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1. 发明授权

US09926240B2 Process for producing BTX from a C5-C12 hydrocarbon mixture 有权
公开(公告)号：US09926240B2
公开(公告)日：2018-03-27
申请号：US14403883
申请日：2013-06-04
申请人： SAUDI BASIC INDUSTRIES CORPORATION
发明人： Andrew Mark Ward
IPC分类号： C07C4/06 , B01J35/00 , B01J23/42 , B01J29/40 , C10G45/62 , C10G45/64 , C10G47/00 , C10G47/14 , C10G47/18 , C10G47/22 , C10G65/10 , B01J21/04 , B01J21/08 , B01J35/10 , C10G45/70 , C07C4/14
CPC分类号： C07C4/06 , B01J21/04 , B01J21/08 , B01J23/42 , B01J29/40 , B01J35/0006 , B01J35/1019 , B01J35/1042 , B01J35/1061 , C07C4/14 , C07C2529/44 , C10G45/62 , C10G45/64 , C10G45/70 , C10G47/00 , C10G47/14 , C10G47/18 , C10G47/22 , C10G65/10 , C10G2300/1044 , C10G2400/30
摘要： The present invention relates to a process for producing chemical grade BTX from a mixed feedstream comprising C5-C12 hydrocarbons by contacting said feedstream in the presence of hydrogen with a catalyst having hydrocracking/hydrodesulphurization activity. Particularly, a process for producing BTX from a feedstream comprising C5-C12 hydrocarbons is provided comprising the steps of: (a) contacting said feedstream in the presence of hydrogen with a combined hydrocracking/hydrodesulphurization catalyst to produce a hydrocracking product stream comprising BTX; and (b) separating the BTX from the hydrocracking product stream. The hydrocracking/hydrodesulphurization catalyst comprises 0.1-1 wt-% hydrogenation metal in relation to the total catalyst weight. The hydrocracking/hydrodesulphurization catalyst further comprises a zeolite having a pore size of 5-8 Å and a silica (SiO2) to alumina (Al2O3) molar ratio of 5-200. The hydrocracking/hydrodesulphurization conditions include a temperature of 450-580° C., a pressure of 300-5000 kPa gauge and a Weight Hourly Space Velocity of 0.1-10 h−1.

2. 发明授权

US09839904B2 Method for producing hydrogenation catalyst 有权
公开(公告)号：US09839904B2
公开(公告)日：2017-12-12
申请号：US14007711
申请日：2012-03-26
申请人： Marie Iwama
发明人： Marie Iwama
IPC分类号： B01J29/10 , B01J29/16 , B01J37/00 , B01J29/12 , C10G47/14 , C10G65/14 , C10G45/10 , C10G49/06 , B01J21/12
CPC分类号： B01J29/126 , B01J21/12 , B01J29/106 , B01J29/166 , B01J37/0018 , B01J2229/20 , B01J2229/42 , C10G45/10 , C10G47/14 , C10G49/06 , C10G65/14 , C10G2300/1022
摘要： The present invention provides a method for producing a hydroprocessing catalyst including a supporting step of allowing a catalyst support having a content of a carbonaceous substance containing carbon atoms of 0.5% by mass or less in terms of carbon atoms to support an active metal component containing at least one active metal element selected from metals belonging to Group 6, Group 8, Group 9 and Group 10 in the periodic table, to obtain a catalyst precursor, and a calcining step of calcining the catalyst precursor obtained in the supporting step to obtain the hydroprocessing catalyst.

3. 发明申请

US20170267937A1 PROCESS FOR HYDROCRACKING HEAVY OIL AND OIL RESIDUE WITH A CARBONACEOUSE ADDITIVE 审中-公开
公开(公告)号：US20170267937A1
公开(公告)日：2017-09-21
申请号：US15115859
申请日：2015-02-12
申请人： BP EUROPA SE
发明人： Andreas Schleiffer , Hong Yang
IPC分类号： C10G47/02 , B01J37/08 , B01J37/06 , B01J37/04 , B01J21/18 , B01J35/10
CPC分类号： C10G47/02 , B01J21/18 , B01J35/0006 , B01J35/1019 , B01J35/1047 , B01J35/1061 , B01J37/04 , B01J37/06 , B01J37/084 , B01J37/20 , C01B32/342 , C10G47/14 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/202 , C10G2300/206 , C10G2300/208
摘要： A process for the hydroprocessing of heavy oils and/or oil residues, the process comprising the steps of contacting a non-metallised carbonaceous material with an acid to form a non-metallised carbonaceous additive; and contacting the heavy oils and/or oil residues with the non-metallised carbonaceous additive in the presence of a hydrogen-containing gas at a temperature of from 250° C. to 600° C.

