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1. 发明申请

US20080254218A1 Metal Precursor Solutions For Chemical Vapor Deposition 审中-公开
标题翻译：用于化学气相沉积的金属前体溶液
公开(公告)号：US20080254218A1
公开(公告)日：2008-10-16
申请号：US12058200
申请日：2008-03-28
申请人： Xinjian Lei , Liam Quinn , John Anthony Thomas Norman , William Franklin Burgoyne , Gauri Sankar Lal , Michael Ulman , Daniel P. Spence
发明人： Xinjian Lei , Liam Quinn , John Anthony Thomas Norman , William Franklin Burgoyne , Gauri Sankar Lal , Michael Ulman , Daniel P. Spence
IPC分类号： C23C18/44
CPC分类号： C23C16/18 , C23C16/16
摘要： Metal source containing precursor liquid solutions for chemical vapor deposition processes, including atomic layer deposition, for fabricating conformal metal-containing films on substrates are described. More specifically, the metal source precursor liquid solutions are comprised of (i) at least one metal complex selected from β-diketonates, β-ketoiminates, β-diiminates, alkyl metal, metal carbonyl, alkyl metal carbonyl, aryl metal, aryl metal carbonyl, cyclopentadienyl metal, cyclopentadienyl metal isonitrile, cyclopentadienyl metal nitrile, cyclopentadienyl metal carbonyl, metal alkoxide, metal ether alkoxide, and metal amides wherein the ligand can be monodentate, bidentate and multidentate coordinating to the metal atom and the metal is selected from group 2 to 14 elements, and (ii) a solvent selected from organic amides including linear amides and cyclic amides for such metal source containing precursors.
摘要翻译：描述了用于在衬底上制造保形的含金属膜的用于化学气相沉积工艺的包含原子层沉积的前体液体溶液的金属源。更具体地说，金属源前体液体溶液包括（i）至少一种选自β-二酮酸酯，β-酮亚胺酸酯，β-二亚胺，烷基金属，金属羰基，烷基金属羰基，芳基金属，芳基金属羰基，环戊二烯基金属，环戊二烯基金属异腈，环戊二烯基金属腈，环戊二烯基金属羰基，金属醇盐，金属醚醇盐和金属酰胺，其中配体可以是单齿，双齿和多齿配位的金属原子，金属选自组2 14元素，和（ii）选自有机酰胺的溶剂，包括用于这种含金属源的前体的线性酰胺和环状酰胺。

2. 发明申请

US20100119726A1 Group 2 Metal Precursors For Deposition Of Group 2 Metal Oxide Films 审中-公开
标题翻译：第2组金属前体用于沉积第2组金属氧化物膜
公开(公告)号：US20100119726A1
公开(公告)日：2010-05-13
申请号：US12266806
申请日：2008-11-07
申请人： Xinjian Lei , Daniel P. Spence , John Anthony Thomas Norman , Michael Ulman
发明人： Xinjian Lei , Daniel P. Spence , John Anthony Thomas Norman , Michael Ulman
IPC分类号： C07C249/00 , C07D307/08 , C09D4/00 , B05D5/12 , C23C4/10
CPC分类号： C07C225/14 , C23C16/403 , C23C16/404
摘要： This invention is related to Group 2 metal-containing polydentate β-ketoiminate precursors and compositions comprising Group 2 metal-containing polydentate β-ketoiminate precursors, wherein the polydentate β-ketoiminate precursors incorporate an alkoxy group in the imino portion of the molecule. The compounds and compositions are useful for fabricating metal containing films on substrates such as silicon, metal nitride, metal oxide and other metal layers via chemical vapor deposition (CVD) processes.
摘要翻译：本发明涉及含有第2族金属的多齿骨架和酮基组合物前体和包含第2族金属的多齿骨架 - 酮基亚胺前体的组合物，其中多齿骨架和重沸石前体在分子的亚氨基部分中并入烷氧基。这些化合物和组合物可用于通过化学气相沉积（CVD）工艺在诸如硅，金属氮化物，金属氧化物和其它金属层的衬底上制造含金属膜。

