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1. 发明授权

US4724256A Urethane linked hydroxy aromatic isocyanates 失效
标题翻译：氨基甲酸酯连接羟基芳族异氰酸酯
公开(公告)号：US4724256A
公开(公告)日：1988-02-09
申请号：US2840
申请日：1987-01-13
申请人： William E. Starner , Barton Milligan , Roland E. Grandin
发明人： William E. Starner , Barton Milligan , Roland E. Grandin
IPC分类号： C07C67/00 , C07C239/00 , C07C271/28 , C08G18/32 , C08G18/48 , C08G18/76 , C08G18/30
CPC分类号： C08G18/4825 , C08G18/3206 , C08G18/7614
摘要： This invention relates to urethane linked hydroxy aromatic isocyanates and to a process for producing such urethane linked hydroxy aromatic isocyanates. The compositions are formed by reacting one equivalent aromatic diisocyanate with one equivalent of an alkylene polyol under conditions such that only one of the isocyanate groups react with the hydroxyl group of the polyol. Conditions are controlled such that the urethane linked hydroxy aromatic isocyanates are formed. The resulting product is suited for producing a variety of elastomers including a one component polyurethane elastomer.

2. 发明授权

US4683279A Low melting urethane linked toluenediisocyanates 失效
标题翻译：低熔点氨基甲酸酯连接甲苯二异氰酸酯
公开(公告)号：US4683279A
公开(公告)日：1987-07-28
申请号：US882994
申请日：1986-07-08
申请人： Barton Milligan , William E. Starner , Roland E. Grandin , Jeremiah P. Casey
发明人： Barton Milligan , William E. Starner , Roland E. Grandin , Jeremiah P. Casey
IPC分类号： C08G18/76 , C07C67/00 , C07C239/00 , C07C271/28 , C08G18/80 , C08G18/81
CPC分类号： C08G18/8019 , C08G18/815 , C08G2120/00
摘要： This invention relates to urethane linked mixtures of 2,4- and 2,6-toluenediisocyanates (ULTDI dimers) having low melting points and to a method of forming these systems. The urethane linked toluenediisocyanates containing from 45-90% of the 2,4- and 10-55% of the 2,6- isomer by weight are formed by reacting two moles of an appropriate isomer mix of toluenediisocyanate, with one mole of a specific alkylene glycol, e.g., 1,2-butanediol, diethylene glycol or dipropylene glycol under conditions such that essentially only one of the isocyanate groups on a toluenediisocyanate molecule reacts with a hydroxyl group of the glycol. Conditions are controlled such that the urethane linked toluenediisocyanates are formed. The resulting product, which has two unreacted isocyanate groups, is suited for producing a variety of elastomers including polyurethane polyurethane/urea or polyurea elastomers.
摘要翻译：本发明涉及具有低熔点的2,4-和2,6-甲苯二异氰酸酯（ULTDI二聚体）与形成这些体系的方法的氨基甲酸酯连接的混合物。含有45-90％的2,4-和10-55％的2,6-异构体的氨基甲酸酯连接的甲苯二异氰酸酯是通过使两摩尔的甲苯二异氰酸酯的合适异构体混合物与1摩尔特定的亚烷基二醇，例如1,2-丁二醇，二甘醇或二丙二醇，在甲苯二异氰酸酯分子上基本上只有一个异氰酸酯基与二醇的羟基反应的条件下进行。控制条件使得形成氨基甲酸酯连接的甲苯二异氰酸酯。得到的具有两个未反应的异氰酸酯基的产物适用于生产各种弹性体，包括聚氨酯聚氨酯/脲或聚脲弹性体。

3. 发明授权

US4722989A Process for producing polyurethane/urea elastomers 失效
标题翻译：生产聚氨酯/尿素弹性体的方法
公开(公告)号：US4722989A
公开(公告)日：1988-02-02
申请号：US025911
申请日：1987-03-16
申请人： William E. Starner , Barton Milligan , Jeremiah P. Casey
发明人： William E. Starner , Barton Milligan , Jeremiah P. Casey
IPC分类号： C08G18/10 , C08G18/32 , C08G18/48 , C08G18/80 , C08G18/81 , C08G81/00
CPC分类号： C08G18/8019 , C08G18/815 , C08G2120/00
摘要： This invention relates to a solvent-free process for producing polyurethane/urea elastomers wherein an aromatic diisocyanate is reacted with a compound having active Zerewitinoff hydrogen atoms and an aromatic diamine chain extender. The improvement for producing urethanes having a wide range of properties comprises including a urethane-linked diisocyanate in the polyurethane urea elastomer. The urethane-linked diisocyanate is one that is formed by reacting toluenediisocyanate or substituent thereof with a short chain diol under conditions such that the urethane linked diisocyanate comprises two equivalents isocyanate per equivalent diol.

