01B37/02 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C07C2/66 , C07C45/46 , C07D301/06 , C07D301/08 , C07D301/10 , C10G2/332 , C10G11/04 , C10G11/05 , C10G27/04 , C10G29/205 , C10G45/00 , C10G45/04 , C10G45/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/08 , C10G50/00 , C07C15/073 , C07C49/84
摘要： A material especially useful for the selective oxidation of hydrocarbons and other organic compounds includes a non-crystalline, porous inorganic oxide having at least 97 volume percent mesopores based on micropores and mesopores, and at least one catalytically active metal selected from the group consisting of one or more transition metal and one or more noble metal.

5. 发明授权

US06906208B2 Mesoporous material and use thereof for the selective oxidation of organic compounds 失效
标题翻译：介孔材料及其用于选择性氧化有机化合物的用途
公开(公告)号：US06906208B2
公开(公告)日：2005-06-14
申请号：US10246495
申请日：2002-09-18
申请人： Zhiping Shan , Thomas Maschmeyer , Jacobus Cornelius Jansen
发明人： Zhiping Shan , Thomas Maschmeyer , Jacobus Cornelius Jansen
IPC分类号： B01J21/06 , B01J21/08 , B01J21/12 , B01J23/26 , B01J23/38 , B01J23/44 , B01J23/50 , B01J23/52 , B01J29/00 , B01J29/03 , B01J29/04 , B01J29/08 , B01J29/40 , B01J29/70 , B01J29/80 , B01J29/87 , B01J29/88 , B01J29/89 , B01J35/00 , B01J35/04 , B01J35/10 , B01J37/00 , B01J37/02 , B01J37/03 , B01J37/08 , B01J37/10 , C01B13/36 , C01B33/12 , C01B37/00 , C01B37/02 , C07B61/00 , C07C2/66 , C07C45/46 , C07D301/06 , C07D301/08 , C07D301/10 , C07D303/04 , C10G2/00 , C10G11/04 , C10G11/05 , C10G27/04 , C10G29/20 , C10G45/00 , C10G45/04 , C10G45/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/08 , C10G50/00 , C07D301/12 , C07D301/14
CPC分类号： B01J29/89 , B01J21/06 , B01J21/063 , B01J21/12 , B01J23/26 , B01J23/38 , B01J23/44 , B01J23/50 , B01J23/52 , B01J29/005 , B01J29/0308 , B01J29/0316 , B01J29/04 , B01J29/042 , B01J29/046 , B01J29/084 , B01J29/40 , B01J29/70 , B01J29/7007 , B01J29/80 , B01J29/87 , B01J29/88 , B01J35/002 , B01J35/1023 , B01J35/1042 , B01J35/1061 , B01J35/1085 , B01J37/0018 , B01J37/033 , B01J37/10 , B01J2229/32 , B01J2229/36 , B01J2229/42 , B01J2229/62 , B82Y30/00 , C01B13/366 , C01B33/126 , C01B37/005 , C01B37/02 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C07C2/66 , C07C45/46 , C07D301/06 , C07D301/08 , C07D301/10 , C10G2/332 , C10G11/04 , C10G11/05 , C10G27/04 , C10G29/205 , C10G45/00 , C10G45/04 , C10G45/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/08 , C10G50/00 , C07C15/073 , C07C49/84
摘要： A material especially useful for the selective oxidation of hydrocarbons and other organic compounds includes a non-crystalline, porous inorganic oxide having at least 97 volume percent mesopores based on micropores and mesopores, and at least one catalytically active metal selected from the group consisting of one or more transition metal and one or more noble metal.
摘要翻译：特别可用于烃和其它有机化合物的选择性氧化的材料包括非结晶多孔无机氧化物，其具有至少97体积％的基于微孔和介孔的介孔，以及至少一种选自以下的催化活性金属：一种或更多的过渡金属和一种或多种贵金属。