3. 发明授权

US07662959B2 Quaternary trifluoromethylcyclohexane derivatives for liquid crystals 有权
标题翻译：用于液晶的季铵三氟甲基环己烷衍生物
公开(公告)号：US07662959B2
公开(公告)日：2010-02-16
申请号：US11970510
申请日：2008-01-07
申请人： Gauri Sankar Lal , Michael Ulman , David Allen Roberts , Wade Hampton Bailey , William Franklin Burgoyne
发明人： Gauri Sankar Lal , Michael Ulman , David Allen Roberts , Wade Hampton Bailey , William Franklin Burgoyne
IPC分类号： C07D237/00
CPC分类号： C07C31/44 , C07C22/00 , C07C47/353 , C07C69/753 , C07C2601/14 , C09K19/54
摘要： A compound having the structure: w-A-x-CY—Z(CF3), where CY is cyclohexane or substituted cyclohexane, exemplified by 4-trifluoromethyl-4-methylcarboxy-4′-propyl-1,1′-(bi)cyclohexane.
摘要翻译：具有结构：w-A-x-CY-Z（CF 3）的化合物，其中CY是环己烷或取代的环己烷，例如4-三氟甲基-4-甲基羧基-4'-丙基-1,1' - （双）环己烷。

4. 发明申请

US20070248754A1 Metal Complexes of Polydentate Beta-Ketoiminates 有权
标题翻译：多齿β-酮基酮的金属配合物
公开(公告)号：US20070248754A1
公开(公告)日：2007-10-25
申请号：US11735603
申请日：2007-04-16
申请人： Xinjian Lei , Michael Ulman , Liam Quinn , Hansong Cheng
发明人： Xinjian Lei , Michael Ulman , Liam Quinn , Hansong Cheng
IPC分类号： C23C16/00
CPC分类号： C07F9/005 , C07F7/003 , C23C16/40
摘要： A plurality of metal-containing complexes of a polydentate beta-ketoiminate, one embodiment of which is represented by the structure are shown: wherein M is a metal such as calcium, strontium, barium, scandium, yttrium, lanthanum, titanium, zirconium, vanadium, tungsten, manganese, cobalt, iron, nickel, ruthenium, zinc, copper, palladium, platinum, iridium, rhenium, osmium; wherein R1 is selected from the group consisting of alkyl, fluoroalkyl, cycloaliphatic, and aryl, having from 1 to 10 carbon atoms; R2 can be from the group consisting of hydrogen, alkyl, alkoxy, cycloaliphatic, and aryl; R3 is linear or branched selected from the group consisting of alkylene, fluoroalkyl, cycloaliphatic, and aryl; R4 is an alkylene bridge; R5-6 are individually linear or branched selected from the group consisting of alkyl, fluoroalkyl, cycloaliphatic, aryl, and they can be connected to form a ring containing carbon, oxygen, or nitrogen atoms; n is an integer equal to the valence of the metal M.
摘要翻译：多结晶β-酮亚胺酸盐的多金属络合物，其一个实施方案由结构表示：其中M是金属如钙，锶，钡，钪，钇，镧，钛，锆，钒钨，锰，钴，铁，镍，钌，锌，铜，钯，铂，铱，铼，锇; 其中R 1选自具有1至10个碳原子的烷基，氟烷基，脂环族和芳基; R 2可以来自氢，烷基，烷氧基，脂环族和芳基; R 3是直链或支链的，选自亚烷基，氟代烷基，脂环族和芳基; R 4是亚烷基桥; R 5-10各自为直链或支链，选自烷基，氟烷基，脂环族，芳基，并且它们可连接形成含有碳，氧或氮原子的环; n是等于金属M的化合价的整数。

5. 发明授权

US07947814B2 Metal complexes of polydentate beta-ketoiminates 有权
标题翻译：多齿β-酮基亚胺的金属络合物
公开(公告)号：US07947814B2
公开(公告)日：2011-05-24
申请号：US11735603
申请日：2007-04-16
申请人： Xinjian Lei , Michael Ulman , Liam Quinn , Hansong Cheng
发明人： Xinjian Lei , Michael Ulman , Liam Quinn , Hansong Cheng
IPC分类号： C07F5/00
CPC分类号： C07F9/005 , C07F7/003 , C23C16/40
摘要： A plurality of metal-containing complexes of a polydentate beta-ketoiminate, one embodiment of which is represented by the structure are shown: wherein M is a metal such as calcium, strontium, barium, scandium, yttrium, lanthanum, titanium, zirconium, vanadium, tungsten, manganese, cobalt, iron, nickel, ruthenium, zinc, copper, palladium, platinum, iridium, rhenium, osmium; wherein R1 is selected from the group consisting of alkyl, fluoroalkyl, cycloaliphatic, and aryl, having from 1 to 10 carbon atoms; R2 can be from the group consisting of hydrogen, alkyl, alkoxy, cycloaliphatic, and aryl; R3 is linear or branched selected from the group consisting of alkylene, fluoroalkyl, cycloaliphatic, and aryl; R4 is an alkylene bridge; R5-6 are individually linear or branched selected from the group consisting of alkyl, fluoroalkyl, cycloaliphatic, aryl, and they can be connected to form a ring containing carbon, oxygen, or nitrogen atoms; n is an integer equal to the valence of the metal M.
摘要翻译：多结晶β-酮亚胺酸盐的多金属络合物，其一个实施方案由结构表示：其中M是金属如钙，锶，钡，钪，钇，镧，钛，锆，钒钨，锰，钴，铁，镍，钌，锌，铜，钯，铂，铱，铼，锇; 其中R 1选自具有1至10个碳原子的烷基，氟烷基，脂环族和芳基; R2可以来自由氢，烷基，烷氧基，脂环族和芳基组成的组; R3是选自亚烷基，氟代烷基，脂环族和芳基的直链或支链; R4是亚烷基桥; R5-6各自为直链或支链，选自烷基，氟烷基，脂环族，芳基，并且它们可连接形成含有碳，氧或氮原子的环; n是等于金属M的化合价的整数。

