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1. 发明申请

US20130257389A1 Supercapacitor with Hexacyanometallate Cathode, Activated Carbone Anode, and Aqueous Electrolyte 有权
标题翻译：超级电容器与六氰基金属阴极，活性炭骨阳极和水电解质
公开(公告)号：US20130257389A1
公开(公告)日：2013-10-03
申请号：US13603322
申请日：2012-09-04
申请人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
IPC分类号： H01G9/155 , H01G9/00 , H02J7/00
CPC分类号： H01G11/30 , Y02E60/13 , Y10T29/417
摘要： A supercapacitor is provided with a method for fabricating the supercapacitor. The method provides dried hexacyanometallate particles having a chemical formula AmM1xM2y(CN)6.pH2O with a Prussian Blue hexacyanometallate, crystal structure, where A is an alkali or alkaline-earth cation, and M1 and M2 are metals with 2+ or 3+ valance positions. The variable m is in the range of 0.5 to 2, x is in the range of 0.5 to 1.5, y is in the range of 0.5 to 1.5, and p is in the range of 0 to 6. The hexacyanometallate particles are mixed with a binder and electronic conductor powder, to form a cathode comprising AmM1xM2y(CN)6.pH2O. The method also forms an activated carbon anode and a membrane separating the cathode from the anode, permeable to A and A′ cations. Finally, an electrolyte is added with a metal salt including A′ cations. The electrolyte may be aqueous.
摘要翻译：超级电容器具有制造超级电容器的方法。该方法提供具有化学式AmM1xM2y（CN）6.pH2O的干燥的六氰基金属盐颗粒与普鲁士蓝六氰基金属酸盐晶体结构，其中A是碱金属或碱土金属阳离子，M1和M2是具有2+或3+价态的金属职位变量m在0.5至2的范围内，x在0.5至1.5的范围内，y在0.5至1.5的范围内，p在0至6的范围内。六氰基金属盐颗粒与粘合剂和电子导体粉末，以形成包含AmM1xM2y（CN )6pH2O的阴极。该方法还形成活性炭阳极和将阴极与阳极分开的膜，其可透过A和A'阳离子。最后，向电解质中加入包含A'阳离子的金属盐。电解质可以是水性的。

2. 发明授权

US09159502B2 Supercapacitor with hexacyanometallate cathode, activated carbon anode, and non-aqueous electrolyte 有权
标题翻译：具有六金属金属阴极，活性炭阳极和非水电解质的超级电容器
公开(公告)号：US09159502B2
公开(公告)日：2015-10-13
申请号：US13603322
申请日：2012-09-04
申请人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
IPC分类号： H01M2/16 , H01G11/30
CPC分类号： H01G11/30 , Y02E60/13 , Y10T29/417
摘要： A supercapacitor is provided with a method for fabricating the supercapacitor. The method provides dried hexacyanometallate particles having a chemical formula AmM1xM2y(CN)6.pH2O with a Prussian Blue hexacyanometallate, crystal structure, where A is an alkali or alkaline-earth cation, and M1 and M2 are metals with 2+ or 3+ valance positions. The variable m is in the range of 0.5 to 2, x is in the range of 0.5 to 1.5, y is in the range of 0.5 to 1.5, and p is in the range of 0 to 6. The hexacyanometallate particles are mixed with a binder and electronic conductor powder, to form a cathode comprising AmM1xM2y(CN)6.pH2O. The method also forms an activated carbon anode and a membrane separating the cathode from the anode, permeable to A and A′ cations. Finally, an electrolyte is added with a metal salt including A′ cations. The electrolyte may be aqueous.
摘要翻译：超级电容器具有制造超级电容器的方法。该方法提供具有化学式AmM1xM2y（CN）6.pH2O的干燥的六氰基金属盐颗粒与普鲁士蓝六氰基金属酸盐晶体结构，其中A是碱金属或碱土金属阳离子，M1和M2是具有2+或3+价态的金属职位变量m在0.5至2的范围内，x在0.5至1.5的范围内，y在0.5至1.5的范围内，p在0至6的范围内。六氰基金属盐颗粒与粘合剂和电子导体粉末，以形成包含AmM1xM2y（CN )6pH2O的阴极。该方法还形成活性炭阳极和将阴极与阳极分开的膜，其可透过A和A'阳离子。最后，向电解质中加入包含A'阳离子的金属盐。电解质可以是水性的。

