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1. 发明授权

US4097444A Process for the dyeing of water-insoluble thermoplastic polymers and polycondensates in the mass 失效
标题翻译：不溶于水的热塑性聚合物和缩聚物的质量染色方法
公开(公告)号：US4097444A
公开(公告)日：1978-06-27
申请号：US772573
申请日：1977-02-28
申请人： Wolfgang Teige , Rudolf Schickfluss
发明人： Wolfgang Teige , Rudolf Schickfluss
IPC分类号： C08K5/00 , C08K5/35 , C08L1/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L67/00 , C08L67/02 , C08L77/00 , C09B23/00 , C09B23/01 , C09B23/06 , C09B57/00 , C09B69/00 , D06P5/00
CPC分类号： C09B57/00 , C08K5/35 , C09B23/0075 , C09B23/06
摘要： Process for the dyeing of a water-insoluble thermoplastic polymer or polycondensate in mass, which comprises adding to the said thermoplastic material before the final molding thereof, an azlactone dyestuff of the formula (1) ##STR1## in which A and B each represents phenyl, lower alkyl-phenyl, lower alkoxy-phenyl, chlorophenyl, nitrophenyl, cyanophenyl, ##STR2## METHYLENE-DIOXY-PHENYLENE OR NAPHTHYL, A and B being identical or different, D represents phenylene, lower alkyl-phenylene, di-lower alkoxy-phenylene, monochlorophenylene, dichlorophenylene, biphenylene or naphthylene, and n represents the integer 0 or 1, or a mixture of dyestuffs of the said formula (1), the dyeings so obtained representing brilliant yellow dyeings of high tinctorial strength being distinguished by very good fastness to light, rubbing and ironing, and, particularly, by an outstanding stability toward heat.
摘要翻译：用于染色水不溶性热塑性聚合物或缩聚物的方法，其包括在其最终模塑之前向所述热塑性材料中加入式（1）的吖内酯染料（1），其中A和 B各自表示苯基，低级烷基 - 苯基，低级烷氧基 - 苯基，氯苯基，硝基苯基，氰基苯基，亚甲基 - 二苯基或萘基，A和B相同或不同，D表示亚苯基，低级烷基亚苯基，二 - 低级烷氧基 - 亚苯基，一氯代亚苯基，二氯亚苯基，亚联苯基或亚萘基，n表示整数0或1，或所述式（1）的染料混合物，所得到的代表亮度高的亮黄染色的染色被区分通过非常好的耐光牢度，摩擦和熨烫，特别是通过对热量的突出的稳定性。

2. 发明授权

US4093585A Process for the dyeing of water-insoluble thermoplastic polymers and polycondensates in the mass 失效
标题翻译：不溶于水的热塑性聚合物和缩聚物的质量染色方法
公开(公告)号：US4093585A
公开(公告)日：1978-06-06
申请号：US772576
申请日：1977-02-28
申请人： Wolfgang Teige , Rudolf Schickfluss
发明人： Wolfgang Teige , Rudolf Schickfluss
IPC分类号： C08K5/00 , C08K5/35 , C08L1/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L67/00 , C08L67/02 , C08L77/00 , C09B23/00 , C09B23/01 , C09B57/00 , C09B69/00
CPC分类号： C09B23/0075 , C08K5/35 , C09B57/00
摘要： Process for the dyeing of a water-insoluble thermoplastic polymer or polycondensate in mass, which comprises adding to the said thermoplastic material before the final molding thereof an azlactone dyestuff of the formula (1) ##STR1## in which A and B each represents naphthyl, phenyl, chlorophenyl, bromophenyl, lower alkyl-phenyl, lower alkoxyphenyl, nitrophenyl, ##STR2## CYANOPHENYL, DICHLOROPHENYL, CHLORO-LOWER ALKYL-PHENYL, NITRO-LOWER ALKYL-PHENYL, CHLORO-NITROPHENYL, A and B being identical or different, D represents naphthylene, phenylene, monochlorophenylene, dichlorophenylene or di-lower alkoxyphenylene, or with a mixture of dyestuffs of the said formula (1), the dyeings so obtained representing brilliant yellow dyeings of high tinctorial strength being distinguished by very good fastness to light, rubbing and ironing and, particularly, an outstanding stability toward heat.
摘要翻译：水不溶性热塑性聚合物或缩聚物的质量染色方法，其包括在最后成型之前向所述热塑性材料中加入式（1）的吖内酯染料（1），其中A和B 各自表示萘基，苯基，氯苯基，溴苯基，低级烷基 - 苯基，低级烷氧基苯基，硝基苯基，苯甲酰基，二氯苯基，氯代低级烷基 - 苯基，硝基 - 低级烷基 - 苯基，氯代硝基，A和B相同或不同的，D代表亚萘基，亚苯基，一氯代苯，二氯亚苯基或二低级烷氧基亚苯基，或与所述式（1）的染料混合物，所得到的代表亮度高的亮黄染色的染色具有非常好的牢度轻，摩擦和熨烫，特别是对热量的突出稳定性。