6. 发明申请

US20080188689A1 Preparation of organic compounds bearing a trifluoromethyl group on a quaternary carbon 审中-公开
标题翻译：在季碳上制备带有三氟甲基的有机化合物
公开(公告)号：US20080188689A1
公开(公告)日：2008-08-07
申请号：US11702742
申请日：2007-02-06
申请人： Gauri Sankar Lal , Michael Ulman , William Jack Casteel
发明人： Gauri Sankar Lal , Michael Ulman , William Jack Casteel
IPC分类号： C07C17/013 , C07C45/41 , C07C33/14
CPC分类号： C07C29/40 , C07B39/00 , C07C17/2635 , C07C45/004 , C07C45/292 , C07C45/41 , C07C47/353 , C07C49/467 , C07C67/307 , C07C253/30 , C07C2601/14 , C07C22/00 , C07C31/44 , C07C69/753 , C07C255/46
摘要： A method for preparing a molecule bearing a trifluoromethyl group on a quaternary carbon atom, includes providing a reactant having a quaternary carbon atom bearing a carboxylic acid group and an electron withdrawing group; and reacting the reactant with SF4 in a solvent to substitute the carboxylic acid group with the trifluoromethyl group and provide a reaction product mixture including the molecule bearing the trifluoromethyl group on the quaternary carbon atom.
摘要翻译：制备在季碳原子上带有三氟甲基的分子的方法包括提供具有带羧酸基和吸电子基团的季碳原子的反应物; 并使反应物与SF 4在溶剂中反应以用三氟甲基代替羧酸基团，并提供包含在季碳原子上带有三氟甲基的分子的反应产物混合物。

7. 发明授权

US06962964B2 Hydrogenation of methylenedianiline homologs and epoxy resins cured with same 有权
标题翻译：亚甲基二苯胺同系物的氢化和用相同固化的环氧树脂
公开(公告)号：US06962964B2
公开(公告)日：2005-11-08
申请号：US10359450
申请日：2003-02-06
申请人： Michael Ulman , Gamini Ananda Vedage , David Alan Dubowik , Stephen Michael Boyce
发明人： Michael Ulman , Gamini Ananda Vedage , David Alan Dubowik , Stephen Michael Boyce
IPC分类号： C08G59/50 , C08G59/00
CPC分类号： C07C211/49 , C08G59/5026
摘要： This invention relates to improved polyepoxide resins cured with a mixture of methylene bridged poly(cycloaliphatic-aromatic)amines and a process for preparing such polyepoxide resins as well as to the methylene bridged poly(cycloaliphatic-aromatic)amine compositions and a method of making them. The improvement resides in using a curative (herein referred to as “Heavy MPCA”) comprised of the partially hydrogenated condensation product of formaldehyde and aniline or methyl substituted aniline containing a substantial amount (from 35 to 85% by weight, preferably 40 to 60% by weight) of oligomers in the form of 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14 and 15 aniline or methyl substituted aniline derivatives.
摘要翻译：本发明涉及用亚甲基桥连的聚（脂环族 - 芳族）胺的混合物固化的改进的聚环氧化物树脂和制备这种聚环氧化物树脂的方法以及亚甲基桥连的聚（脂环族 - 芳族）胺组合物及其制备方法。改进在于使用由部分氢化的甲醛缩合产物和苯胺或甲基取代的苯胺组成的固化剂（以下称为“重MPCA”），其含有相当量的（35至85重量％，优选40至60重量％（重量）的3,4,5,6,7,8,9,10,11,12,13,14和15苯胺或甲基取代的苯胺衍生物形式的低聚物。

