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1. 发明授权

US07696285B2 Carbamate functional reactive polymer composition 有权
标题翻译：氨基甲酸酯官能反应性聚合物组合物
公开(公告)号：US07696285B2
公开(公告)日：2010-04-13
申请号：US10866595
申请日：2004-06-11
申请人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
发明人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
IPC分类号： C08G18/00 , C08C19/22
CPC分类号： C09D201/025 , C08F8/00 , C08F2800/20 , C09D201/02 , C08F220/20
摘要： Disclosed is a carbamate functional reactive polymer composition, comprising an acrylic resin (a′) comprising a functional group (F3) that is at least one of a primary carbamate group, a primary hydroxyl group, a secondary hydroxyl group, and mixtures thereof, and a nonvolatile solvent (b′nv) that is not a crystalline solid at 75° C. but is a fluid solid at a temperature of free radical polymerization and comprises (i) four or more isomers, and (ii) at least two reactive functional groups (F2) that are selected from primary carbamate, primary hydroxyl, and secondary hydroxyl, wherein no more than 10% of the sum of functional groups (F2) and (F3) are primary hydroxyl groups and at least 60% of the sum of functional groups (F2) and (F3) are primary carbamate groups. In one exemplary embodiment, the reactive polymer composition is made by a disclosed method.
摘要翻译：公开了一种氨基甲酸酯官能反应性聚合物组合物，其包含丙烯酸树脂（a'），其包含主要氨基甲酸酯基，伯羟基，仲羟基及其混合物中的至少一种的官能团（F3），以及在75℃下不是结晶固体的非挥发性溶剂（b'nv），但是在自由基聚合温度下是流体固体，并且包含（i）四种或更多种异构体，和（ii）至少两种反应性官能团选自伯氨基甲酸酯，伯羟基和仲羟基的基团（F2），其中不超过10％的官能团（F2）和（F3）的和为伯羟基，并且至少60％官能团（F2）和（F3）是伯氨基甲酸酯基团。在一个示例性实施方案中，通过公开的方法制备反应性聚合物组合物。

2. 发明授权

US07321013B2 Method for obtaining coating compositions having reduced VOC 有权
标题翻译：获得具有降低的VOC的涂料组合物的方法
公开(公告)号：US07321013B2
公开(公告)日：2008-01-22
申请号：US10866596
申请日：2004-06-11
申请人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
发明人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
IPC分类号： C08L67/00 , C08G18/00
CPC分类号： C09D201/02 , C08F8/00 , C08F2800/20 , C08G18/4072 , C08G18/4233 , C08G18/6229 , C08G18/6254 , C08G18/672 , C08G18/8175 , C08G2190/00 , C09D5/02 , C09D133/14 , C09D167/00 , C09D175/04 , C09D201/00 , C09D201/025 , C08F220/20
摘要： Disclosed is a method of making reduced VOC polymers and coating compositions containing such polymers. Provided is a mixture (I) comprising a reactant mixture (a) of polymerizable components and a nonvolatile solvent (bnv) that (i) is not a crystalline solid at 25° C., (ii) is nonvolatile, (iii) comprises at least one functional group (F1) and (iv) is a fluid solid. Reactant mixture (a) is polymerized to provide a polymer (a′). The at least one functional group (F1) of nonvolatile solvent (bnv) is reacted with one or more reactants (e) to obtain a nonvolatile solvent (b′nv) comprising at least two functional groups (F2). Obtained is a mixture (II) comprising polymer (a′) in nonvolatile solvent (b′nv) comprising at least two functional groups (F2). The at least one functional group (F1) is substantially nonreactive: (1) with the components of reactive mixture (a), (2) under the polymerization conditions which polymerize reactant mixture (a), and (3) with polymer (a′).
摘要翻译：公开了一种制备含有这种聚合物的VOC聚合物和涂料组合物的方法。提供了包含可聚合组分的反应物混合物（a）和不挥发性溶剂（b）的混合物（I），（i）在25℃下不是结晶固体，（ii）是非挥发性的，（iii）包含至少一个官能团（F 1 H 1）和（iv）是流体固体。将反应物混合物（a）聚合以提供聚合物（a'）。非挥发性溶剂（b）的至少一个官能团（F 1 N 1）与一种或多种反应物（e）反应，得到非挥发性溶剂（b' 包括至少两个官能团（F 2 N 2）。获得的包含聚合物（a'）在包含至少两个官能团（F 2 N 2）的非挥发性溶剂（b'Nv））中的混合物（II）。至少一个官能团（F 1 H 1）基本上是非反应性的：（1）在聚合反应混合物（a）的聚合条件下与反应混合物（a），（2）的组分反应，和（3）与聚合物（a'）。