3. 发明授权

US4401692A Transfer-printing support 失效
标题翻译：转印支持
公开(公告)号：US4401692A
公开(公告)日：1983-08-30
申请号：US288694
申请日：1981-07-31
申请人： Rudolf Schickfluss , Manfred Schneider , Claus Schuster
发明人： Rudolf Schickfluss , Manfred Schneider , Claus Schuster
IPC分类号： D06P5/00 , D06P5/28 , B41M5/18 , B41M5/20 , C09B29/06 , C09B29/08
CPC分类号： D06P5/006 , Y10S428/913 , Y10S428/914 , Y10S428/915 , Y10S534/01 , Y10T428/24917 , Y10T428/25 , Y10T428/31504 , Y10T428/3179 , Y10T428/31826 , Y10T428/31895 , Y10T428/31982
摘要： Transfer-printing supports, which are impregnated or printed with a formulation containing a mixture of a blue disperse dyestuff which sublimes readily and has the formula ##STR1## in which X is hydrogen or halogen, R, R.sup.1 and R.sup.2 denote alkyl with 1 to 4 carbon atoms and R.sup.3 denotes hydrogen or alkyl with 1 to 4 carbon atoms, and yellow to red disperse dyestuffs which sublime readily, give deep and fast black dyeings on polyester materials and polyester mixed materials by the heat transfer-printing process.
摘要翻译：转印印刷载体用含有易分散的蓝色分散染料和具有其中X为氢或卤素的式“IMAGE”的混合物的制剂浸渍或印刷，R，R 1和R 2表示具有1至4个碳原子，R3表示氢或碳原子数为1〜4的烷基，黄色至红色分散染料，易于染色，通过热转印法在聚酯材料和聚酯混合材料上产生深色和快速的黑色染色。