4. 发明申请

US20170260463A1 PROCESS FOR HYDROCRACKING HEAVY OIL AND OIL RESIDUE WITH A NON-METALLISED CARBONACEOUS ADDITIVE 审中-公开
公开(公告)号：US20170260463A1
公开(公告)日：2017-09-14
申请号：US15115865
申请日：2015-02-12
申请人： BP EUROPA SE
发明人： Andreas SCHLEIFFER , Hong YANG
IPC分类号： C10G47/02 , B01J21/18 , C10G47/30
CPC分类号： C10G47/02 , B01J21/18 , B01J35/0006 , B01J35/1019 , B01J35/1047 , B01J35/1061 , B01J37/04 , B01J37/06 , B01J37/20 , C10G47/14 , C10G47/30 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/4006 , C10G2300/4012 , C10G2300/70
摘要： A process for the hydroprocessing of heavy oils and/or oil residues, the process comprising the steps of contacting a non-metallised carbonaceous material with an oxygen-containing gas at a temperature of at least 120° C. to form a non-metallised carbonaceous additive, and contacting the heavy oils and/or oil residues with the non-metallised carbonaceous additive in the presence of a hydrogen-containing gas at a temperature of from 250° C. to 600° C.

5. 发明授权

US09695368B2 Process and apparatus employing microchannel process technology 有权
公开(公告)号：US09695368B2
公开(公告)日：2017-07-04
申请号：US15041119
申请日：2016-02-11
申请人： Velocys, Inc.
发明人： Anna Lee Tonkovich , Ravi Arora , John Brophy , Francis P. Daly , Soumitra Deshmukh , Maddalena Fanelli , Kai Tod Paul Jarosch , Timothy J. LaPlante , Richard Q. Long , Terry Mazanec , Daniel Francis Ryan , Laura J. Silva , Wayne W. Simmons , Bruce Stangeland , Yong Wang , Thomas Yuschak , Steven T. Perry , Jeffrey Dale Marco , Michael Alan Marchiando , Robert Lewis Litt
IPC分类号： C10G47/00 , C10G45/02 , C10G47/02 , C10G47/14 , B01J19/00 , B01J23/42 , B01J23/75 , B01J23/96 , B01J35/02 , C10G2/00 , B01J21/12
CPC分类号： C10G47/14 , B01J19/0093 , B01J21/12 , B01J23/42 , B01J23/75 , B01J23/96 , B01J35/023 , B01J2219/00783 , B01J2219/00788 , B01J2219/00835 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00984 , C10G2/32 , C10G45/02 , C10G47/00 , C10G47/02 , C10G2300/202 , C10G2300/4018 , Y02P20/582
摘要： This invention relates to a process for conducting a hydrocracking or a hydrotreating process in a microchannel reactor. This invention also relates to a process and apparatus for flowing a vapor and liquid into a plurality of microchannels in a microchannel processing unit.

6. 发明申请

US20160264884A1 Process for Preparation of Hydrocracking Catalyst for Use in Hydrocracking of Hydrocarbon Streams 审中-公开
标题翻译：用于烃流加氢裂化的加氢裂化催化剂的制备方法
公开(公告)号：US20160264884A1
公开(公告)日：2016-09-15
申请号：US15085379
申请日：2016-03-30
申请人： Sabic Global Technologies, B.V.
发明人： Ravichander NARAYANASWAMY , Krishna Kumar RAMAMURTHY , Alexander STANISLAUS , Mohammad JAVEED
IPC分类号： C10G65/00
CPC分类号： C10G65/00 , B01J37/20 , C10G1/10 , C10G45/08 , C10G45/10 , C10G47/14 , C10G49/04 , C10G49/06 , C10G2300/202 , C10G2300/4037 , C10G2300/703
摘要： A process for activating and maintaining a catalyst for use in hydrocracking a hydrocarbon stream includes continuously contacting a hydrocarbon stream with a hydroprocessing catalyst in the presence of hydrogen. Sulphides and chloride compounds in the hydrocarbon stream are used such that the hydroprocessing catalyst has the ability to hydrogenate, dechlorinate, and hydrocrack components of the hydrocarbon stream.
摘要翻译：用于活化和维持用于加氢裂化烃流的催化剂的方法包括在氢存在下使烃流与加氢处理催化剂连续接触。使用烃流中的硫化物和氯化物使得加氢处理催化剂具有氢化，脱氯和加氢裂化烃流组分的能力。

