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1. 发明授权

US11158830B2 Perovskite film layer, device and preparation method for effectively improving efficiency of light-emitting device 有权
公开(公告)号：US11158830B2
公开(公告)日：2021-10-26
申请号：US16771230
申请日：2018-12-05
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Jianpu Wang , Nana Wang , Yu Cao , Wei Huang
IPC分类号： H01L51/50 , H01L51/00 , H01L51/52 , H01L51/56
摘要： The disclosure discloses a perovskite film layer, a device and a preparation method for effectively improving the efficiency of perovskite optoelectronics. The perovskite film layer consists of a layer with discontinuous, irregularly distributed perovskite crystal grains and an organic insulating layer with a low refractive index embedded between the perovskite crystal grains. The perovskite crystal grains form a plurality of convex portions, and the organic insulating layer forms a plurality of concave portions between the convex portions. By adding an excess of an alkylammonium salt and/or an organic molecule with a specific functional group to perovskite precursor solution, a concave-convex film layer structure is spontaneously formed, and an upper charge transport layer and an electrode form pleated concave-convex structures. Such a special perovskite thin film structure formed by a simple solution method can effectively improve the light-outcoupling efficiency and enhance the performance of the perovskite light-emitting device.

2. 发明申请

US20200062657A1 METHOD FOR PREPARING COMPOSITE METAL OXIDE HOLLOW FIBRE 审中-公开
公开(公告)号：US20200062657A1
公开(公告)日：2020-02-27
申请号：US16466066
申请日：2017-05-10
申请人： Nanjing University of Technology
发明人： Wanqin JIN , Jiawei ZHU , Zhengkun LIU
IPC分类号： C04B35/622 , C04B35/26 , C04B26/28 , C04B26/10
摘要： The invention relates to a method for preparing a composite metal oxide hollow fibre. A certain stoichiometry of composite metal oxide raw material and a polymer binding agent are added to an organic solvent, and mixed mechanically to obtain an evenly dispersed spinning solution having a suitable viscosity. After defoaming treatment, the spinning solution is extruded through a spinneret and, after undergoing a certain dry spinning process, enters an external coagulation bath; during this period, a phase inversion process occurs and composite metal oxide hollow fibre blanks are formed. The blanks are immersed in the external coagulation bath and the organic solvent is displaced; after natural drying, the blanks undergo a heat treatment process; during this period, polymer burn off, in situ reaction, and in situ sintering processes occur to obtain the composite metal oxide hollow fibre.

3. 发明申请

US20170130254A1 NUCLEOTIDE PRODUCTION PROCESS 审中-公开
公开(公告)号：US20170130254A1
公开(公告)日：2017-05-11
申请号：US15127373
申请日：2014-03-26
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Hanjie YING , Zhi CAO , Yong CHEN , Xiaochun CHEN , Jinglan WU , Jingjing XIE
IPC分类号： C12P19/30
CPC分类号： C12P19/30 , C12Y301/11005
摘要： A nucleotide production process comprises: decomposing an RNA by using a nuclease P1 so as to obtain nucleotides AMP, GMP, CMP and UMP, converting part or all of the nucleotide AMP into a nucleotide IMP by using adenosine deaminase, separating the obtained nucleotide by using an ion exchange resin, and then performing concentration and crystallization to obtain purified nucleotides AMP, GMP, CMP, UMP and IMP or obtain purified nucleotides GMP, CMP, UMP and IMP. The whole biocatalysis production of nucleotides is implemented by using a double-enzyme catalysis method, and high-purity nucleotides are obtained by using an ion resin separation technology and a solvent crystallization method; and the production process is simple and environmentally-friendly, and has low costs, high product safety and purity.

