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1. 发明授权

US09559358B2 Alkali and alkaline-earth ion batteries with hexacyanometallate cathode and non-metal anode 有权
标题翻译：碱金属和碱土金属离子电池与六金属金属阴极和非金属阳极
公开(公告)号：US09559358B2
公开(公告)日：2017-01-31
申请号：US13449195
申请日：2012-04-17
申请人： Yuhao Lu , Jong-Jan Lee , Motoaki Nishijima , Seizoh Kakimoto
发明人： Yuhao Lu , Jong-Jan Lee , Motoaki Nishijima , Seizoh Kakimoto
IPC分类号： H01M4/58 , H01M4/04 , H01M4/136 , H01M4/587 , H01M4/139 , H01M4/02 , H01M10/36 , H01M10/054
CPC分类号： H01M4/58 , H01M4/0404 , H01M4/0438 , H01M4/0445 , H01M4/0459 , H01M4/136 , H01M4/139 , H01M4/587 , H01M10/054 , H01M10/36 , H01M2004/028 , Y02E60/122
摘要： A battery structure is provided for making alkali ion and alkaline-earth ion batteries. The battery has a hexacyanometallate cathode, a non-metal anode, and non-aqueous electrolyte. A method is provided for forming the hexacyanometallate battery cathode and non-metal battery anode prior to the battery assembly. The cathode includes hexacyanometallate particles overlying a current collector. The hexacyanometallate particles have the chemical formula A′n′AmM1xM2y(CN)6, and have a Prussian Blue hexacyanometallate crystal structure.
摘要翻译：提供用于制造碱性离子和碱土离子电池的电池结构。电池具有六金属金属阴极，非金属阳极和非水电解质。提供了一种用于在电池组装之前形成六氰基金属盐电池阴极和非金属电池阳极的方法。阴极包括覆盖集电器的六氰基金属盐颗粒。六氰基金属盐颗粒具有化学式A'n'AmM1xM2y（CN）6，并具有普鲁士蓝六氰基金属酸盐晶体结构。

2. 发明申请

US20130260222A1 Electrode Forming Process for Metal-Ion Battery with Hexacyanometallate Electrode 有权
标题翻译：金属离子电池与六氰基金属电极的电极成型工艺
公开(公告)号：US20130260222A1
公开(公告)日：2013-10-03
申请号：US13432993
申请日：2012-03-28
申请人： Yuhao Lu , Jong-Jan Lee
发明人： Yuhao Lu , Jong-Jan Lee
IPC分类号： H01M4/38 , H01M4/02 , H01M4/40 , H01M4/58 , H01M10/02
CPC分类号： H01M4/58 , H01M4/0404 , H01M4/0438 , H01M4/0445 , H01M4/0459 , H01M4/139 , H01M4/587 , H01M10/054
摘要： A method is provided for forming a metal-ion battery electrode with large interstitial spacing. A working electrode with hexacyanometallate particles overlies a current collector. The hexacyanometallate particles have a chemical formula AmM1xM2y(CN)6·zH2O, and have a Prussian Blue hexacyanometallate crystal structure, where A is either alkali or alkaline-earth cations. M1 and M2 are metals with 2+ or 3+ valance positions. The working electrode is soaked in an organic first electrolyte including a salt including alkali or alkaline earth cations. A first electric field is created in the first electrolyte between the working electrode and a first counter electrode, causing A cations and water molecules to he simultaneously removed from interstitial spaces in the Prussian Blue hexacyanometallate crystal structure, forming hexacyanometallate particles having the chemical formula of Am′mM1xM2y(CN)6·z′H2O, where m′
摘要翻译：提供一种用于形成具有大间隙间距的金属离子电池电极的方法。具有六氰基金属酸盐颗粒的工作电极覆盖集电器。六氰基金属盐颗粒具有化学式AmM1xM2y（CN）6·zH2O，并具有普鲁士蓝六氰基金属酸盐晶体结构，其中A为碱金属或碱土金属阳离子。 M1和M2是具有2+或3+价位的金属。将工作电极浸渍在包含碱金属或碱土金属阳离子的盐的有机第一电解质中。在工作电极和第一对电极之间的第一电解质中产生第一电场，使得阳离子和水分子同时从普鲁士蓝六氰基金属酸盐晶体结构中的间隙中除去，形成化学式为Am的六氰基金属盐颗粒 'mM1xM2y（CN）6·z'H2O，其中m'