4. 发明授权

US4786703A Process for the preparation of polyisocyanate prepolymers and polyurethanes having high temperature performance and low hysteresis 失效
标题翻译：具有高温性能和低滞后性的多异氰酸酯预聚物和聚氨酯的制备方法
公开(公告)号：US4786703A
公开(公告)日：1988-11-22
申请号：US38810
申请日：1987-04-15
申请人： William E. Starner , Jeremiah P. Casey , Barton Milligan , Susan M. Clift
发明人： William E. Starner , Jeremiah P. Casey , Barton Milligan , Susan M. Clift
IPC分类号： C08G18/10 , C08G18/65 , C08G18/76 , C08G18/30
CPC分类号： C08G18/7621 , C08G18/10
摘要： This invention relates to a polyisocyanate prepolymer for polyurethane/urea elastomer synthesis and to the resulting elastomer. The prepolymer is formed by reacting toluenediisocyanate with a long chain polyol under conditions such that essentially a 2:1 adduct is formed. Excess toluenediisocyanate is removed prior to forming the elastomer.

5. 发明授权

US4332736A Production of 1-hydroxyalkylidene-1, 1-diphosphonic acid esters 失效
标题翻译： 1-羟基亚烷基-1,1-二膦酸酯的制备
公开(公告)号：US4332736A
公开(公告)日：1982-06-01
申请号：US190009
申请日：1980-09-22
申请人： William E. Starner , Walter F. Yext
发明人： William E. Starner , Walter F. Yext
IPC分类号： C07F9/38 , C07F9/40
CPC分类号： C07F9/4093 , C07F9/386
摘要： Acylated 1-hydroxyalkylidene-1, 1-diphosphonic acid (HADPA) can be produced almost instantaneously with less than 5% (by weight) phosphorus acid byproduct by introducing PX.sub.3 (where X is a halide) into a reactor containing R--COOH at or above a specified temperature. The acylated HADPA can then be hydrolyzed and substantially pure HADPA obtained by vacuum distillation. Of particular importance is the addition of PCl.sub.3 to acetic acid at a temperature of between 105.degree. C. and 120.degree. C. to produce acetylated 1-hydroxyethylidene-1, 1-diphosphonic acid (HEDPA).
摘要翻译：通过将PX3（其中X是卤化物）引入到含有R-COOH的反应器中，可以通过将小于5％（重量）的磷酸副产物几乎瞬间生产酰化的1-羟基亚烷基-1,1-二膦酸（HADPA）高于指定温度。然后可以将酰化的HADPA水解并通过真空蒸馏获得基本上纯的HADPA。特别重要的是在105℃至120℃的温度下将PCl3加入到乙酸中以产生乙酰化的1-羟基亚乙基-1,1-二膦酸（HEDPA）。

6. 发明授权

US5426157A Flexibilized polyepoxide resins incorporating poly-N-methylated secondary amines 失效
标题翻译：结合聚-N-甲基化仲胺的柔性聚环氧化物树脂
公开(公告)号：US5426157A
公开(公告)日：1995-06-20
申请号：US213647
申请日：1994-03-16
申请人： William E. Starner , John A. Marsella , Richard S. Myers
发明人： William E. Starner , John A. Marsella , Richard S. Myers
IPC分类号： C08G18/58 , C08G18/67 , C08G59/06 , C08G59/40 , C08G59/50 , C08L63/00 , C08G18/04
CPC分类号： C08G59/5006 , C08G18/672 , C08L63/00 , Y10S525/92
摘要： This invention relates to improved polyepoxide resins having enhanced physical and elastic properties. The polyepoxide resins comprise a polyepoxide resin based on a polyglycidyl ether of a phenolic-type compound and an acrylate-terminated urethane prepolymer. The improvement in the polyepoxide resin formulation comprises incorporating a polymethylated amine curative having two secondary amine hydrogens represented by the formula: ##STR1## wherein R is alkylene or polyalkylene polyamine having from 2 to 20 carbon atoms. The presence of the aliphatic amine reactive component along with the acrylate-terminated urethane prepolymer results in an epoxy resin having enhanced properties.
摘要翻译：本发明涉及具有增强的物理和弹性特性的改进的聚环氧化物树脂。聚环氧化物树脂包括基于酚类化合物的多缩水甘油醚和丙烯酸酯封端的氨基甲酸酯预聚物的聚环氧树脂。聚环氧化物树脂制剂的改进包括加入具有由下式表示的两个仲胺氢的聚甲基化胺固化剂：其中R是亚烷基或具有2至20个碳原子的聚亚烷基多胺。脂族胺反应性成分与丙烯酸酯封端的氨基甲酸酯预聚物的存在导致具有增强性能的环氧树脂。