4. 发明授权

US08993810B2 Preparation method of lycopene intermediate 3-methyl-4,4-dialkoxy-1-butaldehyde 有权
标题翻译：番茄红素中间体3-甲基-4,4-二烷氧基-1-丁醛的制备方法
公开(公告)号：US08993810B2
公开(公告)日：2015-03-31
申请号：US14369137
申请日：2012-12-10
申请人： Nanjing University of Technology , Zhejiang Medicine Co., Ltd. Xinchang Pharmaceutical Factory
发明人： Chunlei LV , Shiqing Pi , Jianhui Chen , Dingqiang Lu , Pingkai Ouyang
IPC分类号： C07C45/00 , C07C45/30 , C07C41/22
CPC分类号： C07C45/30 , C07C41/22 , C07C45/00 , C07C45/516 , C07C47/198
摘要： Disclosed is a preparation method of the lycopene intermediate 3-methyl-4,4-dialkoxy-1-butaldehyde. The preparation method comprises the following steps: (1) reacting 2-methyl-3,3-dialkoxy-1-halopropane with magnesium powder in the solvent of anhydrous tetrahydrofuran at a temperature of 45˜65° C. to generate a mixture of Grignard reagents under the protection of an inert gas; and (2) adding N,N-disubstituted carboxamide to the mixture of Grignard reagents and reacting at a temperature of 10° C.˜35° C. to obtain 3-methyl-4,4-dialkoxy-1-butaldehyde. The process route of the present invention is simple and direct, the operation is easy, the conditions are mild and the yield is good, and thus the invention has commercial value.
摘要翻译：公开了番茄红素中间体3-甲基-4,4-二烷氧基-1-丁醛的制备方法。制备方法包括以下步骤：（1）在45〜65℃的温度下，将2-甲基-3,3-二烷氧基-1-卤代丙烷与镁粉末在无水四氢呋喃的溶剂中反应，生成格利雅在惰性气体保护下的试剂; 和（2）将N，N-二取代的甲酰胺加入到格氏试剂混合物中，并在10℃〜35℃的温度下反应，得到3-甲基-4,4-二烷氧基-1-丁醛。本发明的工艺路线简单直接，操作容易，条件温和，产量好，因此本发明具有商业价值。

5. 发明申请

US20150050579A1 MEDIUM AND HIGH-TEMPERATURE CARBON-AIR CELL 有权
标题翻译：中高碳气囊
公开(公告)号：US20150050579A1
公开(公告)日：2015-02-19
申请号：US14387942
申请日：2013-03-26
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Ran Ran , Huangang Shi , Binbin Yang , Guangming Yang , Chao Li , Zongping Shao
IPC分类号： H01M8/12 , H01M8/00 , H01M8/10
CPC分类号： H01M8/1233 , H01M4/9025 , H01M8/004 , H01M8/1009 , H01M8/124 , H01M2008/1293 , H01M2300/0074 , H01M2300/0077 , Y02E60/525 , Y02P70/56
摘要： The present invention relates to a medium and high-temperature carbon-air cell, which include a solid oxide fuel cell, a CO2 separation membrane and a carbon fuel. The solid oxide fuel cell is a tubular solid oxide fuel cell with one end closed, the carbon fuel is placed inside the tubular solid oxide fuel cell, and the CO2 separation membrane is sealed at the open end of the solid oxide fuel cell. In the carbon-air cell, with carbon as fuel and oxygen in the air as an oxidizing gas, electrochemical reactions occur. The carbon-air cell of the present invention has a novel structural design, and can achieve electricity generation with the solid oxide fuel cell without externally charging a gas, and at the same time, CO2 generated inside the solid oxide fuel cell can be discharged from the system through the CO2 separation membrane in time.
摘要翻译：本发明涉及一种中高温碳空气电池，其包括固体氧化物燃料电池，CO 2分离膜和碳燃料。固体氧化物型燃料电池是一端封闭的管状固体氧化物型燃料电池，碳素燃料配置在管状固体氧化物型燃料电池内，CO 2分离膜密封在固体氧化物型燃料电池的开放端。在碳 - 空气池中，作为燃料的碳和空气中的氧作为氧化气体，发生电化学反应。本发明的碳 - 空气电池具有新的结构设计，并且可以在不从外部充入气体的状态下实现固体氧化物型燃料电池的发电，同时可以在固体氧化物型燃料电池内产生的CO 2从系统通过CO2分离膜及时。