4. 发明授权

US4293306A Process for the dyeing and printing of hydrophobic synthetic organic fiber materials with water-insoluble azo dyestuffs 失效
标题翻译：用水不溶性偶氮染料染色和印刷疏水性合成有机纤维材料的方法
公开(公告)号：US4293306A
公开(公告)日：1981-10-06
申请号：US118902
申请日：1980-02-06
申请人： Ernst Hoyer , Willi Steckelberg , Walter Deucker , Rudolf Schickfluss
发明人： Ernst Hoyer , Willi Steckelberg , Walter Deucker , Rudolf Schickfluss
IPC分类号： C09B29/36 , C09B31/14 , C09B43/00 , D06P1/18 , D06P5/28
CPC分类号： D06P1/18 , C09B29/3686 , C09B31/14 , C09B43/003 , D06P5/006 , Y10S8/922
摘要： A process for the dyeing or printing of a hydrophobic organic fibrous material containing or consisting of polyester, wherein(a) the fibrous material is dyed (.alpha.) from an aqueous dispersion with a dyestuff of the formula (1) indicated below at a pH value between 2 and 9 and at a temperature above 100.degree. C. or at about 100.degree. C. in the presence of a carrier, or (.beta.) by impregnating it with an aqueous dispersion of a dyestuff of the formula (1), said dispersion having a pH value between 2 and 9, and subsequently exposing the fibrous material so treated to a short heat treatment between about 180.degree. and 210.degree. C., or(b) the fibrous material is printed with a dyestuff of the formula (1) by the transfer printing method, the dyestuff used in methods (a) and (b) being of the formula (1) ##STR1## in which X represents alkyl of 1 to 4 carbon atoms, phenyl, lower alkyl-phenyl, lower alkoxy-phenyl, nitro-phenyl, chloro-phenyl or bromo-phenyl, and D represents phenyl, lower alkyl-phenyl, lower alkoxy-phenylene, nitro-phenylene, chloro-phenylene, benzoyl-phenylene, phenyl-phenylene, phenoxy-phenylene, lower alkyl-sulfonyl-phenylene, aminocarbonyl-phenylene, aminosulfonyl-phenyl, ##STR2## chloro-nitro-phenyl, lower alkyl-nitro-phenyl, lower alkoxy-nitro-phenyl, di(cyano)-phenyl, trifluoromethyl-nitro-phenyl or hydroxyalkoxy-nitro-phenyl.
摘要翻译：用于染色或印刷含有聚酯或由聚酯组成的疏水性有机纤维材料的方法，其中（a）纤维材料用下式表示的式（1）的染料从水分散体染色（α），pH值为 2和9之间，在高于100℃的温度下或在载体存在下在约100℃，或（β）通过用式（1）的染料的水性分散体浸渍，所述分散体 pH值介于2和9之间，随后将经过处理的纤维材料暴露于约180℃至210℃之间的短热处理，或（b）用式（1）的染料印刷纤维材料，通过转印法，在方法（a）和（b）中使用的式（1）的化合物其中X表示1至4个碳原子的烷基，苯基，低级烷基 - 苯基，低级烷氧基 - 苯基，硝基 - 苯基，氯 - 苯基或溴 - 苯基，D代表苯基，低级烷基苯基，低级烷氧基 - 亚苯基，硝基亚苯基，氯 - 亚苯基，苯甲酰基 - 亚苯基，苯基 - 亚苯基，苯氧基 - 亚苯基，低级烷基 - 磺酰基亚苯基，氨基羰基 - 亚苯基，氨基磺酰基 - 苯基，苯基，低级烷基 - 硝基 - 苯基，低级烷氧基 - 硝基 - 苯基，二（氰基） - 苯基，三氟甲基 - 硝基 - 苯基或羟基烷氧基 - 硝基 - 苯基。