3. 发明授权

US09537192B2 Battery with low temperature molten salt (LTMS) cathode 有权
标题翻译：电池与低温熔盐（LTMS）阴极
公开(公告)号：US09537192B2
公开(公告)日：2017-01-03
申请号：US13564015
申请日：2012-08-01
申请人： Yuhao Lu , Sean Andrew Vail , Gregory M. Stecker , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Gregory M. Stecker , Jong-Jan Lee
IPC分类号： H01M12/08 , H01M2/40 , H01M4/58 , H01M10/39 , H01M8/04276 , H01M8/04
CPC分类号： H01M12/08 , H01M2/40 , H01M4/58 , H01M8/04276 , H01M10/399 , Y02E60/128 , Y02E60/50
摘要： A battery is provided with an associated method for transporting metal-ions in the battery using a low temperature molten salt (LTMS). The battery comprises an anode, a cathode formed from a LTMS having a liquid phase at a temperature of less than 150° C., a current collector submerged in the LTMS, and a metal-ion permeable separator interposed between the LTMS and the anode. The method transports metal-ions from the separator to the current collector in response to the LTMS acting simultaneously as a cathode and an electrolyte. More explicitly, metal-ions are transported from the separator to the current collector by creating a liquid flow of LTMS interacting with the current collector and separator.
摘要翻译：电池具有使用低温熔融盐（LTMS）在电池中输送金属离子的相关方法。电池包括阳极，由LTMS形成的阴极，其温度低于150℃时具有液相，浸没在LTMS中的集电体以及介于LTMS和阳极之间的金属离子可渗透隔板。响应于同时作为阴极和电解质的LTMS，该方法将金属离子从分离器输送到集电器。更明确地说，通过产生与集电器和分离器相互作用的LTMS的液体流，将金属离子从分离器输送到集电器。

4. 发明授权

US09159502B2 Supercapacitor with hexacyanometallate cathode, activated carbon anode, and non-aqueous electrolyte 有权
标题翻译：具有六金属金属阴极，活性炭阳极和非水电解质的超级电容器
公开(公告)号：US09159502B2
公开(公告)日：2015-10-13
申请号：US13603322
申请日：2012-09-04
申请人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
IPC分类号： H01M2/16 , H01G11/30
CPC分类号： H01G11/30 , Y02E60/13 , Y10T29/417
摘要： A supercapacitor is provided with a method for fabricating the supercapacitor. The method provides dried hexacyanometallate particles having a chemical formula AmM1xM2y(CN)6.pH2O with a Prussian Blue hexacyanometallate, crystal structure, where A is an alkali or alkaline-earth cation, and M1 and M2 are metals with 2+ or 3+ valance positions. The variable m is in the range of 0.5 to 2, x is in the range of 0.5 to 1.5, y is in the range of 0.5 to 1.5, and p is in the range of 0 to 6. The hexacyanometallate particles are mixed with a binder and electronic conductor powder, to form a cathode comprising AmM1xM2y(CN)6.pH2O. The method also forms an activated carbon anode and a membrane separating the cathode from the anode, permeable to A and A′ cations. Finally, an electrolyte is added with a metal salt including A′ cations. The electrolyte may be aqueous.
摘要翻译：超级电容器具有制造超级电容器的方法。该方法提供具有化学式AmM1xM2y（CN）6.pH2O的干燥的六氰基金属盐颗粒与普鲁士蓝六氰基金属酸盐晶体结构，其中A是碱金属或碱土金属阳离子，M1和M2是具有2+或3+价态的金属职位变量m在0.5至2的范围内，x在0.5至1.5的范围内，y在0.5至1.5的范围内，p在0至6的范围内。六氰基金属盐颗粒与粘合剂和电子导体粉末，以形成包含AmM1xM2y（CN )6pH2O的阴极。该方法还形成活性炭阳极和将阴极与阳极分开的膜，其可透过A和A'阳离子。最后，向电解质中加入包含A'阳离子的金属盐。电解质可以是水性的。

