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1. 发明授权

US10034823B2 Method of coloring hair with washfast blue imidazolium direct dye compounds 有权
公开(公告)号：US10034823B2
公开(公告)日：2018-07-31
申请号：US15267585
申请日：2016-09-16
申请人： Noxell Corporation
发明人： Bryan Patrick Murphy , Guiru Zhang , Jielu Zhao
IPC分类号： A61Q5/10 , A61K8/49 , C09B29/036
CPC分类号： A61K8/4946 , A61K2800/4324 , A61Q5/10 , C09B1/285 , C09B29/0037 , C09B29/0051 , C09B29/083 , C09B29/3665 , C09B29/3686
摘要： Described herein is a method of dyeing the hair. The method includes applying to the hair a hair color composition including one or more direct dye compounds and rinsing the hair with water. The one or more direct dye compounds each include a blue-violet or blue chromophore, one or two permanent cations, one to four incipient cations, and one or more hydrophobic moieties. The incipient cations are pendant to the core structure and are neutral. The direct dye compounds enter the hair shaft after the hair color composition is applied to the hair. The hair color composition has a pH of from about 6 to about 11. The pH of the hair after rinsing is from about 3.5 to about 6. The rinsing of the hair causes one or more of the one to four incipient cations to change from neutral to positively charged inside of the hair shaft.

2. 发明授权

US4435320A Disperse azo dyes from 2-amino-3,5-bisfluorosulphonyl thiophene and aniline, tetrahydroquinoline, and benzomorpholine couplers 失效
标题翻译：从2-氨基-3,5-二氟磺酰基噻吩和苯胺，四氢喹啉和苯并吗啉偶联剂分散偶氮染料
公开(公告)号：US4435320A
公开(公告)日：1984-03-06
申请号：US346831
申请日：1982-02-08
申请人： Robert N. Gourley
发明人： Robert N. Gourley
IPC分类号： C09B29/00 , C09B29/08 , C09B29/36 , C09B29/44 , C09B29/033 , C09B29/09
CPC分类号： C09B29/0059 , C09B29/0807 , C09B29/3643 , C09B29/3686
摘要： Disclosed are new azo dyes from 2-amino-3,5-bisfluorosulphonyl thiophene which may be further substituted, and certain aniline, tetrahydroquinoline and benzomorpholine couplers. These dyes produce bright blue shades on hydrophobic fibres including polyesters, polyamides and cellulose esters, both by dyeing and heat transfer printing, and show improvements in one or more properties of dyeability, low energy of application, fastness to light, gas and wash, and heat stability, and have the general formula ##STR1## wherein R is hydrogen, alkyl or alkyl substituted with aryl or cycloalkyl; and C' represents an aniline, 1,2,3,4-tetrahydroquinoline, or benzomorpholine disperse dye coupling component.
摘要翻译：公开了可以进一步取代的2-氨基-3,5-二氟磺酰基噻吩的新偶氮染料，以及某些苯胺，四氢喹啉和苯并吗啉偶联剂。这些染料通过染色和热转移印刷在疏水性纤维上产生明亮的蓝色色调，包括聚酯，聚酰胺和纤维素酯，并且显示出一种或多种染色性能，低应用能力，耐光性，气体和洗涤性能的改进，以及热稳定性，通式为：其中R为氢，被芳基或环烷基取代的烷基或烷基; C'表示苯胺，1,2,3,4-四氢喹啉或苯并吗啉分散染料偶合组分。

3. 发明授权

US09567464B2 Disperse dyes, their preparation and their use 有权
标题翻译：分散染料，其制备及其用途
公开(公告)号：US09567464B2
公开(公告)日：2017-02-14
申请号：US15032869
申请日：2014-10-22
申请人： DyStar Colours Distribution GmbH
发明人： Yongnian Gao , Si Sl Liew , Samuel Shantong Fu , Roxana Barbieru
IPC分类号： C09B29/42 , C09B29/36 , C09B29/46 , C07D215/38 , C07D417/12 , C07D409/12 , C07D401/12
CPC分类号： C09B29/3617 , C07D215/38 , C07D401/12 , C07D409/12 , C07D417/12 , C09B29/0003 , C09B29/0025 , C09B29/3643 , C09B29/3652 , C09B29/3682 , C09B29/3686 , C09B29/3691
摘要： The present invention refers to dyes of the formula (I) and mixtures thereof a process for their production and to their use.
摘要翻译：本发明涉及式（I）的染料及其混合物，其制备方法及其用途。