8. 发明授权

US07348103B2 Polyfluorinated boron cluster anions for lithium electrolytes 有权
标题翻译：用于锂电解质的多氟硼簇阴离子
公开(公告)号：US07348103B2
公开(公告)日：2008-03-25
申请号：US10924293
申请日：2004-08-23
申请人： Sergei Vladimirovich Ivanov , William Jack Casteel, Jr. , Guido Peter Pez , Michael Ulman
发明人： Sergei Vladimirovich Ivanov , William Jack Casteel, Jr. , Guido Peter Pez , Michael Ulman
IPC分类号： H01M6/16 , H01M2/26 , H01M6/04 , H01M10/26
CPC分类号： C01B35/06 , H01M10/052 , H01M10/0568
摘要： The present invention relates to an improvement in lithium secondary batteries comprised of a negative electrode, a positive electrode, a separator, and a lithium-based electrolyte carried in an aprotic solvent and to the electrolyte compositions. The improvement resides in the use of a lithium salt of the formula: Li2B12FxZ12-x wherein x greater than or equal to 4 and Z represents H, Cl, and Br.
摘要翻译：本发明涉及由在非质子传递溶剂中负载的负极，正极，隔膜和锂基电解质组成的锂二次电池的改进。改进在于使用下式的锂盐：<？in-line-formula description =“In-line formula”end =“lead”？> Li 2 B 12 β-in-line-formula description =“In-line Formulas”end =“tail”？>其中x大于或等于4，Z表示H，Cl和Br。

9. 发明申请

US20060293397A1 Surfactants derived from phenolic aldehydes 审中-公开
标题翻译：衍生自酚醛的表面活性剂
公开(公告)号：US20060293397A1
公开(公告)日：2006-12-28
申请号：US11159535
申请日：2005-06-23
申请人： Kevin Lassila , Michael Ulman
发明人： Kevin Lassila , Michael Ulman
IPC分类号： B01F17/00 , B01F3/08
CPC分类号： B01F17/0028 , B01F17/0021 , B01F17/0092
摘要： Surfactants derived from phenolic aldehydes include compounds according to formulas (I) and (II) wherein R is (CH2CH2O)xR4 or (C3H6O2)xR4. R1 and R2 are each hydrogen or C1-C20 hydrocarbyl moieties, provided that neither R1 nor R2 may be hydrogen when the compound is of formula (I). If the compound is according to formula (II) wherein n=0, one of R1 and R2 may further be C1-C20 alkoxymethylene while the other is H. The Z moiety is hydrogen, OR, or OR3, wherein R3 is hydrogen, methyl, ethyl or propyl; R4 is hydrogen, methyl or ethyl; x is an integer from 1 to 20; and n is 0 or 1. Compositions containing the surfactants, and methods of using the surfactants, are also disclosed.
摘要翻译：衍生自酚醛的表面活性剂包括根据式（I）和（II）的化合物，其中R是（CH 2 CH 2 CH 2 O）x R 或（C 3）3个或更多个，其中R 1，R 2，R 3， 4 。 R 1和R 2各自为氢或C 1 -C 20烃基部分，条件是R 1和R 2都不为当化合物为式（I）时，可以是氢。如果化合物是其中n = 0的式（II）化合物，R 1和R 2中的一个可以进一步是C 1 -C 20烷氧基亚甲基，而另一个是H. Z部分是氢，OR或OR 3，其中R 3是氢，甲基，乙基或丙基; R 4为氢，甲基或乙基; x是1至20的整数; 并且n是0或1.还公开了含有表面活性剂的组合物和使用表面活性剂的方法。

10. 发明申请

US20050053841A1 Polyfluorinated boron cluster anions for lithium electrolytes 有权
标题翻译：用于锂电解质的多氟硼簇阴离子
公开(公告)号：US20050053841A1
公开(公告)日：2005-03-10
申请号：US10655476
申请日：2003-09-04
申请人： Sergei Ivanov , William Casteel , Guido Pez , Michael Ulman
发明人： Sergei Ivanov , William Casteel , Guido Pez , Michael Ulman
IPC分类号： H01M10/052 , H01M10/0568 , H01M10/40
CPC分类号： C01B35/06 , H01M10/052 , H01M10/0568
摘要： The present invention relates to an improvement in lithium secondary batteries comprised of a negative electrode, a positive electrode, a separator, and a lithium-based electrolyte carried in an aprotic solvent and to the electrolyte compositions. The improvement resides in the use of a lithium electrolyte of the formula: Li2B12FxZ12-x wherein x=>5 and Z represents H, Cl, and Br. Preferably, when x is less than 12, Z is Cl.
摘要翻译：本发明涉及由在非质子传递溶剂中负载的负极，正极，隔膜和锂基电解质组成的锂二次电池的改进。改进在于使用下式的锂电解质：其中x = 5且Z代表H，Cl和Br的Li2B12FxZ12-x。优选地，当x小于12时，Z是Cl。

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