3. 发明授权

US09099718B2 Transition metal hexacyanoferrate battery cathode with single plateau charge/discharge curve 有权
标题翻译：过渡金属hexacyanoferrate电池阴极与单一平台充电/放电曲线
公开(公告)号：US09099718B2
公开(公告)日：2015-08-04
申请号：US13752930
申请日：2013-01-29
申请人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
发明人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
IPC分类号： H01M8/02 , H01M4/136 , H02J7/00 , H01M4/58 , H01M10/054 , H01M10/0568 , H01M10/44
CPC分类号： H01M4/5825 , H01M4/136 , H01M4/58 , H01M4/625 , H01M10/054 , H01M10/0568 , H01M10/446 , H01M2004/028 , H02J7/0063 , H02J7/0068 , Y02E60/122
摘要： A transition metal hexacyanoferrate (TMH) cathode battery is provided. The battery has a AxMn[Fe(CN)6]y.zH2O cathode, where the A cations are either alkali or alkaline-earth cations, such as sodium or potassium, where x is in the range of 1 to 2, where y is in the range of 0.5 to 1, and where z is in the range of 0 to 3.5. The AxMn[Fe(CN)6]y.zH2O has a rhombohedral crystal structure with Mn2+/3+ and Fe2+3+ having the same reduction/oxidation potential. The battery also has an electrolyte, and anode made of an A metal, an A composite, or a material that can host A atoms. The battery has a single plateau charging curve, where a single plateau charging curve is defined as a constant charging voltage slope between 15% and 85% battery charge capacity. Fabrication methods are also provided.
摘要翻译：提供了一种过渡金属六氰基铁酸盐（TMH）阴极电池。电池具有AxMn [Fe（CN）6] y.zH 2 O阴极，其中A阳离子是碱金属或碱土金属阳离子，如钠或钾，其中x在1至2的范围内，其中y是在0.5至1的范围内，其中z在0至3.5的范围内。 AxMn [Fe（CN）6] y.zH2O具有具有相同还原/氧化电位的Mn2 + / 3 +和Fe2 + 3 +的菱方晶体结构。电池还具有电解质和由A金属，A复合材料或能够承载A原子的材料制成的阳极。电池具有单个平台充电曲线，其中单个平台充电曲线被定义为电池充电容量的15％至85％之间的恒定充电电压斜率。还提供制造方法。

4. 发明申请

US20130257378A1 Transition Metal Hexacyanoferrate Battery Cathode with Single Plateau Charge/Discharge Curve 有权
标题翻译：过渡金属Hexacyanoferrate电池阴极与单一高原充电/放电曲线
公开(公告)号：US20130257378A1
公开(公告)日：2013-10-03
申请号：US13752930
申请日：2013-01-29
申请人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
发明人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
IPC分类号： H01M4/136 , H02J7/00
CPC分类号： H01M4/5825 , H01M4/136 , H01M4/58 , H01M4/625 , H01M10/054 , H01M10/0568 , H01M10/446 , H01M2004/028 , H02J7/0063 , H02J7/0068 , Y02E60/122
摘要： A transition metal hexacyanoferrate (TMH) cathode battery is provided. The battery has a AxMn[Fe(CN)6]y.zH2O cathode, where the A cations are either alkali or alkaline-earth cations, such as sodium or potassium, where x is in the range of 1 to 2, where y is in the range of 0.5 to 1, and where z is in the range of 0 to 3.5. The AxMn[Fe(CN)6]y.zH2O has a rhombohedral crystal structure with Mn2+/3+ and Fe2+3+ having the same reduction/oxidation potential. The battery also has an electrolyte, and anode made of an A metal, an A composite, or a material that can host A atoms. The battery has a single plateau charging curve, where a single plateau charging curve is defined as a constant charging voltage slope between 15% and 85% battery charge capacity. Fabrication methods are also provided.
摘要翻译：提供了一种过渡金属六氰基铁酸盐（TMH）阴极电池。电池具有AxMn [Fe（CN）6] y.zH 2 O阴极，其中A阳离子是碱金属或碱土金属阳离子，如钠或钾，其中x在1至2的范围内，其中y为在0.5至1的范围内，其中z在0至3.5的范围内。 AxMn [Fe（CN）6] y.zH2O具有具有相同还原/氧化电位的Mn2 + / 3 +和Fe2 + 3 +的菱方晶体结构。电池还具有电解质和由A金属，A复合材料或能够承载A原子的材料制成的阳极。电池具有单个平台充电曲线，其中单个平台充电曲线被定义为电池充电容量的15％至85％之间的恒定充电电压斜率。还提供制造方法。