5. 发明授权

US3951591A Process for dyeing synthetic fiber materials 失效
标题翻译：染色合成纤维材料的工艺
公开(公告)号：US3951591A
公开(公告)日：1976-04-20
申请号：US408643
申请日：1973-10-23
申请人： Walter Birke , Rudolf Schickfluss , Franz Schon
发明人： Walter Birke , Rudolf Schickfluss , Franz Schon
IPC分类号： C09B29/085 , C09B62/51 , D06P1/90 , D06P1/04 , C09B43/00
CPC分类号： D06P1/908 , C09B62/51 , Y10S8/92 , Y10S8/921 , Y10S8/924 , Y10S8/926 , Y10S8/927 , Y10S8/928
摘要： A process for the continuous dyeing of synthetic fibrous materials from organic solvents, which comprises impregnating the said fibrous materials with organic dyebaths containing at least one dyestuff of the formula (1) ##SPC1##In which R represents a secondary or tertiary amino group of the formula (2) ##EQU1## in which R.sub.4, R.sub.5 each represents, straight chain or branched alkyl, hydroxyalkyl, lower alkyl --COO-- lower alkylene, and R.sub.4 additionally represents hydrogen lower alkyl --o-- lower alkylene, or R.sub.4 and R.sub.5 represent together with the nitrogen atom the heterocyclic ring ##EQU2## R.sub.1 and R.sub.1 ' each represents hydrogen, chlorine, bromine, lower alkyl, lower alkoxy, nitro or --SO.sub.2 -- lower alkyl, R.sub.2 and R.sub.3 each represents hydrogen, lower alkyl, cyano-lower alkylene, hydroxy- lower alkylene, lower alkylene ##EQU3## lower alkyl, lower alkylene LOWER ALKYL, ##EQU4## lower alkylene-phenyl or phenyl, X represents hydrogen, chlorine, bromine, lower alkyl or lower alkoxy, Y represents hydrogen, chlorine, bromine, lower alkyl, lower alkoxy or acylamino, and subsequently fixing the applied dyestuffs by a heat treatment.
摘要翻译：一种用于从有机溶剂中连续染色合成纤维材料的方法，其包括用含有至少一种式（1）的染料的有机染浴浸渍所述纤维材料，其中R表示式（2）的仲或叔氨基）R4 ANGLE N-CH2-CH2-（2）R5其中R4，R5各自表示直链或支链烷基，羟烷基，低级烷基-COO-低级亚烷基，R4另外表示氢低级烷基 - 低级亚烷基，或者R 4和R 5与氮原子一起表示杂环CH 2 -CH 2 CH 2 ANGLE ANGLE N-，CH 2 -CH 2 R 1和R 1'各自表示氢，氯，溴，低级烷基，低级烷氧基，硝基或-SO 2 - 低级烷基，R 2和R 3各自表示氢，低级烷基，氰基 - 低级亚烷基，羟基 - 低级亚烷基，低级亚烷基-CO-仲丁基低级烷基，低级亚烷基低级烷基，-OC-对映异构体低级亚烷基 - 苯基或苯基，X表示氢，氯，溴，低烷基或低级烷氧基，Y代表氢，氯，溴，低级烷基，低级烷氧基或酰基氨基，并随后通过热处理固定所施加的染料。

6. 发明授权

US4460375A Dyeing-stable monoazo dyestuff, a process for its preparation, and its use 失效
标题翻译：染色稳定的单偶氮染料，其制备方法及其用途
公开(公告)号：US4460375A
公开(公告)日：1984-07-17
申请号：US551271
申请日：1983-11-14
申请人： Karl Sommer , Manfred Schneider , Rudolf Schickfluss
发明人： Karl Sommer , Manfred Schneider , Rudolf Schickfluss
IPC分类号： C09B67/48 , C09B29/08 , C09B29/085 , C09B67/00 , C09B67/10
CPC分类号： C09B29/081 , C09B29/0834 , C09B67/0015 , C09B67/0029 , Y10S8/921 , Y10S8/922
摘要： A dyeing-stable modification (.beta.-modification) of the dyestuff of the formula (I) ##STR1## which has the X-ray diffraction diagram shown in FIG. 1 and having the characteristic reflections at the following glancing angles and relative intensities:______________________________________ [.theta.] 2.74 4.27 4.70 5.50 8.74 11.24 12.44 relative 100 72 40 23 27 32 26 intensity ______________________________________ a process for its preparation by heating the dyestuff of said formula (I) of the dyeing-unstable .alpha.-modification, characterized by an X-ray diffraction diagram having the characteristic reflections at the following glancing angles and relative intensities______________________________________ [.theta.] 3.55 4.15 5.35 9.45 10.41 12.71 13.89 relative 42 100 35 24 34 94 48 intensity ______________________________________ at temperatures of 60.degree. to 120.degree. C. in an organic solvent, and its use for dyeing fiber materials made of cellulose esters or synthetic linear polyesters.
摘要翻译：具有图1所示的X射线衍射图的式（I）染料的染色稳定性改性（β-改性）图像（I）。具有以下扫掠角度和相对强度的特征反射：-θ2.74 4.27 4.70 5.50 8.74 11.24 12.44相对100 72 40 23 27 32 26 - 强度 - 通过加热所述式（I）染色不稳定的α-改性，其特征在于具有以下扫掠角度的特征反射和相对强度的X射线衍射图-θ3.55 4.15 5.35 9.45 10.41 12.71 13.89相对值42 100 35 24 34 94 48-密度 - 在有机溶剂中在60℃至120℃的温度下，以及其用于由纤维素酯或合成线性聚酯制成的纤维材料的染色用途。