6. 发明申请

US20140378711A1 METHOD FOR SYNTHESIZING 2,7-DIMETHYL-2,4,6-OCTATRIENE-1,8-DIALDEHYDE 审中-公开
标题翻译：合成2,7-二甲基-2,4,6-四甲基-1,1-二氢二氢呋喃的方法
公开(公告)号：US20140378711A1
公开(公告)日：2014-12-25
申请号：US14369164
申请日：2012-12-10
申请人： NANJING UNIVERSITY OF TECHNOLOGY , Zhejiang Medicine Co., Ltd. Xinchang Pharmaceutical Factory
发明人： Chunlei LV , Shiqing Pi , Jianhui Chen , Dingqiang Lu , Pingkai Ouyang
IPC分类号： C07C45/42 , C07C1/32 , C07C41/22 , C07F9/38 , C07C41/06 , C07C41/18
CPC分类号： C07C45/42 , C07C1/324 , C07C41/06 , C07C41/18 , C07C41/22 , C07C45/52 , C07F9/38 , C07C47/21
摘要： Provided in the present invention is a method for synthesizing 2,7-dimethyl-2,4,6-octatriene-1,8-dialdehyde. The synthesis method comprises the following steps: (1) adding acetaldehyde diethyl acetal and ethyl-(1-propenyl)-ether under the effect of a catalyst to produce 1,1,3-triethoxy-2-methyl-butane; (2) pyrolysis synthesizing 1,1,3-triethoxy-2-methyl-butane under the catalytic effects of isoquinoline and p-Toluenesulfonic acid to produce 1-methoxy-2-methyl-1,3-butadiene; (3) dissolving 1-methoxy-2-methyl-1,3-butadiene in anhydrous ethanol solvent for synthesis with a phase transfer catalyst, cetyl-trimethyl ammonium bromide, and a chlorinating agent, trichloroisocyanuric acid, to generate 4,4-diethoxy-3-methyl-1-chloro-butene; (4) combining 4,4-diethoxy-3-methyl-1-chloro-butene with a triphenylphosphine salt to produce a phosphonium salt; and (5) condensing the phosphonium salt under the effects of hydrogen peroxide in conjunction with sodium carbonate solution to generate 1,1,8,8-tetramethyl-2,7-dimethyl-2,4,6-octatriene; then hydrolyzing under acidic conditions to synthesize 2,7-dimethyl-2,4,6-octatriene-1,8-dialdehyde. The present invention has a simple process route, is easy to operate, and has mild conditions, great yield, and great industrial value.
摘要翻译：本发明提供了合成2,7-二甲基-2,4,6-辛二烯-1,8-二醛的方法。合成方法包括以下步骤：（1）在催化剂作用下加入乙醛缩二乙醇和乙基 - （1-丙烯基） - 醚，制得1,1,3-三乙氧基-2-甲基 - 丁烷; （2）在异喹啉和对甲苯磺酸的催化作用下热解合成1,1,3-三乙氧基-2-甲基丁烷，得到1-甲氧基-2-甲基-1,3-丁二烯; （3）将1-甲氧基-2-甲基-1,3-丁二烯溶于无水乙醇溶剂中，用相转移催化剂，十六烷基三甲基溴化铵和氯化剂三氯异氰脲酸合成，得到4,4-二乙氧基 -3-甲基-1-氯 - 丁烯; （4）将4,4-二乙氧基-3-甲基-1-氯 - 丁烯与三苯基膦盐结合以产生鏻盐; 和（5）在过氧化氢与碳酸钠溶液的作用下使鏻盐缩合，生成1,1,8,8-四甲基-2,7-二甲基-2,4,6-辛二烯; 然后在酸性条件下水解合成2,7-二甲基-2,4,6-辛二烯-1,8-二醛。本发明工艺路线简单，操作方便，条件温和，产量大，工业价值高。

7. 发明授权

US11278846B2 Method for preparing defect-free DDR molecular sieve membrane 有权
公开(公告)号：US11278846B2
公开(公告)日：2022-03-22
申请号：US16470230
申请日：2017-06-09
申请人： Nanjing University of Technology
发明人： Xuehong Gu , Lin Wang , Chun Zhang
IPC分类号： B01D67/00 , B01D53/22 , B01D71/02 , B01D69/10
摘要： Provided is a method for preparing a defect-free DDR molecular sieve membrane. Sigma-1 molecular sieve is used as an inducing seed crystal to prepare and obtain a continuous and compact DDR molecular sieve membrane on the surface of a porous ceramic support. An ozone atmosphere or an external field assisted technology is used to remove a template in the pores of the molecular sieve membrane at a low temperature. The invention avoids the formation of intercrystal defects and cracks, an activated DDR molecular sieve membrane has a good selectivity for separating CO2, and the membrane preparation time is significantly reduced.

8. 发明授权

US11033884B2 Catalyst for benzene hydroxylation for preparation of phenol and preparation method thereof 有权
公开(公告)号：US11033884B2
公开(公告)日：2021-06-15
申请号：US15028438
申请日：2014-09-12
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Rizhi Chen , Yaohui Bao , Hong Jiang , Yiqun Fan , Weihong Xing
IPC分类号： B01J29/03 , C07C37/58 , B01J35/10 , B01J37/06
摘要： The invention relates to a catalyst for benzene hydroxylation for preparation of phenol and a preparation method thereof, wherein said catalyst uses a mesoporous material as carrier, and the catalyst is prepared by first modifying the surface of the carrier using aminosilane, then immersing with acetylacetonate salt of metal, and finally washing and drying. Advantage of the invention is that a reactive metal is loaded on the silane-modified mesoporous material to form a homogeneous-heterogeneous composite catalyst, wherein, the reactive metal component is present in a reaction system in a homogeneous form, which ensures high catalytic performance of the catalyst component, and it is loaded on the carrier through bridging action of aminosilane, which improves the acting force between the metal component and the carrier, enhances stability of the catalyst, and facilitates separation of the catalyst from the product. The catalyst has a simple preparation process, has excellent catalytic performance, and can be applied to the reaction system of benzene hydroxylation for preparation of phenol.