7. 发明授权

US09416324B2 Cross flow gas-liquid catalytic reaction systems 有权
标题翻译：横流气液催化反应体系
公开(公告)号：US09416324B2
公开(公告)日：2016-08-16
申请号：US13926413
申请日：2013-06-25
申请人： ExxonMobil Research and Engineering Company
发明人： Hans G. Korsten
IPC分类号： C10G45/00 , C10G45/72 , C10G65/12 , B01J8/04 , B01J8/00 , B01J8/02 , C10G45/10 , C10G47/14 , C10G49/00
CPC分类号： C10G65/12 , B01J8/008 , B01J8/0214 , B01J8/0221 , B01J8/025 , B01J8/0257 , B01J8/0278 , B01J8/0415 , B01J8/043 , B01J8/0453 , B01J8/0469 , B01J8/048 , B01J8/0492 , B01J2208/00884 , B01J2208/00893 , C10G45/00 , C10G45/10 , C10G47/14 , C10G49/002
摘要： A gas-liquid catalyzed reaction is performed by introducing at least a portion of the reactive gas into the catalyst as a cross-flow or radial-flow stream. Introducing at least a portion of the reactive gas as a radial flow stream allows the reactive gas to travel through the catalyst bed along a shorter path length. This reduces the pressure drop for the radial flow portion of the gas. The reactive gas can be introduced into the catalyst bed at various heights relative to the height of the catalyst bed.
摘要翻译：通过将至少一部分反应性气体作为交叉流动或径流流引入催化剂来进行气液催化反应。将反应性气体的至少一部分引入作为径向流动流允许反应性气体沿着较短的路径长度行进通过催化剂床。这降低了气体的径向流动部分的压降。反应气体可以相对于催化剂床的高度以各种高度引入催化剂床。

8. 发明申请

US20150166434A1 PROCESS FOR PRODUCING BTX FROM A C5-C12 HYDROCARBON MIXTURE 有权
标题翻译：从C5-C12烃油混合生产BTX的方法
公开(公告)号：US20150166434A1
公开(公告)日：2015-06-18
申请号：US14403883
申请日：2013-06-04
申请人： SAUDI BASIC INDUSTRIES CORPORATION
发明人： Andrew Mark Ward
IPC分类号： C07C4/06 , C07C4/14
CPC分类号： C07C4/06 , B01J21/04 , B01J21/08 , B01J23/42 , B01J29/40 , B01J35/0006 , B01J35/1019 , B01J35/1042 , B01J35/1061 , C07C4/14 , C07C2529/44 , C10G45/62 , C10G45/64 , C10G45/70 , C10G47/00 , C10G47/14 , C10G47/18 , C10G47/22 , C10G65/10 , C10G2300/1044 , C10G2400/30
摘要： The present invention relates to a process for producing chemical grade BTX from a mixed feedstream comprising C5-C12 hydrocarbons by contacting said feedstream in the presence of hydrogen with a catalyst having hydrocracking/hydrodesulphurisation activity. Particularly, a process for producing BTX from a feedstream comprising C5-C12 hydrocarbons is provided comprising the steps of: (a) contacting said feedstream in the presence of hydrogen with a combined hydrocracking/hydrodesulphurisation catalyst to produce a hydrocracking product stream comprising BTX; and (b) separating the BTX from the hydrocracking product stream. The hydrocracking/hydrodesulphurisation catalyst comprises 0.1-1 wt-% hydrogenation metal in relation to the total catalyst weight. The hydrocracking/hydrodesulphurisation catalyst further comprises a zeolite having a pore size of 5-8 Å and a silica (SiO2) to alumina (Al2O3) molar ratio of 5-200. The hydrocracking/hydrodesulphurisation conditions include a temperature of 450-580° C., a pressure of 300-5000 kPa gauge and a Weight Hourly Space Velocity of 0.1-10 h−1.
摘要翻译：本发明涉及通过在氢气存在下使所述原料流与具有加氢裂化/加氢脱硫活性的催化剂接触从包含C 5 -C 12烃的混合进料流中生产化学级BTX的方法。特别地，提供了一种从包含C5-C12烃的进料流中生产BTX的方法，包括以下步骤：（a）在氢气存在下将所述原料流与组合的加氢裂化/加氢脱硫催化剂接触以产生包含BTX的加氢裂化产物流; 和（b）从加氢裂化产物流中分离BTX。加氢裂化/加氢脱硫催化剂相对于总催化剂重量包含0.1-1重量％的氢化金属。加氢裂化/加氢脱硫催化剂还包含孔径为5-8的二氧化硅（SiO 2）与氧化铝（Al 2 O 3）摩尔比为5-200的沸石。加氢裂化/加氢脱硫条件包括450-580℃的温度，300-5000kPa表压的压力和0.1-10h-1的重量每小时空间速度。