5. 发明授权

US09537192B2 Battery with low temperature molten salt (LTMS) cathode 有权
标题翻译：电池与低温熔盐（LTMS）阴极
公开(公告)号：US09537192B2
公开(公告)日：2017-01-03
申请号：US13564015
申请日：2012-08-01
申请人： Yuhao Lu , Sean Andrew Vail , Gregory M. Stecker , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Gregory M. Stecker , Jong-Jan Lee
IPC分类号： H01M12/08 , H01M2/40 , H01M4/58 , H01M10/39 , H01M8/04276 , H01M8/04
CPC分类号： H01M12/08 , H01M2/40 , H01M4/58 , H01M8/04276 , H01M10/399 , Y02E60/128 , Y02E60/50
摘要： A battery is provided with an associated method for transporting metal-ions in the battery using a low temperature molten salt (LTMS). The battery comprises an anode, a cathode formed from a LTMS having a liquid phase at a temperature of less than 150° C., a current collector submerged in the LTMS, and a metal-ion permeable separator interposed between the LTMS and the anode. The method transports metal-ions from the separator to the current collector in response to the LTMS acting simultaneously as a cathode and an electrolyte. More explicitly, metal-ions are transported from the separator to the current collector by creating a liquid flow of LTMS interacting with the current collector and separator.
摘要翻译：电池具有使用低温熔融盐（LTMS）在电池中输送金属离子的相关方法。电池包括阳极，由LTMS形成的阴极，其温度低于150℃时具有液相，浸没在LTMS中的集电体以及介于LTMS和阳极之间的金属离子可渗透隔板。响应于同时作为阴极和电解质的LTMS，该方法将金属离子从分离器输送到集电器。更明确地说，通过产生与集电器和分离器相互作用的LTMS的液体流，将金属离子从分离器输送到集电器。

6. 发明申请

US20140037999A1 Battery with Low Temperature Molten Salt (LTMS) Cathode 有权
标题翻译：低温熔盐（LTMS）阴极电池
公开(公告)号：US20140037999A1
公开(公告)日：2014-02-06
申请号：US13564015
申请日：2012-08-01
申请人： Yuhao Lu , Sean Andrew Vail , Gregory M. Stecker , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Gregory M. Stecker , Jong-Jan Lee
IPC分类号： H01M4/36 , H01M2/38
CPC分类号： H01M12/08 , H01M2/40 , H01M4/58 , H01M8/04276 , H01M10/399 , Y02E60/128 , Y02E60/50
摘要： A battery is provided with an associated method for transporting metal-ions in the battery using a low temperature molten salt (LTMS). The battery comprises an anode, a cathode formed from a LTMS having a liquid phase at a temperature of less than 150° C., a current collector submerged in the LTMS, and a metal-ion permeable separator interposed between the LTMS and the anode. The method transports metal-ions from the separator to the current collector in response to the LTMS acting simultaneously as a cathode and an electrolyte. More explicitly, metal-ions are transported from the separator to the current collector by creating a liquid flow of LTMS interacting with the current collector and separator.
摘要翻译：电池具有使用低温熔融盐（LTMS）在电池中输送金属离子的相关方法。电池包括阳极，由LTMS形成的阴极，其温度低于150℃时具有液相，浸没在LTMS中的集电体以及介于LTMS和阳极之间的金属离子可渗透隔板。响应于同时作为阴极和电解质的LTMS，该方法将金属离子从分离器输送到集电器。更明确地说，通过产生与集电器和分离器相互作用的LTMS的液体流，将金属离子从分离器输送到集电器。