4. 发明申请

US20160280922A1 DISPERSE DYES, THEIR PREPARATION AND THEIR USE 有权
标题翻译：分散染料及其制备及其使用
公开(公告)号：US20160280922A1
公开(公告)日：2016-09-29
申请号：US15032869
申请日：2014-10-22
申请人： DYSTAR COLOURS DISTRIBUTION GMBH
发明人： Yongnian GAO , Si SI LIEW , Samuel SHANTONG FU , Roxana BARBIERU
IPC分类号： C09B29/42 , C09B29/46 , C07D401/12 , C07D417/12 , C07D409/12 , C09B29/36 , C07D215/38
CPC分类号： C09B29/3617 , C07D215/38 , C07D401/12 , C07D409/12 , C07D417/12 , C09B29/0003 , C09B29/0025 , C09B29/3643 , C09B29/3652 , C09B29/3682 , C09B29/3686 , C09B29/3691
摘要： The present invention refers to dyes of the formula (1) and mixtures thereof a process for their production and to their use.
摘要翻译：一个生产和使用的过程。

5. 发明授权

US4593088A 2-amino-cinnamoylthiophene azo dyes having aniline, tetrahydroquinoline, or benzomorpholine couplers 失效
标题翻译：具有苯胺，四氢喹啉或苯并吗啉偶联剂的2-氨基 - 肉桂酰基噻吩偶氮染料
公开(公告)号：US4593088A
公开(公告)日：1986-06-03
申请号：US573185
申请日：1984-01-23
申请人： Robert N. Gourley
发明人： Robert N. Gourley
IPC分类号： C09B29/00 , C09B29/36 , C09B29/44 , C09B29/033 , C09B29/03 , C09B29/09 , D06P3/54
CPC分类号： C09B29/3643 , C09B29/0059 , C09B29/3686
摘要： Disclosed are new disperse azo dyes prepared from 2-amino-cinnamoylthiophene compounds. These dyes give bright blue shades, for example, on polyester, cellulose acetate and other synthetic fibers and exhibit improvements in one or more of such properties as bathochromic shift, fastness to light, sublimation, chlorine, heat, ozone, gas, perspiration, crock, and wash, build, pH stability, bloom resistance, depth of shade, leveling, strike rate, migration, and the like. The dyes have the general formula: ##STR1## wherein each R is a substituent selected for example from alkyl, substituted alkyl, hydroxy, alkoxy, halogen, nitro, alkoxycarbonyl, alkanoyloxy, alkanoyl, cyano, alkylamino, and dialkylamino, R.sup.14 is hydrogen or alkyl, C.sup.1 represents an aniline, tetrahydroquinoline or benzomorpholine coupling component which may be extensively substituted, and each of R.sup.12 and R.sup.13 is hydrogen or a substituent such as acyl, acylamido, alkyl, halogen, and cyano.
摘要翻译：公开了由2-氨基 - 肉桂酰噻吩化合物制备的新的分散偶氮染料。这些染料例如在聚酯，乙酸纤维素和其他合成纤维上产生明亮的蓝色色调，并且在一种或多种性能中显示出改善，例如红移，耐光牢度，升华，氯，热，臭氧，气体，出汗，，洗涤，构建，pH稳定性，耐开花性，遮荫深度，平整度，打击速度，迁移等。染料具有以下通式：其中每个R是选自例如烷基，取代的烷基，羟基，烷氧基，卤素，硝基，烷氧基羰基，烷酰氧基，烷酰基，氰基，烷基氨基和二烷基氨基的取代基，R 14是氢或烷基，C1表示可被广泛取代的苯胺，四氢喹啉或苯并吗啉偶联组分，R 12和R 13各自为氢或取代基如酰基，酰基酰氨基，烷基，卤素和氰基。

6. 发明授权

US4552951A Disperse and acid azo dyes having one or two cinnamoyl substituents on a phenyl diazonium moiety and containing an aniline, tetrahydroquinoline or benzomorpholine coupler 失效
标题翻译：在苯基重氮部分上具有一个或两个肉桂酰取代基的分散和酸性偶氮染料，并含有苯胺，四氢喹啉或苯并吗啉偶合剂
公开(公告)号：US4552951A
公开(公告)日：1985-11-12
申请号：US573243
申请日：1984-01-23
申请人： Robert N. Gourley
发明人： Robert N. Gourley
IPC分类号： C09B29/08 , C09B29/36 , C09B29/44 , C09B29/01 , C09B29/085
CPC分类号： C09B29/08 , C09B29/3643 , C09B29/3686
摘要： This invention relates to azo dyes which may be unsubstituted or substituted with a variety of groups known to the dye art, and containing a diazonium moieties from an aniline type compound and certain coupler moieties from aniline, tetrahydroquinoline, or benzomorpholine compounds, wherein the diazonium moiety has one or two cinnamoyl substituents, and wherein one or more water-solubilizing groups such as a sulfonic acid group or its metal or amine salt may be present as a substituent in the dye molecule for acid dyeing. These dyes are particularly useful in dyeing one or more of polyamide cellulose acetate polyester, wool and other fibers.
摘要翻译：本发明涉及偶氮染料，其可以是未被取代的或被染料领域已知的各种基团取代，并且含有来自苯胺型化合物的重氮部分和来自苯胺，四氢喹啉或苯并吗啉化合物的某些成色剂部分，其中重氮部分具有一个或两个肉桂酰取代基，并且其中一个或多个水溶性基团如磺酸基或其金属或胺盐可以作为用于酸性染色的染料分子中的取代基存在。这些染料特别可用于染色一种或多种聚酰胺纤维素醋酸酯聚酯，羊毛和其它纤维。