6. 发明授权

US06544923B1 Surface-confined catalytic compositions 失效
标题翻译：表面封闭催化剂组合物
公开(公告)号：US06544923B1
公开(公告)日：2003-04-08
申请号：US09648928
申请日：2000-08-25
申请人： Jackie Y. Ying , Christian P. Mehnert , John S. Lettow , Dejian Huang
发明人： Jackie Y. Ying , Christian P. Mehnert , John S. Lettow , Dejian Huang
IPC分类号： B01J3100
CPC分类号： B01J35/1061 , B01J21/08 , B01J29/0308 , B01J29/0316 , B01J31/1608 , B01J31/1616 , B01J31/1625 , B01J31/2286 , B01J31/2295 , B01J31/2409 , B01J35/10 , B01J35/1023 , B01J35/1042 , B01J35/108 , B01J2229/32 , B01J2231/321 , B01J2231/4205 , B01J2231/4211 , B01J2231/4261 , B01J2231/645 , B01J2531/0266 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/827 , B01J2531/828
摘要： The present invention provides a novel catalytic system comprising catalysts immobilized on ultra-large mesoporous compositions, and particularly compositions having a large percentage of pores with a mean diameter of at least about 50 Å. Catalysts, such as organometallic complexes can reside in these pores to effect catalytic reactions. Such compositions include silicates covalently bound to a ligand that in turn can covalently bind an organometallic fragment. For asymmetric organometallic catalysts, the catalyst is bound to the mesoporous composition via an achiral ligand. The catalytic reactions include hydrogenation, hydroformylation, carbonylation and carbon-carbon coupling reactions, such as Heck or Suzuki reactions. The present invention provides catalyst for performing asymmetric reactions to achieve products of high stereoselectivities. The present invention also relates to ionically immobilized catalysts. In addition, the large pore sizes of these compositions can be used for polymerization reactions where the pore sizes can be tuned to achieve a particular molecular weight distribution. Other uses of the porous compositions include support materials for combinatorial chemistry.
摘要翻译：本发明提供了一种包含固定在超大介孔组合物上的催化剂的新型催化体系，特别是具有大百分比的平均直径至少为约的孔的组合物。催化剂，例如有机金属配合物可以存在于这些孔中以进行催化反应。这样的组合物包括与配体共价结合的硅酸盐，其又可以共价结合有机金属片段。对于不对称有机金属催化剂，催化剂通过非手性配体与介孔组合物结合。催化反应包括氢化，加氢甲酰化，羰基化和碳 - 碳偶联反应，如Heck或Suzuki反应。本发明提供用于进行不对称反应以获得高立体选择性产物的催化剂。本发明还涉及离子固定的催化剂。此外，这些组合物的大孔径可用于聚合反应，其中孔径可被调整以获得特定的分子量分布。多孔组合物的其它用途包括用于组合化学的支撑材料。