7. 发明授权

US5202001A Preparation of urethane prepolymers having low levels of residual toluene diisocyanate 失效
标题翻译：制备具有低残留甲苯二异氰酸酯含量的氨基甲酸酯预聚物
公开(公告)号：US5202001A
公开(公告)日：1993-04-13
申请号：US727501
申请日：1991-07-09
申请人： William E. Starner , Bernard A. Toseland , Reinaldo M. Machado
发明人： William E. Starner , Bernard A. Toseland , Reinaldo M. Machado
IPC分类号： C07C269/08 , C08G18/10 , C08G18/76
CPC分类号： C07C269/08 , C08G18/10 , C08G18/7621 , Y10S159/10
摘要： A wiped film evaporation process for reducing the amount of residual organic polyisocyanate, especially toluene diisocyanate, in a polyurethane prepolymer reaction product mixture. An inert sweeping gas is added to the evaporation process, preferably after first passing through a holdup volume of the prepolymer which has passed through the evaporation zone.
摘要翻译：用于在聚氨酯预聚物反应产物混合物中减少残余有机多异氰酸酯，特别是甲苯二异氰酸酯的量的擦膜蒸发方法。优选在首先通过已经通过蒸发区的预聚物的滞留体积之后，向蒸发过程中加入惰性清扫气体。

8. 发明授权

US5334654A Flexibilized polyepoxide resins 失效
标题翻译：柔性聚环氧树脂
公开(公告)号：US5334654A
公开(公告)日：1994-08-02
申请号：US56728
申请日：1993-05-03
申请人： William E. Starner , Susan G. Musselman
发明人： William E. Starner , Susan G. Musselman
IPC分类号： C08G59/18 , C08G59/40 , C08G59/50 , C08L63/00
CPC分类号： C08L63/00
摘要： This invention relates to improved polyepoxide resins having enhanced physical and elastic properties. The polyepoxide resins comprise an polyepoxide resin based on a polyglycidyl ether of a phenolic type compound and an acrylate terminated urethane prepolymer. The improvement in the polyepoxide resin formulation comprises incorporating an aliphatic, aliphatic ether or ester component having monofunctional reactivity with an amine hydrogen and an amine curative having from 3 to 10, and preferably 3 to 5 epoxide reactive hydrogen atoms into the epoxy resin. The presence of the monofunctional and aliphatic amine reactive component along with the acrylate terminated urethane prepolymer results in an epoxy resin having the enhanced properties.
摘要翻译：本发明涉及具有增强的物理和弹性特性的改进的聚环氧化物树脂。聚环氧化物树脂包括基于酚类化合物的聚缩水甘油醚和丙烯酸酯封端的氨基甲酸酯预聚物的聚环氧树脂。聚环氧树脂制剂的改进包括将具有单胺官能反应性的脂族，脂族醚或酯组分与胺氢和具有3至10个，优选3至5个环氧化物反应性氢原子的胺固化剂掺入环氧树脂中。单官能和脂族胺反应性组分与丙烯酸酯封端的氨基甲酸酯预聚物的存在导致具有增强性能的环氧树脂。

9. 发明授权

US5041670A Preparation of n-aryl amines from isocyanates 失效
标题翻译：从异氰酸酯制备正 - 芳基胺
公开(公告)号：US5041670A
公开(公告)日：1991-08-20
申请号：US174663
申请日：1988-03-29
申请人： Franklin A. Davis , William E. Starner
发明人： Franklin A. Davis , William E. Starner
IPC分类号： C07C209/62
CPC分类号： C07C209/62
摘要： Methods of producing N-phenyl amines comprise reacting a phenyl-containing isocyanate with HR, and a boron complexing agent in an aprotic solvent, wherein R, is --OH or --COOH (i.e., water or formic acid), neutralizing the resulting N-aryl amide to N-aryl amine and recovering the N-aryl amine.
摘要翻译：生产N-苯基胺的方法包括使含苯基的异氰酸酯与HR反应，和硼络合剂在非质子传递溶剂中反应，其中R 1为-OH或-COOH（即水或甲酸），中和得到的N- 芳基酰胺转化成N-芳基胺并回收N-芳基胺。

10. 发明授权

US5618905A Partially methylated polyamines as epoxy curing agents 失效
标题翻译：部分甲基化多胺作为环氧固化剂
公开(公告)号：US5618905A
公开(公告)日：1997-04-08
申请号：US584937
申请日：1996-01-16
申请人： John A. Marsella , William E. Starner , Richard S. Myers
发明人： John A. Marsella , William E. Starner , Richard S. Myers
IPC分类号： C08G59/40 , C08G59/50 , C08L63/00 , C08G59/44
CPC分类号： C08G59/5006 , C08G59/50
摘要： A curable epoxy resin composition comprising a polyepoxide resin and an amine curative characterized in that the amine curative comprises a partially methylated polyalkylene polyamine having at least three amine nitrogens and at least two active amine hydrogens.
摘要翻译：一种可固化环氧树脂组合物，其包含聚环氧树脂和胺固化剂，其特征在于所述胺固化剂包含具有至少三个胺氮和至少两个活性胺氢的部分甲基化聚亚烷基多胺。

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