3. 发明授权

US07368501B2 Method for improving environmental durability of materials 失效
标题翻译：提高材料耐候性的方法
公开(公告)号：US07368501B2
公开(公告)日：2008-05-06
申请号：US10866607
申请日：2004-06-11
申请人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
发明人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
IPC分类号： C08G18/08 , C08K5/13 , C08F18/00
CPC分类号： C08F4/28 , C08F2/06 , C08F2/52 , C08F2/56 , C08F4/04 , C09D175/04 , C09D201/02 , C09D201/025 , C08L2666/16
摘要： Disclosed is a method of making an environmentally durable material, the method requiring providing a material comprising at least one functional group Fc, and subjecting the material to a free radical source such that substantially all functional groups Fc are eliminated but the material is not polymerized. In one embodiment, the functional group Fc is at least one of a nonaromatic carbon-carbon double bond, a hydrogen atom alpha to an aromatic ring, a hydrogen atom alpha to a carbon-carbon double bond, or a hydrogen atom attached to a tertiary substituted carbon. In another embodiment, functional group Fc is present in the material as a contaminant. In one exemplary embodiment, the material comprises from 0.05 to less than 15% by weight of functional group Fc, based on the total weight of the material.
摘要翻译：公开了一种制备环境耐久材料的方法，该方法需要提供包含至少一个官能团F 1的材料，并使材料经受自由基源，使得基本上所有官能团F < SUB> c 被消除，但材料未聚合。在一个实施方案中，官能团F C是至少一种非芳族碳 - 碳双键，芳环的α，氢原子，碳 - 碳双键的氢原子，或与叔取代的碳连接的氢原子。在另一个实施方案中，作为污染物的材料中存在官能团F C c。在一个示例性实施方案中，基于材料的总重量，该材料包含0.05至小于15重量％的官能团F C c C。

4. 发明授权

US07691951B2 Method for obtaining coating compositions having reduced VOC 有权
标题翻译：获得具有降低的VOC的涂料组合物的方法
公开(公告)号：US07691951B2
公开(公告)日：2010-04-06
申请号：US11868104
申请日：2007-10-05
申请人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
发明人： Walter H. Ohrbom , Marvin L. Green , Gregory G. Menovcik
IPC分类号： C08L67/00 , C08G18/00
CPC分类号： C09D201/02 , C08F8/00 , C08F2800/20 , C08G18/4072 , C08G18/4233 , C08G18/6229 , C08G18/6254 , C08G18/672 , C08G18/8175 , C08G2190/00 , C09D5/02 , C09D133/14 , C09D167/00 , C09D175/04 , C09D201/00 , C09D201/025 , C08F220/20
摘要： Disclosed is a method of making reduced VOC polymers and coating compositions containing such polymers. Provided is a mixture (I) comprising a reactant mixture (a) of polymerizable components and a nonvolatile solvent (bnv) that (i) is not a crystalline solid at 25° C., (ii) is nonvolatile, (iii) comprises at least one functional group (F1) and (iv) is a fluid solid. Reactant mixture (a) is polymerized to provide a polymer (a′). The at least one functional group (F1) of nonvolatile solvent (bnv) is reacted with one or more reactants (e) to obtain a nonvolatile solvent (b′nv) comprising at least two functional groups (F2). Obtained is a mixture (II) comprising polymer (a′) in nonvolatile solvent (b′nv) comprising at least two functional groups (F2). The at least one functional group (F1) is substantially nonreactive: (1) with the components of reactive mixture (a), (2) under the polymerization conditions which polymerize reactant mixture (a), and (3) with polymer (a′).
摘要翻译：公开了一种制备含有这种聚合物的VOC聚合物和涂料组合物的方法。提供了包含可聚合组分的反应物混合物（a）和不挥发性溶剂（bnv）的混合物（I），其中（i）在25℃下不是结晶固体，（ii）是非挥发性的，（iii）包含至少一个官能团（F1）和（iv）是流体固体。将反应物混合物（a）聚合以提供聚合物（a'）。将不挥发性溶剂（bnv）的至少一种官能团（F1）与一种或多种反应物（e）反应，得到包含至少两个官能团（F2）的非挥发性溶剂（b'nv）。获得的是包含至少两个官能团（F2）的非挥发性溶剂（b'nv）中的聚合物（a'）的混合物（II）。至少一个官能团（F1）基本上是非反应性的：（1）在反应混合物（a）和（3）与聚合物（a'）聚合的聚合条件下，反应混合物（a），（2））。