7. 发明授权

US4422854A Transfer printing support, process for the manufacture thereof, with blue azo dye:di-cyano-nitro-phenyl-azo aniline 失效
标题翻译：用蓝色偶氮染料：二氰基 - 硝基 - 苯基 - 偶氮苯胺的转印印刷载体，其制备方法
公开(公告)号：US4422854A
公开(公告)日：1983-12-27
申请号：US383732
申请日：1982-06-01
申请人： Reinhard Hahnle , Manfred Schneider , Claus Schuster , Rudolf Schickfluss
发明人： Reinhard Hahnle , Manfred Schneider , Claus Schuster , Rudolf Schickfluss
IPC分类号： D06P5/00 , B41J2/325 , B41M5/385 , B41M5/388 , B41M5/39 , D06P5/28 , B41M5/02
CPC分类号： D06P5/006 , Y10S8/922
摘要： Transfer printing supports impregnated or printed with a formulation containing a dyestuff of the formula I ##STR1## in which R.sup.1 is alkyl having from 1 to 4 carbon atoms, R.sup.2 is hydrogen or has the meaning of R.sup.1, R.sup.3 is methyl, methoxy or ethoxy, and R.sup.4 is hydrogen, methyl, methoxy or ethoxy, or containing mixtures of such dyestuffs, a process for the manufacture of these supports, which comprises impregnating or printing the support material with formulations containing a dyestuff of the formula I or mixtures of such dyestuffs, and the use of these supports for the dyeing and printing of flat web or sheet structures of synthetic or natural materials according to the heat transfer printing process.
摘要翻译：用含有式I的染料（I）的制剂浸渍或印刷的转印印刷载体，其中R 1是具有1至4个碳原子的烷基，R 2是氢或具有R 1的意义，R 3是甲基，甲氧基或乙氧基，R 4为氢，甲基，甲氧基或乙氧基，或含有这些染料的混合物，制备这些载体的方法，其包括用含有式I染料的制剂浸渍或印刷载体材料或这种染料，以及根据热转印印刷方法使用这些载体用于染色和印刷合成或天然材料的平板或片状结构。

8. 发明授权

US4381262A Water-insoluble azo dyestuffs, their manufacture and their use 失效
标题翻译：水不溶性偶氮染料，其制造及其用途
公开(公告)号：US4381262A
公开(公告)日：1983-04-26
申请号：US349574
申请日：1982-02-17
申请人： Ulrich Buhler , Dieter Cornelius , Rudolf Lowenfeld , Uwe Kosubek , Reinhard Hahnle , Rudolf Schickfluss
发明人： Ulrich Buhler , Dieter Cornelius , Rudolf Lowenfeld , Uwe Kosubek , Reinhard Hahnle , Rudolf Schickfluss
IPC分类号： C09B29/085 , C09B29/08 , C09B43/42
CPC分类号： C09B43/42 , C09B29/081
摘要： An azo dyestuff of the formula ##STR1## wherein R is linear alkyl having 2 to 4 carbon atoms and R' is linear alkyl having 3 to 5 carbon atoms and isopropyl.
摘要翻译：式IMA的偶氮染料，其中R是具有2至4个碳原子的直链烷基，R'是具有3至5个碳原子的直链烷基和异丙基。