7. 发明授权

US4377518A Azo dyestuffs derived from polycyclo-hetercyclic coupler components 失效
标题翻译：衍生自多环异环成色剂的偶氮染料
公开(公告)号：US4377518A
公开(公告)日：1983-03-22
申请号：US183872
申请日：1980-09-03
申请人： Dieter vor der Bruck , Hans-Joachim Kabbe
发明人： Dieter vor der Bruck , Hans-Joachim Kabbe
IPC分类号： C07D491/04 , C07D491/14 , C07D493/04 , C09B29/01 , C09B29/36 , C09B62/085 , D21H21/28
CPC分类号： C07D491/04 , C07D491/14 , C07D493/04 , C09B29/0003 , C09B29/0022 , C09B29/3686 , C09B62/085 , D21H21/28
摘要： Dyestuffs of the formulaD--N.dbd.N--A Iin whichD represents the radical of a diazo component andA represents the radical of a coupling component of the formulae ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 designate hydrogen or non-ionic radicals,R designates hydrogen or an optionally substituted alkyl, cycloalkyl, aryl, aralkyl or heterocyclic radical,X designates OH or ##STR2## T designates the remaining members of a fused-on ring and Y and Z designate hydrogen, optionally substituted alkyl or optionally substituted aryl, processes for their preparation and process for pigmenting organic material using the dyestuffs of the formula I.
摘要翻译：式DN = NA I的染料，其中D表示重氮组分的基团，A表示式的耦合组分的基团，其中R 1，R 2和R 3表示氢或非离子性基团，R表示氢或任选取代的烷基，环烷基，芳基，芳烷基或杂环基，X表示OH或Y表示稠合环的其余成员，Y和Z表示氢，任选取代的烷基或任选地取代的芳基，其制备方法和使用式I的染料着色有机材料的方法。

8. 发明授权

US4264495A 2-Thienyl azo dyestuff compounds 失效
标题翻译： 2-噻吩基偶氮染料化合物
公开(公告)号：US4264495A
公开(公告)日：1981-04-28
申请号：US253633
申请日：1972-05-15
申请人： Ronald J. Maher , John G. Fisher , Max A. Weaver
发明人： Ronald J. Maher , John G. Fisher , Max A. Weaver
IPC分类号： C09B29/033 , C09B29/00 , C09B29/06 , C09B29/36 , C09B29/44 , C09B31/02 , C07C107/04
CPC分类号： C09B31/02 , C09B29/0059 , C09B29/06 , C09B29/3643 , C09B29/3686
摘要： Azo compounds having the formula ##STR1## in which R.sup.1 is cyano, aryl, an acyl radical or a carbamoyl radical, R.sup.2 is hydrogen, alkyl, alkoxy, aralkyl or aryl, R.sup.3 is alkyl, halogen, thiocyanato, arylazo or one of the substituents which R.sup.1 can represent, and A is an aniline, tetrahydroquinoline, benzomorpholine or .alpha.-naphthylamine disperse azo dye coupling component. The azo compounds produce red to blue shades on polyamide, polyester and cellulose acetate fibers and exhibit improved fastness and dyeability properties on synthetic polyamide fibers.
摘要翻译：具有式“IMAGE”的偶氮化合物，其中R 1是氰基，芳基，酰基或氨基甲酰基，R 2是氢，烷基，烷氧基，芳烷基或芳基，R 3是烷基，卤素，氰硫基，芳基偶氮或其中一个取代基其中R1可以表示，A是苯胺，四氢喹啉，苯并吗啉或α-萘胺分散偶氮染料偶合组分。偶氮化合物在聚酰胺，聚酯和醋酸纤维素纤维上产生红色至蓝色，并在合成聚酰胺纤维上表现出改善的牢度和染色性能。