5. 发明授权

US06962730B2 Coating composition containing crosslinkable monomeric difunctional compounds having at least thirty carbon atoms 有权
标题翻译：包含具有至少30个碳原子的可交联单体双官能化合物的涂料组合物
公开(公告)号：US06962730B2
公开(公告)日：2005-11-08
申请号：US10351079
申请日：2003-01-23
申请人： Walter H. Ohrbom , John A. Gilbert , Patricia A. Herrel , Marvin L. Green , Joanne Casale , Thomas G. Savino
发明人： Walter H. Ohrbom , John A. Gilbert , Patricia A. Herrel , Marvin L. Green , Joanne Casale , Thomas G. Savino
IPC分类号： C09D5/02 , C09D133/14 , C09D201/00 , C09D201/02 , B05D3/00
CPC分类号： C09D5/02 , C09D133/14 , C09D201/00 , C09D201/02 , C09D201/025
摘要： The invention provides coating compositions comprising a reactive component (a) which is substantially free of any heteratoms and is a not a crystalline solid at room temperature and which comprises from (i) 12 to 72 carbon atoms, and (ii) at least two functional groups, and (b) a crosslinking agent comprising a plurality of functional groups (iii) reactive with the functional groups (ii) of compound (a), wherein functional groups (ii) and (iii) are selected such that reaction there between produces a thermally irreversible chemical linkage. The coating compositions of the invention provide improved solids, chip resistance, flexibility and/or scratch & mar resistance while maintaining desirable and/or improved performance characteristics with regard to environmental etch, relative humidity, QCT, chip resistance, thermoshock resistance, cold crack resistance, adhesion and the like.
摘要翻译：本发明提供涂料组合物，其包含基本上不含任何杂原子的反应性组分（a），并且在室温下不是结晶固体，并且其包含（i）12至72个碳原子，和（ii）至少两个官能基团，和（b）包含与化合物（a）的官能团（ⅱ）反应的多个官能团（ⅲ）的交联剂，其中选择官能团（ⅱ）和（ⅲ），使得其中的反应产生热不可逆化学键。本发明的涂料组合物在环境蚀刻，相对湿度，QCT，芯片电阻，耐热裂纹性，耐寒裂纹性方面保持理想和/或改进的性能特征，提供了改进的固体，耐芯片性，柔性和/ ，粘合等。

6. 发明授权

US06531560B1 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
公开(公告)号：US06531560B1
公开(公告)日：2003-03-11
申请号：US09677063
申请日：2000-09-29
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C08F12602
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.

7. 发明授权

US5994479A Curable coating compositions containing blends of carbamate-functional compounds 失效
标题翻译：含有氨基甲酸酯官能化合物的混合物的可固化涂料组合物
公开(公告)号：US5994479A
公开(公告)日：1999-11-30
申请号：US997317
申请日：1997-12-23
申请人： Marvin L. Green , John D. McGee , Brian D. Bammel , Danielle A. Regulski , Walter H. Ohrbom
发明人： Marvin L. Green , John D. McGee , Brian D. Bammel , Danielle A. Regulski , Walter H. Ohrbom
IPC分类号： C08G18/40 , C08G18/80 , C09D5/02 , C09D5/03 , C09D161/20 , C09D175/00 , C09D201/02 , C08G8/28 , C08G59/14 , C08L63/00 , C08L67/04
CPC分类号： C09D161/20 , C08G18/8077 , C09D201/025 , Y10T428/31551
摘要： The present invention provides a curable coating composition comprising(a) a first component comprising at least two functional groups, at least one of which is a carbamate or urea group that is the reaction product of:(1) a hydroxyl group that is the result of a ring-opening reaction between an epoxy group and an organic acid group, and(2) cyanic acid or a carbamate or urea group;(b) a curing agent having a plurality of functional groups that are reactive with component (a), and(c) a second component having functional groups that are reactive with component (a) or component (b) or both components (a) and (b).
摘要翻译：本发明提供一种可固化涂料组合物，其包含（a）包含至少两个官能团的第一组分，其中至少一个为氨基甲酸酯或脲基，其为：（1）作为结果的羟基的反应产物的环氧基和有机酸基之间的开环反应，和（2）氰酸或氨基甲酸酯或脲基; （b）具有多个与组分（a）反应的官能团的固化剂，和（c）具有与组分（a）或组分（b）或两种组分（a）反应的官能团的第二组分）和（b）。