9. 发明授权

US09056771B2 Gasification of heavy residue with solid catalyst from slurry hydrocracking process 有权
标题翻译：从淤浆加氢裂化过程中用固体催化剂气化重质残渣
公开(公告)号：US09056771B2
公开(公告)日：2015-06-16
申请号：US13236923
申请日：2011-09-20
申请人： Omer Refa Koseoglu , Jean-Pierre Ballaguet
发明人： Omer Refa Koseoglu , Jean-Pierre Ballaguet
IPC分类号： C10G67/12 , C10G47/00 , C10G65/00 , C01B3/36 , C10G65/14 , C10G47/26 , C10G47/06 , C10G47/14
CPC分类号： F01K23/067 , C01B3/36 , C01B2203/0255 , C01B2203/0283 , C01B2203/063 , C10G47/06 , C10G47/10 , C10G47/14 , C10G47/26 , C10G65/14 , C10G67/12 , C10J3/466 , C10J3/82 , C10J2300/0946 , C10J2300/0959 , C10J2300/0976 , C10J2300/1675 , C10J2300/1846 , Y02P20/145
摘要： A cost-effective solution for the disposal of heavy residue bottoms recovered from a slurry hydrocracking process that include solid heterogeneous catalyst particles is provided by their introduction into a membrane wall gasification reactor in the form of a flowable slurry to produce a synthesis gas and, optionally, subjecting the synthesis gas to a water-gas shift reaction to produce a more hydrogen-rich product stream. Process steam and electricity are produced by recovering the sensible heat values from the hot synthesis gas.
摘要翻译：通过将其以可流动浆料的形式引入到膜壁气化反应器中以产生合成气，并且任选地通过任选地提供，用于处理从包括固体非均相催化剂颗粒的浆料加氢裂化过程中回收的重质残渣底物的经济有效的解决方案，使合成气进行水煤气变换反应以产生更富氢的产物流。通过从热合成气中回收显热值来生产蒸汽和电力。

10. 发明申请

US20140183098A1 PREPARATION OF CATALYST 有权
标题翻译：催化剂的制备
公开(公告)号：US20140183098A1
公开(公告)日：2014-07-03
申请号：US14132741
申请日：2013-12-18
申请人： Shell Oil Company
发明人： David Allen COOPER , Sjoerd ALKEMA , Lay Hwa ONG , Bart PELGRIM , Laszlo DOMOKOS , Ferry WINTER
IPC分类号： B01J23/888 , C10G47/20
CPC分类号： B01J23/888 , B01J21/12 , B01J35/1019 , B01J35/1042 , B01J35/1047 , B01J37/0009 , B01J37/0203 , B01J37/03 , B01J37/036 , B01J37/20 , C10G47/12 , C10G47/14
摘要： A process for preparing a hydrocarbon conversion catalyst that comprises a specially made silica-alumina composition and a metal or metal compound selected from Group VIB and Group VIII metals. The silica-alumina composition is made by preparing an aqueous mixture containing aluminum sulfate followed by adding alkali metal aluminate to the mixture to inhance the pH to within specified range and then adding aluminum sulfate to the mixture to lower the pH. Then alkali metal silicate is added followed by several other pH swings to provide a mixture containing silica-alumina. The resulting mixture is treated with an alkaline solution to provide a precipitate solid that is recovered to obtain a silica-alumina composition containing of from 30 to 70% wt silica and of from 70 to 30% wt of alumina.
摘要翻译：一种制备烃转化催化剂的方法，其包含特殊制备的二氧化硅 - 氧化铝组合物和选自VIB族和VIII族金属的金属或金属化合物。二氧化硅 - 氧化铝组合物通过制备含有硫酸铝的含水混合物，然后向混合物中加入碱金属铝酸盐以将pH提高到规定范围内，然后向混合物中加入硫酸铝以降低pH。然后加入碱金属硅酸盐，然后加入几种其它pH波动，以提供含有二氧化硅 - 氧化铝的混合物。所得混合物用碱性溶液处理以提供沉淀固体，回收得到二氧化硅 - 氧化铝组合物，其含有30至70重量％的二氧化硅和70至30重量％的氧化铝。

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