7. 发明申请

US20160250623A1 Catalyst for Benzene Hydroxylation for Preparation of Phenol and Preparation Method Thereof 审中-公开
标题翻译：用于制备苯酚的苯羟基化催化剂及其制备方法
公开(公告)号：US20160250623A1
公开(公告)日：2016-09-01
申请号：US15028438
申请日：2014-09-12
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Rizhi CHEN , Yaohui BAO , Hong JIANG , Yiqun FAN , Weihong XING
IPC分类号： B01J29/03 , B01J37/06
CPC分类号： B01J29/0341 , B01J29/0316 , B01J29/0325 , B01J29/0333 , B01J37/06 , B01J2229/186 , B01J2229/32 , C07C37/58 , Y02P20/52 , C07C39/04
摘要： The invention relates to a catalyst for benzene hydroxylation for preparation of phenol and a preparation method thereof, wherein said catalyst uses a mesoporous material as carrier, and the catalyst is prepared by first modifying the surface of the carrier using aminosilane, then immersing with acetylacetonate salt of metal, and finally washing and drying. Advantage of the invention is that a reactive metal is loaded on the silane-modified mesoporous material to form a homogeneous-heterogeneous composite catalyst, wherein, the reactive metal component is present in a reaction system in a homogeneous form, which ensures high catalytic performance of the catalyst component, and it is loaded on the carrier through bridging action of aminosilane, which improves the acting force between the metal component and the carrier, enhances stability of the catalyst, and facilitates separation of the catalyst from the product. The catalyst has a simple preparation process, has excellent catalytic performance, and can be applied to the reaction system of benzene hydroxylation for preparation of phenol.
摘要翻译：本发明涉及一种用于制备苯酚的苯羟基化催化剂及其制备方法，其中所述催化剂使用介孔材料作为载体，催化剂通过首先用氨基硅烷改性载体的表面，然后用乙酰丙酮盐的金属，最后洗涤和干燥。本发明的优点是将反应性金属负载在硅烷改性介孔材料上以形成均相 - 非均相复合催化剂，其中反应性金属组分以均匀形式存在于反应体系中，这确保了高的催化性能催化剂组分，并通过氨基硅烷的桥接作用负载在载体上，改善了金属组分与载体之间的作用力，提高了催化剂的稳定性，有利于催化剂与产物的分离。该催化剂具有简单的制备方法，具有优异的催化性能，可应用于苯羟基化反应体系制备苯酚。

8. 发明申请

US20050181930A1 Porous silicate materials and their uses as catalytic systems for diesel improvement 审中-公开
标题翻译：多孔硅酸盐材料及其用作柴油改进的催化体系
公开(公告)号：US20050181930A1
公开(公告)日：2005-08-18
申请号：US10503381
申请日：2003-01-31
申请人： Jacques Roziere , Deborah Jones , Melanie Jacquin , Antonio Jimenez-Lopez , Enrique Rodriguez-Castellon , Pedro Maireles-Torres , Jose-Manuel Trejo-Menayo , Angelo Vaccari , Maurizio Lenarda , Guido Busca
发明人： Jacques Roziere , Deborah Jones , Melanie Jacquin , Antonio Jimenez-Lopez , Enrique Rodriguez-Castellon , Pedro Maireles-Torres , Jose-Manuel Trejo-Menayo , Angelo Vaccari , Maurizio Lenarda , Guido Busca
IPC分类号： B01J21/08 , B01J29/04 , B01J37/03 , C10G45/48 , C10G45/52
CPC分类号： B01J29/042 , B01J21/08 , B01J29/0316 , B01J29/043 , B01J37/033 , B01J37/036 , C10G2400/04
摘要： A process of preparation of silicon-based multifunctional catalytic systems synthesised together with one or more surface active agents is described. Also described is a multifunctional silicon-based porous catalytic system including at least one porous catalytic support structurally including silica and at least one other metal or non-metal oxide chosen from aluminium, zirconium, and boron. The catalytic support is synthesised together with one or more surface active agents, and at least one or more catalyst chosen from among metallic elements of groups 6-10 of the periodic table of the elements. The catalytic systems are useful in hydrogenation and/or decyclisation reactions of (poly)aromatic compounds, especially for improving the quality of diesel fuels and increasing their cetane number.
摘要翻译：描述了与一种或多种表面活性剂一起制备的硅基多功能催化体系的制备方法。还描述了一种多功能硅基多孔催化体系，其包括至少一种结构上包含二氧化硅和选自铝，锆和硼的至少一种其它金属或非金属氧化物的多孔催化剂载体。催化载体与一种或多种表面活性剂和至少一种或多种选自元素周期表的6-10族金属元素的催化剂一起合成。催化体系可用于（多）芳族化合物的氢化和/或二环化反应，特别是用于改善柴油燃料的质量和增加其十六烷值。