8. 发明授权

US08686090B2 Use of urea crystals for non-polymeric coatings 有权
标题翻译：尿素晶体用于非聚合物涂层
公开(公告)号：US08686090B2
公开(公告)日：2014-04-01
申请号：US10732850
申请日：2003-12-10
申请人： Marvin L. Green , Swaminathan Ramesh , Walter H. Ohrbom
发明人： Marvin L. Green , Swaminathan Ramesh , Walter H. Ohrbom
IPC分类号： B01F17/00 , B05D3/02 , C08F283/00 , C08F283/02 , C08F283/04 , C08G6/02 , C08G8/28 , C08G12/42 , C08G18/00 , C08G18/08 , C08G18/28 , C08G18/42 , C08G18/67 , C08G18/83 , C08G63/08 , C08G63/44 , C08G63/91 , C08G65/32 , C08G67/02 , C08G69/00 , C08G69/44 , C08K5/00 , C08L51/00 , C08L61/00 , C08L61/02 , C08L63/00 , C08L67/00 , C08L67/02 , C08L69/00 , C08L71/00 , C08L75/00 , C08L77/00 , C08L79/00
CPC分类号： C09D175/02 , C08G18/2865 , C08G18/4615 , C09D201/025
摘要： The thermosetting, non-polymeric coating composition includes at least one monomeric material having a plurality of carbamate and/or urea groups, at least one crosslinker reactive with the at least one monomeric material, and a sag control agent that is a crystalline reaction product of an amine and an isocyanate.
摘要翻译：热固性非聚合物涂料组合物包括至少一种具有多个氨基甲酸酯和/或脲基团的单体材料，至少一种与至少一种单体材料反应的交联剂，以及一种下垂控制剂，其为下列物质的结晶反应产物：胺和异氰酸酯。

9. 发明授权

US06696535B2 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
标题翻译：具有改进粘合性的氨基甲酸酯官能树脂，其制备方法以及改进层间粘附性的方法
公开(公告)号：US06696535B2
公开(公告)日：2004-02-24
申请号：US10348492
申请日：2003-01-21
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C08F12602
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.
摘要翻译：本发明提供氨基甲酸酯官能树脂和包含所述树脂的涂料组合物，其相对于随后施加的膜或涂层具有改善的粘合性。更具体地说，本发明涉及具有每个氨基甲酸酯基团至少250克聚合物的氨基甲酸酯官能加成聚合物，它们以小于35重量％的非官能单体，优选小于20重量％，最优选0至小于10重量％，基于聚合物的总重量。本发明还提供一种制备通过所要求保护的方法制备的氨基甲酸酯官能聚合物和氨基甲酸酯官能聚合物的方法。最后，本发明提供了一种用于改善第一涂料组合物与随后施加的材料的粘附性的方法，以及制备包含涂覆的基材，粘合剂组合物和具有至少一个表面的玻璃的复合材料的方法。

10. 发明授权

US06462144B1 Carbamate-functional resins and their use in high solids coating compositions 有权
标题翻译：氨基甲酸酯官能树脂及其在高固含量涂料组合物中的应用
公开(公告)号：US06462144B1
公开(公告)日：2002-10-08
申请号：US09793289
申请日：2001-02-26
申请人： Swaminathan Ramesh , Marvin L. Green , Donald H. Campbell , Walter H. Ohrbom
发明人： Swaminathan Ramesh , Marvin L. Green , Donald H. Campbell , Walter H. Ohrbom
IPC分类号： C08G1832
CPC分类号： C09D201/025 , C09D201/005 , Y10T428/31511 , Y10T428/31551
摘要： The present invention provides a coating composition containing 1) a carbamate-functional resin having in its structure a hyperbranched or star polyol core, a first chain extension based on a polycarboxylic acid or anbydride, a second chain extension based on an epoxy containing compound, and having carbamate functional groups on the core, the second chain extension, or both; and 2) a second resin containing functional groups reactive with the carbamate groups on the carbamate-functional resin. In one embodiment, the coating compositions are used as a cloarcoat to be applied over a basecoat to form a composite coating. The compositions exhibit a combination of desirable properties, such as scratch and mar resistance, resistance to environmental etch, good intercoat adhesion, and high solids.
摘要翻译：本发明提供了一种涂料组合物，其含有1）氨基甲酸酯官能树脂，其结构是其超结构或星型多元醇芯，基于多元羧酸或二硼化物的第一链延伸，基于含环氧化合物的第二链延伸，以及在芯上具有氨基甲酸酯官能团，第二链延伸部分或两者; 和2）含有与氨基甲酸酯官能树脂上的氨基甲酸酯基反应的官能团的第二树脂。在一个实施方案中，涂料组合物用作蜡涂层以涂覆在底涂层上以形成复合涂层。组合物显示出所需性能的组合，例如耐刮擦和耐擦伤性，耐环境腐蚀性，良好的涂层间粘合性和高固含量。

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