7. 发明授权

US09082700B2 Ultraviolet treatment of metal oxide electrodes 有权
标题翻译：金属氧化物电极的紫外线处理
公开(公告)号：US09082700B2
公开(公告)日：2015-07-14
申请号：US13296191
申请日：2011-11-14
申请人： Sean Andrew Vail , David R. Evans , Wei Pan , Jong-Jan Lee
发明人： Sean Andrew Vail , David R. Evans , Wei Pan , Jong-Jan Lee
IPC分类号： H01L21/44 , H01L21/268 , H01G9/20 , H01L21/02 , H01L29/786
CPC分类号： H01L21/2686 , H01G9/2031 , H01G9/2059 , H01L21/02554 , H01L29/7869 , Y02E10/542
摘要： An ultraviolet treatment method is provided for a metal oxide electrode. A metal oxide electrode is exposed to an ultraviolet (UV) light source in a humid environment. The metal oxide electrode is then treated with a moiety having at least one anchor group, where the anchor group is a chemical group capable of promoting communication between the moiety and the metal oxide electrode. As a result, the moiety is bound to the metal oxide electrode. In one aspect the metal oxide electrode is treated with a photoactive moiety. Exposing the metal oxide electrode to the UV light source in the humid environment induces surface defects in the metal oxide electrode in the form of oxygen vacancies. In response to the humidity, atmospheric water competes favorably with oxygen for dissociative adsorption on the metal oxide electrode surface, and hydroxylation of the metal oxide electrode surface is induced.
摘要翻译：为金属氧化物电极提供紫外线处理方法。金属氧化物电极在潮湿环境中暴露于紫外（UV）光源。然后用具有至少一个锚定基团的部分处理金属氧化物电极，其中锚定基团是能够促进部分和金属氧化物电极之间的连通的化学基团。结果，该部分与金属氧化物电极结合。在一个方面，用光活性部分处理金属氧化物电极。在潮湿环境中将金属氧化物电极暴露于UV光源以氧空位的形式引起金属氧化物电极中的表面缺陷。响应于湿度，大气水与氧反应，在金属氧化物电极表面上进行离解吸附，诱导金属氧化物电极表面的羟基化。

8. 发明申请

US20140134792A1 Solution-Processed Metal Selenide Semiconductor using Deposited Selenium Film 审中-公开
标题翻译：使用沉积的硒膜的溶液加工的金属硒化物半导体
公开(公告)号：US20140134792A1
公开(公告)日：2014-05-15
申请号：US13719052
申请日：2012-12-18
申请人： Sean Andrew Vail , Alexey Koposov , Wei Pan , Gary D. Foley , Jong-Jan Lee
发明人： Sean Andrew Vail , Alexey Koposov , Wei Pan , Gary D. Foley , Jong-Jan Lee
IPC分类号： H01L21/02
CPC分类号： H01L21/02628 , H01L21/02491 , H01L21/02568 , H01L21/02614 , H01L31/0322 , Y02E10/541
摘要： Methods are provided for fabricating a solution-processed metal and mixed-metal selenide semiconductor using a selenium (Se) film layer. One aspect provides a conductive substrate and deposits a first Se film layer over the conductive substrate. A first solution, including a first material set of metal salts, metal complexes, or combinations thereof, is dissolved in a solvent and deposited on the first Se film layer. A first intermediate film comprising metal precursors is formed from corresponding members of the first material set. In one aspect, a plurality of intermediate films is formed using metal precursors from the first material set or a different material set. In another aspect, a second Se film layer is formed overlying the intermediate film(s). Thermal annealing is performed in an environment including hydrogen (H2), hydrogen selenide (H2Se), or Se/H2. The metal precursors are transformed in the intermediate film(s), and a metal selenide-containing semiconductor is formed.
摘要翻译：提供了使用硒（Se）膜层制造溶液处理金属和混合金属硒化物半导体的方法。一个方面提供一种导电衬底并且在导电衬底上沉积第一Se膜层。包括金属盐，金属络合物或其组合的第一材料组合的第一溶液溶解在溶剂中并沉积在第一Se膜层上。包含金属前体的第一中间膜由第一材料组的相应构件形成。在一个方面，使用来自第一材料组或不同材料组的金属前体形成多个中间膜。在另一方面，形成覆盖中间膜的第二Se膜层。在包括氢（H 2），硒化氢（H 2 Se）或Se / H 2的环境中进行热退火。金属前体在中间膜中转变，形成含金属硒化物的半导体。