9. 发明申请

US20160137557A1 Method for Preparing Multichannel Ceramic Hollow Fiber Membrane 审中-公开
标题翻译：多通道陶瓷中空纤维膜的制备方法
公开(公告)号：US20160137557A1
公开(公告)日：2016-05-19
申请号：US14898471
申请日：2014-05-09
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Xuehong GU , Zhenzhou SHI , Yuanyuan CHEN , Chun ZHANG , Nanping XU
IPC分类号： C04B35/622 , B01D69/08 , B01D67/00 , B01D71/02
CPC分类号： C04B35/6225 , B01D67/0041 , B01D69/081 , B01D69/082 , B01D71/024 , B01D71/025 , B01D2325/04 , B01D2325/24 , C04B2235/3246 , C04B2235/6021
摘要： The Invention relates to a method for preparing a multichannel hollow fiber membrane. According to a certain ratio, ceramic powder, a macromolecular polymer, an organic solvent, and a dispersant are mixed evenly to prepare a membrane casting solution; and after bubble removing processing is performed on the membrane casting solution, a membrane green body is formed with the cooperation of a multichannel hollow fiber die and phase inversion. After the membrane green body is roasted at a high temperature, a multichannel ceramic hollow fiber membrane is formed. The multichannel ceramic hollow fiber membrane has an asymmetric structure and a skeleton structure in an inner cavity and can meet the strength and flux requirements of a ceramic hollow fiber membrane.
摘要翻译：本发明涉及一种制备多通道中空纤维膜的方法。按照一定的比例，将陶瓷粉末，高分子聚合物，有机溶剂和分散剂均匀混合以制备膜浇铸溶液; 并且在膜浇铸溶液进行气泡去除处理之后，通过多通道中空纤维管芯的配合形成膜生坯并进行相转化。在高温下烘烤膜生坯后，形成多孔陶瓷中空纤维膜。多通道陶瓷中空纤维膜在内腔中具有不对称结构和骨架结构，可以满足陶瓷中空纤维膜的强度和通量要求。

10. 发明申请

US20160032272A1 PREPARATION METHOD OF YEAST CELL IMMOBILIZATION MEDIUM AND APPLICATION THEREOF 审中-公开
标题翻译： YEAST细胞固定培养基的制备方法及其应用
公开(公告)号：US20160032272A1
公开(公告)日：2016-02-04
申请号：US14651071
申请日：2012-12-13
申请人： NANJING UNIVERSITY OF TECHNOLOGY
发明人： Hanjie YING , Yong CHEN , Qingguo LIU , Jinglan WU , Xiaochun CHEN , Jingjing XIE
IPC分类号： C12N11/08 , C12P7/06
CPC分类号： C12N11/08 , C12N11/02 , C12N11/12 , C12P7/06 , D06M13/123 , D06M13/332 , D06M13/418 , D06M15/59 , Y02E50/17
摘要： Provided is a preparation method of a yeast cell immobilization medium, which comprises the following steps: (1) boiling a fiber material in boiling water and drying the fiber material; (2) soaking the fiber material in a surface modified aqueous solution with a concentration of 1-100 g/L, using hydrochloric acid to adjust a PH of the solution to 7.0, fully rinsing the fiber material in deionized water and drying the fiber material; (3) soaking the fiber material in a cross-linking agent aqueous solution with a concentration of 1-100 g/L, fully rinsing the fiber material in deionized water and drying the fiber material; and (4) attaching the fiber material to supporting framework. Also provided is the yeast cell immobilization medium prepared using the preparation method and a method for producing ethanol using the yeast cell immobilization medium.
摘要翻译：提供酵母细胞固定培养基的制备方法，其包括以下步骤：（1）在沸水中煮沸纤维材料并干燥纤维素材料; （2）将纤维材料浸泡在浓度为1-100g / L的表面改性水溶液中，使用盐酸将溶液的PH调节至7.0，将去离子水中的纤维材料充分漂洗并干燥纤维材料 ; （3）将纤维材料浸泡在浓度为1-100g / L的交联剂水溶液中，在去离子水中充分漂洗纤维材料并干燥纤维材料; 和（4）将纤维材料连接到支撑框架上。还提供了使用制备方法制备的酵母细胞固定培养基和使用酵母细胞固定培养基生产乙醇的方法。

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