9. 发明授权

US4255326A Nitrogen and/or sulfur containing heterocyclic azo dyes with aniline, tetrahydroquinoline and benzomorpholine couplers having sulfate group 失效
标题翻译：含氮和/或含硫杂环偶氮染料与苯胺，四氢喹啉和具有硫酸根基团的苯并吗啉成色剂
公开(公告)号：US4255326A
公开(公告)日：1981-03-10
申请号：US25685
申请日：1979-03-30
申请人： Ralph R. Giles , Max A. Weaver
发明人： Ralph R. Giles , Max A. Weaver
IPC分类号： C09B29/033 , C09B29/08 , C09B29/36 , C09B29/44 , C09B29/26 , D06P3/24
CPC分类号： C09B29/3643 , C09B29/0025 , C09B29/0803 , C09B29/3686
摘要： Disclosed are azo dyes prepared by diazotizing heterocyclic amines such as 2-aminobenzothiazole, 3-amino-2,1-benzisothiazole, 5-amino-1,2,4-thiadiazole, 5-aminoisothiazole, 5-aminopyrazole, 2-aminothiophene and 2-amino-1,3,4-thiadiazole, followed by coupling with certain aniline, tetrahydroquinoline, or benzomorpholine compounds containing sulfate groups. These amines may be substituted with a large variety of groups including lower alkyl, lower alkoxy, cyano, carbamoyl, sulfamoyl, and halogen. These dyes have excellent dyeing properties on polyamide fibers and also impart color to cellulose acetate fibers and wool.
摘要翻译：公开了通过重氮化杂环胺如2-氨基苯并噻唑，3-氨基-2,1-苯并异噻唑，5-氨基-1,2,4-噻二唑，5-氨基异噻唑，5-氨基吡唑，2-氨基噻吩和2 - 氨基-1,3,4-噻二唑，然后与含硫酸根的某些苯胺，四氢喹啉或苯并吗啉化合物偶联。这些胺可以被大量各种基团取代，包括低级烷基，低级烷氧基，氰基，氨基甲酰基，氨磺酰基和卤素。这些染料在聚酰胺纤维上具有优异的染色性能，并赋予醋酸纤维素纤维和羊毛颜色。

10. 发明授权

US4409143A Monoazo dyes containing phosphamic acid diester groups 失效
标题翻译：含有氨基酸二酯基团的单偶氮染料
公开(公告)号：US4409143A
公开(公告)日：1983-10-11
申请号：US258245
申请日：1981-04-28
申请人： John Lenoir , Gerald Jan
发明人： John Lenoir , Gerald Jan
IPC分类号： G03C7/02 , C09B29/08 , C09B29/085 , C09B29/36 , C09B29/44 , C09B31/043 , G03C7/28 , G03C7/29 , C09B29/09 , C09B29/26 , G03C1/10
CPC分类号： C09B29/0836 , C09B29/3643 , C09B29/3686 , C09B31/043 , G03C7/29 , Y10S534/02
摘要： Azo dyes of the formula in which X.sub.1 and X.sub.2 independently of one another are alkyl, cycloalkyl, alkenyl, aryl or aralkyl, Y.sub.1 is hydrogen or alkyl, Y.sub.2 is hydrogen, alkyl, alkenyl or aryl or together with Y.sub.1 stands for the atoms required to complete a ring, Z.sub.1 is hydrogen, alkyl, alkenyl, alkoxy, aryl, aryloxy, alkylmercapto, arylmercapto, halogen, cyano, carbalkoxy or stands for the atoms which together with Y.sub.1 form a ring, and D.sub.1 is the radical of a heterocyclic azo component such as a thienyl, thiazolyl, benzthiazolyl, pyrazolyl or imidazolyl radical, or is phenyl optionally substituted by alkyl, cycloalkyl, alkoxy, alkenyl, electronegative substituents such as halogen, cyano, nitro or carboxylic acid, alkyl- or phenylsulfone or N-alkyl or N,N-dialkyl-substituted sulfonamido, can be used as image dyes in photographic silver dye-bleach materials, or for dyeing textile materials.
摘要翻译：其中X1和X2彼此独立地是烷基，环烷基，烯基，芳基或芳烷基，Y1是氢或烷基，Y2是氢，烷基，烯基或芳基或与Y1一起代表所需的原子完成一个环，Z1是氢，烷基，烯基，烷氧基，芳基，芳氧基，烷基巯基，芳基巯基，卤素，氰基，烷氧基或代表与Y1一起形成环的原子，D1是杂环偶氮组分例如噻吩基，噻唑基，苯并噻唑基，吡唑基或咪唑基，或者是任选被烷基，环烷基，烷氧基，烯基，电负性取代基如卤素，氰基，硝基或羧酸取代的苯基，烷基或苯基砜或N-烷基或 N，N-二烷基取代的亚磺酰氨基可用作照相银染料漂白材料中的图像染料，或染色纺织材料。

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