9. 发明申请

US20030017943A1 Mesoporous material and use thereof for the selective oxidation of organic compounds 失效
标题翻译：介孔材料及其用于选择性氧化有机化合物的用途
公开(公告)号：US20030017943A1
公开(公告)日：2003-01-23
申请号：US10246495
申请日：2002-09-18
发明人： Zhiping Shan , Thomas Maschmeyer , Jacobus Cornelius Jansen
IPC分类号： B01J023/48
CPC分类号： B01J29/89 , B01J21/06 , B01J21/063 , B01J21/12 , B01J23/26 , B01J23/38 , B01J23/44 , B01J23/50 , B01J23/52 , B01J29/005 , B01J29/0308 , B01J29/0316 , B01J29/04 , B01J29/042 , B01J29/046 , B01J29/084 , B01J29/40 , B01J29/70 , B01J29/7007 , B01J29/80 , B01J29/87 , B01J29/88 , B01J35/002 , B01J35/1023 , B01J35/1042 , B01J35/1061 , B01J35/1085 , B01J37/0018 , B01J37/033 , B01J37/10 , B01J2229/32 , B01J2229/36 , B01J2229/42 , B01J2229/62 , B82Y30/00 , C01B13/366 , C01B33/126 , C01B37/005 , C01B37/02 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C07C2/66 , C07C45/46 , C07D301/06 , C07D301/08 , C07D301/10 , C10G2/332 , C10G11/04 , C10G11/05 , C10G27/04 , C10G29/205 , C10G45/00 , C10G45/04 , C10G45/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/08 , C10G50/00 , C07C15/073 , C07C49/84
摘要： A material especially useful for the selective oxidation of hydrocarbons and other organic compounds includes a non-crystalline, porous inorganic oxide having at least 97 volume percent mesopores based on micropores and mesopores, and at least one catalytically active metal selected from the group consisting of one or more transition metal and one or more noble metal.
摘要翻译：特别可用于烃和其它有机化合物的选择性氧化的材料包括非结晶多孔无机氧化物，其具有至少97体积％的基于微孔和介孔的介孔，以及至少一种选自以下的催化活性金属：一种或更多的过渡金属和一种或多种贵金属。

10. 发明授权

US06489258B1 Synthesis and application of vapor grafted porous materials 失效
标题翻译：蒸气接枝多孔材料的合成与应用
公开(公告)号：US06489258B1
公开(公告)日：2002-12-03
申请号：US09419365
申请日：1999-10-15
申请人： Jackie Y. Ying , Christian P. Mehnert
发明人： Jackie Y. Ying , Christian P. Mehnert
IPC分类号： B01J3116
CPC分类号： B01J29/0341 , B01J29/0308 , B01J29/0316 , B01J29/0325 , B01J29/0333 , B01J29/041 , B01J35/0053 , B01J35/006 , B01J37/0238 , B01J2229/18 , B01J2229/32 , B01J2229/34 , C07B37/04 , Y02P20/588
摘要： This invention provides an article, compositions, methods of making and uses of vapor-deposited metal compounds immobilized on porous substrates. The substrate is a porous substrate having an average pore size of at least about 8 Å and a surface area of at least about 10 m2/g. The methods describe the vapor-deposition of an inorganic compound onto the substrate where the deposition is accomplished with a relatively small amount of ligand loss. The substrate can be pre-treated to achieve a uniformly dispersed metal compound deposited on the substrate. The inorganic compound can decompose into a metal compound. The article can also function as a catalyst for carbon-heteroatom coupling reactions such as carbon-carbon coupling reactions, most notably, the Heck reaction.
摘要翻译：本发明提供一种制备和使用固定在多孔基材上的气相沉积金属化合物的制品，组合物，方法。基材是平均孔径至少约为8，表面积至少约10m 2 / g的多孔基材。该方法描述了无机化合物在基底上的蒸镀，其中以相对少量的配体损失完成沉积。可以对基底进行预处理，以实现沉积在基底上的均匀分散的金属化合物。无机化合物可分解成金属化合物。该文章还可以用作碳 - 杂原子偶联反应的催化剂，如碳 - 碳偶联反应，最着名的是Heck反应。

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