9. 发明授权

US4319880A Monoazo dyestuff being stable under dyeing conditions; its manufacture and its use 失效
标题翻译：单色染料在染色条件下稳定; 其制造和使用
公开(公告)号：US4319880A
公开(公告)日：1982-03-16
申请号：US152552
申请日：1980-05-23
申请人： Konrad Opitz , Rudolf Schickfluss
发明人： Konrad Opitz , Rudolf Schickfluss
IPC分类号： C09B67/48 , C09B29/08 , C09B67/00
CPC分类号： C09B29/0813 , C09B67/0029
摘要： The invention relates to a novel crystallographic modification (".beta.-modification") being stable under dyeing conditions of the dyestuff of the formula ##STR1## which is characterized by an X-ray diffraction pattern as shown in FIG. 1 with characteristic reflexes at the following glance angles .theta. (CuK.sub..alpha. radiation) with the relative intensities:______________________________________ .phi. 3.71 6.62 7.85 8.6 9.43 10.51 11.8 12.57 relat. 67 44 34 36 60 60 46 100 intensity ______________________________________ to processes for their manufacture and to their use for dyeing fibrous materials of cellulose esters or of synthetic linear polyesters or blended fabrics of these polyesters and wool or rayon.
摘要翻译：本发明涉及一种新颖的结晶学修饰（“β-改性”）在染色条件下稳定的式“IMAGE”的染料，其特征在于如图1所示的X射线衍射图。 1具有以下瞥角θ（CuKα辐射）的特征反射，具有相对强度： - phi 3.71 6.62 7.85 8.6 9.43 10.51 11.8 12.57 -relat。 67 44 34 36 60 60 46 100 - 强度 - 其制造方法及其用于染色纤维素酯或这些聚酯和羊毛或人造丝的合成线性聚酯或混纺织物的纤维材料的用途。

10. 发明授权

US4007213A Process for preparing 1-(N-.beta.-cyanethylaminol-3-acylaminobenzenes 失效
标题翻译：制备1-（N- {62-氰乙基氨基-3-酰氨基苯
公开(公告)号：US4007213A
公开(公告)日：1977-02-08
申请号：US680706
申请日：1976-04-27
申请人： Rudolf Schickfluss
发明人： Rudolf Schickfluss
IPC分类号： C07C253/00 , B01J27/00 , B01J27/20 , B01J31/00 , B01J31/04 , C07B61/00 , C07C20060101 , C07C67/00 , C07C231/00 , C07C255/24 , C07C121/78
CPC分类号： C07C253/30
摘要： Process for the manufacture of 1-(N-.beta.-cyanethylamino)-3-acylaminobenzenes of the formula (1) ##STR1## in which R.sub.1 represents hydrogen, methyl or alkoxy of 1 to 4 carbon atoms, R.sub.2 represents hydrogen, alkyl from 1 to 3 carbon atoms or phenyl, R.sub.3 represents hydrogen or alkyl from 1 to 3 carbon atoms, and n represents the integer 0 or 1, which comprises reacting 1 mole of an amino of the formula (2) ##STR2## in which R.sub.1, R.sub.2 and R.sub.3 are defined as above, with 1 to 1.75 moles of acrylonitrile between 70.degree. and 150.degree. C in water with the addition of 1 to 30% by weight of an organic carboxylic acid or carbonic acid, and oxethylating the compound at the said formula (1) obtained, if n stands for the integer 0, without or after isolation, with 1 to 10 moles of ethylene oxide between 50.degree. and 100.degree. C.
摘要翻译：制备式（1）的1-（N-β-氰基乙基氨基）-3-酰氨基苯的方法其中R1代表氢，甲基或1-4个碳原子的烷氧基，R2代表氢， 1至3个碳原子的烷基或苯基，R 3表示氢或1至3个碳原子的烷基，n表示整数0或1，其包括使1摩尔式（2）的氨基），其中R 1，R 2和R 3如上定义，在水中加入1至30重量％的有机羧酸或碳酸，其中1至1.75摩尔丙烯腈在70至150℃之间，并加入氧乙基化所述式（1）中的化合物，如果n代表整数0，则在分离后没有或分离后，其中1至10摩尔环氧乙烷在50至100℃之间。

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