5. 发明申请

US20130257378A1 Transition Metal Hexacyanoferrate Battery Cathode with Single Plateau Charge/Discharge Curve 有权
标题翻译：过渡金属Hexacyanoferrate电池阴极与单一高原充电/放电曲线
公开(公告)号：US20130257378A1
公开(公告)日：2013-10-03
申请号：US13752930
申请日：2013-01-29
申请人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
发明人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
IPC分类号： H01M4/136 , H02J7/00
CPC分类号： H01M4/5825 , H01M4/136 , H01M4/58 , H01M4/625 , H01M10/054 , H01M10/0568 , H01M10/446 , H01M2004/028 , H02J7/0063 , H02J7/0068 , Y02E60/122
摘要： A transition metal hexacyanoferrate (TMH) cathode battery is provided. The battery has a AxMn[Fe(CN)6]y.zH2O cathode, where the A cations are either alkali or alkaline-earth cations, such as sodium or potassium, where x is in the range of 1 to 2, where y is in the range of 0.5 to 1, and where z is in the range of 0 to 3.5. The AxMn[Fe(CN)6]y.zH2O has a rhombohedral crystal structure with Mn2+/3+ and Fe2+3+ having the same reduction/oxidation potential. The battery also has an electrolyte, and anode made of an A metal, an A composite, or a material that can host A atoms. The battery has a single plateau charging curve, where a single plateau charging curve is defined as a constant charging voltage slope between 15% and 85% battery charge capacity. Fabrication methods are also provided.
摘要翻译：提供了一种过渡金属六氰基铁酸盐（TMH）阴极电池。电池具有AxMn [Fe（CN）6] y.zH 2 O阴极，其中A阳离子是碱金属或碱土金属阳离子，如钠或钾，其中x在1至2的范围内，其中y为在0.5至1的范围内，其中z在0至3.5的范围内。 AxMn [Fe（CN）6] y.zH2O具有具有相同还原/氧化电位的Mn2 + / 3 +和Fe2 + 3 +的菱方晶体结构。电池还具有电解质和由A金属，A复合材料或能够承载A原子的材料制成的阳极。电池具有单个平台充电曲线，其中单个平台充电曲线被定义为电池充电容量的15％至85％之间的恒定充电电压斜率。还提供制造方法。

6. 发明授权

US09269953B2 Electrode forming process for metal-ion battery with hexacyanometallate electrode 有权
标题翻译：金属离子电池与六金属金属电极的电极形成工艺
公开(公告)号：US09269953B2
公开(公告)日：2016-02-23
申请号：US13432993
申请日：2012-03-28
申请人： Yuhao Lu , Jong-Jan Lee
发明人： Yuhao Lu , Jong-Jan Lee
IPC分类号： H01M4/38 , H01M10/04 , H01M4/29 , H01M4/58 , H01M4/04 , H01M10/054
CPC分类号： H01M4/58 , H01M4/0404 , H01M4/0438 , H01M4/0445 , H01M4/0459 , H01M4/139 , H01M4/587 , H01M10/054
摘要： A method is provided for forming a metal-ion battery electrode with large interstitial spacing. A working electrode with hexacyanometallate particles overlies a current collector. The hexacyanometallate particles have a chemical formula AmM1xM2y(CN)6.zH2O, and have a Prussian Blue hexacyanometallate crystal structure, where A is either alkali or alkaline-earth cations. M1 and M2 are metals with 2+ or 3+ valance positions. The working electrode is soaked in an organic first electrolyte including a salt including alkali or alkaline earth cations. A first electric field is created in the first electrolyte between the working electrode and a first counter electrode, causing A cations and water molecules to be simultaneously removed from interstitial spaces in the Prussian Blue hexacyanometallate crystal structure, forming hexacyanometallate particles having the chemical formula of Am′M1xM2y(CN)6.z′H2O, where m′
摘要翻译：提供一种用于形成具有大间隙间距的金属离子电池电极的方法。具有六氰基金属酸盐颗粒的工作电极覆盖集电器。六氰基金属盐颗粒具有化学式AmM1xM2y（CN）6.zH2O，并具有普鲁士蓝六氰基金属酸盐晶体结构，其中A为碱金属或碱土金属阳离子。 M1和M2是具有2+或3+价位的金属。将工作电极浸渍在包含碱金属或碱土金属阳离子的盐的有机第一电解质中。在工作电极和第一对电极之间的第一电解质中产生第一电场，从而在普鲁士蓝六氰基金属酸盐晶体结构中的间隙中同时去除阳离子和水分子，形成化学式为Am的六氰基金属盐颗粒 'M1xM2y（CN）6.z'H2O，其中m'