9. 发明申请

US20140116509A1 Solid-State Dye-Sensitized Solar Cell Using Oxidative Dopant 审中-公开
标题翻译：使用氧化掺杂剂的固态染料敏化太阳能电池
公开(公告)号：US20140116509A1
公开(公告)日：2014-05-01
申请号：US13664256
申请日：2012-10-30
申请人： Sean Andrew Vail , Alexey Koposov , Wei Pan , Gary D. Foley , Jong-Jan Lee
发明人： Sean Andrew Vail , Alexey Koposov , Wei Pan , Gary D. Foley , Jong-Jan Lee
IPC分类号： H01L51/00 , H01B1/12
CPC分类号： H01L51/4226 , H01L51/002 , H01L51/0058 , Y02E10/549
摘要： A solid-state hole transport composite material (ssHTM) is provided. The ssHTM is made from a neutral charge first p-type organic semiconductor, and a chemically oxidized first p-type semiconductor, where the dopants are silver(I) containing materials. A reduced form of the silver(I) containing material is also retained as functional component in the ssHTM. In one aspect, the silver(I) containing material is silver bis(trifluoromethanesulfonyl)imide (TFSI). In another aspect, the first p-type organic semiconductor is 2,2′,7,7′-tetrakis(N,N-di-p-methoxyphenylamine)-9,9′-spirobifluorene (Spiro-OMeTAD). In one variation, the ssHTM additionally includes a first p-type organic semiconductor doped with an ionic dopant such as lithium (Li+), sodium (Na+), potassium (K+), or combinations of the above-mentioned materials. Also provided are a method for synthesizing the above-described ssHTM, and a solid-state dye solar cell (ssDSC) fabricated from the ssHTM.
摘要翻译：提供固态空穴传输复合材料（ssHTM）。 ssHTM由中性电荷第一p型有机半导体和化学氧化的第一p型半导体制成，其中掺杂剂是含银（I）的材料。含有银（I）的材料的还原形式也作为ssHTM中的功能组分保留。一方面，含有银（I）的材料是双（三氟甲磺酰）酰亚胺（TFSI）。另一方面，第一p型有机半导体是2,2'，7,7'-四（N，N-二 - 对甲氧基苯胺）-9,9'-螺二芴（Spiro-OMeTAD）。在一个实施方案中，ssHTM还包括掺杂有离子掺杂剂如锂（Li +），钠（Na +），钾（K +）或上述材料的组合的第一p型有机半导体。还提供了合成上述ssHTM的方法和由ssHTM制造的固态染料太阳能电池（ssDSC）。

10. 发明申请

US20140255770A1 Carbon-Sulfur Composite Cathode Passivation and Method for Making Same 审中-公开
标题翻译：碳硫复合阴极钝化及其制备方法
公开(公告)号：US20140255770A1
公开(公告)日：2014-09-11
申请号：US13793559
申请日：2013-03-11
申请人： Jong-Jan Lee , Sean Andrew Vail
发明人： Jong-Jan Lee , Sean Andrew Vail
IPC分类号： H01M4/36 , H01M4/1393 , H01M4/04
CPC分类号： H01M4/366 , H01M4/0404 , H01M4/133 , H01M4/136 , H01M4/1393 , H01M4/1397 , H01M4/62 , H01M10/052
摘要： A method is provided for forming a carbon-sulfur (C—S) battery cathode. The method forms a C—S nanocomposite material overlying metal current collector. A dielectric is formed overlying the C—S material that is permeable to lithium (Li) ions and electrolyte, but impermeable to polysulfides. Typically, the C—S nanocomposite material is porous and the dielectric forms a uniform coating of dielectric inside C—S nanocomposite pores. The dielectric includes a metal (M) oxide with an oxy bridge formation (M-O-M). The metal (M) may, for example, be Mg, Al, Si, Ti, Zn, In, Sn, Mn, Ni, or Cu. A C—S battery cathode, and a battery with a C—S are also provided.
摘要翻译：提供了形成碳 - 硫（C-S）电池阴极的方法。该方法形成了覆盖金属集电器的C-S纳米复合材料。形成电介质覆盖可透过锂（Li）离子和电解质但对多硫化物不渗透的C-S材料。通常，C-S纳米复合材料是多孔的，并且电介质在C-S纳米复合材料孔内形成均匀的电介质涂层。电介质包括具有氧桥形成（M-O-M）的金属（M）氧化物。金属（M）可以是例如Mg，Al，Si，Ti，Zn，In，Sn，Mn，Ni或Cu。还提供C-S电池阴极和具有C-S的电池。

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