7. 发明申请

US20130260021A1 Electron Transport in Hexacyanometallate Electrode for Electrochemical Applications 有权
标题翻译：用于电化学应用的六氰基金属酸盐电极中的电子传输
公开(公告)号：US20130260021A1
公开(公告)日：2013-10-03
申请号：US13523694
申请日：2012-06-14
申请人： Yuhao Lu , Jong-Jan Lee
发明人： Yuhao Lu , Jong-Jan Lee
IPC分类号： H01B1/04 , C01C3/08 , H01M4/04 , B05D3/00 , B82Y30/00 , B82Y99/00
CPC分类号： H01B1/122 , B82Y30/00 , H01M4/0404 , H01M4/133 , H01M4/587
摘要： A structure of intimately contacting carbon-hexacyanometallate is provided for forming a metal-ion battery electrode. Several methods are provided for forming the carbon-hexacyanometallate intimate contact. These methods include (1) adding conducting carbon during the synthesis of hexacyanometallate and forming the carbon-hexacyanometallate powder prior to forming the paste for electrode printing; (2) coating with conducting carbon after hexacyanometallate powder formation and prior to forming the paste for electrode printing; and (3) coating a layer of conducting carbon over the hexacyanometallate electrode.
摘要翻译：为了形成金属离子电池电极，提供了紧密接触六氰基金属碳酸盐的结构。提供几种形成碳六氰基金属酸盐紧密接触的方法。这些方法包括（1）在合成六氰基金属盐酸盐期间加入导电碳，并在形成用于电极印刷的糊料之前形成碳 - 六金属金属酸盐粉末; （2）在六金属金属酸盐粉末形成之后，在形成用于电极印刷的糊料之前用导电碳涂覆; 和（3）在六氰基金属盐电极上涂覆一层导电碳。

8. 发明申请

US20130257389A1 Supercapacitor with Hexacyanometallate Cathode, Activated Carbone Anode, and Aqueous Electrolyte 有权
标题翻译：超级电容器与六氰基金属阴极，活性炭骨阳极和水电解质
公开(公告)号：US20130257389A1
公开(公告)日：2013-10-03
申请号：US13603322
申请日：2012-09-04
申请人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
发明人： Yuhao Lu , Sean Andrew Vail , Hidayat Kisdarjono , Jong-Jan Lee
IPC分类号： H01G9/155 , H01G9/00 , H02J7/00
CPC分类号： H01G11/30 , Y02E60/13 , Y10T29/417
摘要： A supercapacitor is provided with a method for fabricating the supercapacitor. The method provides dried hexacyanometallate particles having a chemical formula AmM1xM2y(CN)6.pH2O with a Prussian Blue hexacyanometallate, crystal structure, where A is an alkali or alkaline-earth cation, and M1 and M2 are metals with 2+ or 3+ valance positions. The variable m is in the range of 0.5 to 2, x is in the range of 0.5 to 1.5, y is in the range of 0.5 to 1.5, and p is in the range of 0 to 6. The hexacyanometallate particles are mixed with a binder and electronic conductor powder, to form a cathode comprising AmM1xM2y(CN)6.pH2O. The method also forms an activated carbon anode and a membrane separating the cathode from the anode, permeable to A and A′ cations. Finally, an electrolyte is added with a metal salt including A′ cations. The electrolyte may be aqueous.
摘要翻译：超级电容器具有制造超级电容器的方法。该方法提供具有化学式AmM1xM2y（CN）6.pH2O的干燥的六氰基金属盐颗粒与普鲁士蓝六氰基金属酸盐晶体结构，其中A是碱金属或碱土金属阳离子，M1和M2是具有2+或3+价态的金属职位变量m在0.5至2的范围内，x在0.5至1.5的范围内，y在0.5至1.5的范围内，p在0至6的范围内。六氰基金属盐颗粒与粘合剂和电子导体粉末，以形成包含AmM1xM2y（CN )6pH2O的阴极。该方法还形成活性炭阳极和将阴极与阳极分开的膜，其可透过A和A'阳离子。最后，向电解质中加入包含A'阳离子的金属盐。电解质可以是水性的。

9. 发明授权

US09099718B2 Transition metal hexacyanoferrate battery cathode with single plateau charge/discharge curve 有权
标题翻译：过渡金属hexacyanoferrate电池阴极与单一平台充电/放电曲线
公开(公告)号：US09099718B2
公开(公告)日：2015-08-04
申请号：US13752930
申请日：2013-01-29
申请人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
发明人： Yuhao Lu , Hidayat Kisdarjono , Jong-Jan Lee , David Evans
IPC分类号： H01M8/02 , H01M4/136 , H02J7/00 , H01M4/58 , H01M10/054 , H01M10/0568 , H01M10/44
CPC分类号： H01M4/5825 , H01M4/136 , H01M4/58 , H01M4/625 , H01M10/054 , H01M10/0568 , H01M10/446 , H01M2004/028 , H02J7/0063 , H02J7/0068 , Y02E60/122
摘要： A transition metal hexacyanoferrate (TMH) cathode battery is provided. The battery has a AxMn[Fe(CN)6]y.zH2O cathode, where the A cations are either alkali or alkaline-earth cations, such as sodium or potassium, where x is in the range of 1 to 2, where y is in the range of 0.5 to 1, and where z is in the range of 0 to 3.5. The AxMn[Fe(CN)6]y.zH2O has a rhombohedral crystal structure with Mn2+/3+ and Fe2+3+ having the same reduction/oxidation potential. The battery also has an electrolyte, and anode made of an A metal, an A composite, or a material that can host A atoms. The battery has a single plateau charging curve, where a single plateau charging curve is defined as a constant charging voltage slope between 15% and 85% battery charge capacity. Fabrication methods are also provided.
摘要翻译：提供了一种过渡金属六氰基铁酸盐（TMH）阴极电池。电池具有AxMn [Fe（CN）6] y.zH 2 O阴极，其中A阳离子是碱金属或碱土金属阳离子，如钠或钾，其中x在1至2的范围内，其中y是在0.5至1的范围内，其中z在0至3.5的范围内。 AxMn [Fe（CN）6] y.zH2O具有具有相同还原/氧化电位的Mn2 + / 3 +和Fe2 + 3 +的菱方晶体结构。电池还具有电解质和由A金属，A复合材料或能够承载A原子的材料制成的阳极。电池具有单个平台充电曲线，其中单个平台充电曲线被定义为电池充电容量的15％至85％之间的恒定充电电压斜率。还提供制造方法。

10. 发明授权

US08956760B2 Electron transport in hexacyanometallate electrode for electrochemical applications 有权
标题翻译：用于电化学应用的六氰基金属酸盐电极中的电子传输
公开(公告)号：US08956760B2
公开(公告)日：2015-02-17
申请号：US13523694
申请日：2012-06-14
申请人： Yuhao Lu , Jong-Jan Lee
发明人： Yuhao Lu , Jong-Jan Lee
IPC分类号： H01M4/136
CPC分类号： H01B1/122 , B82Y30/00 , H01M4/0404 , H01M4/133 , H01M4/587
摘要： A structure of intimately contacting carbon-hexacyanometallate is provided for forming a metal-ion battery electrode. Several methods are provided for forming the carbon-hexacyanometallate intimate contact. These methods include (1) adding conducting carbon during the synthesis of hexacyanometallate and forming the carbon-hexacyanometallate powder prior to forming the paste for electrode printing; (2) coating with conducting carbon after hexacyanometallate powder formation and prior to forming the paste for electrode printing; and (3) coating a layer of conducting carbon over the hexacyanometallate electrode.
摘要翻译：为了形成金属离子电池电极，提供了紧密接触六氰基金属碳酸盐的结构。提供几种形成碳六氰基金属酸盐紧密接触的方法。这些方法包括（1）在合成六氰基金属盐酸盐期间加入导电碳，并在形成用于电极印刷的糊料之前形成碳 - 六金属金属酸盐粉末; （2）在六金属金属酸盐粉末形成之后，在形成用于电极印刷的糊料之前用导电碳涂覆; 和（3）在六氰基金属盐电极上涂覆一层导电碳。

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