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1. 发明授权

US06624336B1 Process for producing tetrafluorobenzenemethanols 失效
标题翻译：四氟苯甲醇的制备方法
公开(公告)号：US06624336B1
公开(公告)日：2003-09-23
申请号：US09959715
申请日：2001-11-05
申请人： Toru Sasaki , Tetsuhiro Furukawa , Toru Yoshida , Yutaka Ohnishi , Hiroyuki Monzen , Hideo Miyata , Kohei Morikawa
发明人： Toru Sasaki , Tetsuhiro Furukawa , Toru Yoshida , Yutaka Ohnishi , Hiroyuki Monzen , Hideo Miyata , Kohei Morikawa
IPC分类号： C07C3346
CPC分类号： C07C47/55 , B01J25/02 , B01J27/055 , C07C29/141 , C07C43/313 , C07C45/44 , C07C45/515 , C07C33/46
摘要： The present invention relates to a process by a series of reactions using tetrafluorocyanobenzens as material for producing tetrafluorobenzenemethanols, tetrafluorobenzenecarbaldehyde dialkylacetals and tetrafluorobenzenecarbaldehydes in a high purity and a high yield which are useful as intermediates in the production of cyclopropanecarboxylic acid esters having insecticidal action, and also relates to a novel tetrafluorobenzenecarbaldehyde dimethylacetal.
摘要翻译：本发明涉及一种通过一系列反应的方法，该反应使用四氟氰基化合物作为生产具有杀虫作用的环丙烷羧酸酯的中间体而制备四氟苯甲醇，四氟苯甲醛二烷基缩醛和四氟苯甲醛的高纯度和高收率的材料，涉及一种新的四氟苯甲醛二甲缩醛。

2. 发明授权

US6020517A Process for production of benzonitrile and benzyl alcohol 失效
标题翻译：苄腈和苄醇的生产方法
公开(公告)号：US6020517A
公开(公告)日：2000-02-01
申请号：US65043
申请日：1998-04-27
申请人： Hiroyuki Monzen , Katsutoshi Morinaka , Hideo Miyata , Tsutomu Nozawa , Haruaki Ito , Kohei Morikawa
发明人： Hiroyuki Monzen , Katsutoshi Morinaka , Hideo Miyata , Tsutomu Nozawa , Haruaki Ito , Kohei Morikawa
IPC分类号： C07C29/00 , C07C29/141 , C07C29/149 , C07C253/30 , C07C255/50 , C07C255/00 , C07C27/00 , C07C33/46
CPC分类号： C07C29/00 , C07C253/30 , C07C29/141 , C07C29/149
摘要： A process for producing a fluorinated benzonitrile comprising hydrogenolyzing a fluorinated dicyanobenzene substituted with 1 to 4 fluorine atoms and having the remainder which may be substituted with a chlorine atom in the presence of a catalyst to cause hydrodecyanation of only the cyano group of one side and a process for producing a fluorinated benzyl alcohol comprising reducing the fluorinated benzonitrile and hydrolyzing the fluorinated benzonitrile and reducing the resultant corresponding fluorinated benzoic acid to convert the cyano group to a hydroxymethyl group.
摘要翻译： PCT No.PCT / JP97 / 03037 Sec。 371日期：1998年4月27日 102（e）日期1998年4月27日PCT 1997年8月29日PCT公布。出版物WO98 / 08795 日期：1998年3月5日一种氟化苄腈的制造方法，其特征在于，在催化剂存在下，使用氟原子取代的氟代二氰基苯取代有氟原子，剩余部分可以被氯原子取代，使氰基只进行水解，并且包括还原氟化苄腈并水解氟化苄腈并还原所得相应的氟代苯甲酸以将氰基转化为羟甲基。

3. 发明授权

US06180801B2 Method for manufacturing 3-isochromanone 失效
标题翻译： 3-异色满酮的制备方法
公开(公告)号：US06180801B2
公开(公告)日：2001-01-30
申请号：US09277941
申请日：1999-03-29
申请人： Hiroyuki Monzen , Hideo Miyata , Kimitaka Ooshiro , Kohei Morikawa
发明人： Hiroyuki Monzen , Hideo Miyata , Kimitaka Ooshiro , Kohei Morikawa
IPC分类号： C07D31102
CPC分类号： C07D311/76
摘要： The present invention intends to provide a method for producing 3-isochromanones represented by formula (II) useful as a synthetic starting material of medicals or agricultural chemicals and the cyano compound represented by formula (I) by an industrially advantageous method in a high yield. Disclosed herein is a method for manufacturing a 3-isochromanone represented by the following formula (II): (wherein R2, R3, R4 and R5 each independently represents a hydrogen atom, a halogen atom, an alkyl group or an alkoxy group), said method is characterized by comprising the steps of: hydrolyzing a cyano compound represented by formula (I): (wherein R1 represents a hydrogen atom, an alkyl group or an aryl group, and R2, R3, R4 and R5 have the same meanings as defined above) and subjecting the hydrolyzate to intra-molecular cyclization.
摘要翻译：本发明意在提供一种由工业上有利的方法以高产率制备可用作医药或农药合成原料的式（II）表示的3-异色满酮和由式（I）表示的氰基化合物的方法。本文公开了一种制备由下式（II）表示的3-异色满酮的方法：其中R2，R3，R4和R5各自独立地表示氢原子，卤原子，烷基或烷氧基），所述方法的特征在于包括以下步骤：水解由式（I）表示的氰基化合物:(其中R1表示氢原子，烷基或芳基，R2，R3，R4和R5具有与定义相同的含义）并使水解产物进行分子内环化。

4. 发明授权

US06245920B1 Metal raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：金属催化剂和氢化化合物的制备
公开(公告)号：US06245920B1
公开(公告)日：2001-06-12
申请号：US09451145
申请日：1999-11-30
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07D30702
CPC分类号： B01J25/00
摘要： Noble metal, particularly ruthenium, Raney catalysts which can hydrogenate (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，可加氢氢化（1）芳香性显示有机化合物的环部分的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧酸或其酯基在具有这种环部分的化合物和羧酸或其酯部分中，和（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

5. 发明授权

US5496532A Process for producing hydrogen peroxide 失效
标题翻译：生产过氧化氢的方法
公开(公告)号：US5496532A
公开(公告)日：1996-03-05
申请号：US256603
申请日：1994-07-19
申请人： Hiroyuki Monzen , Kazuhiko Hiromoto , Shuji Hirayama , Nobuyuki Kondo , Haruki Ishigami , Yoshimasa Ishimura
发明人： Hiroyuki Monzen , Kazuhiko Hiromoto , Shuji Hirayama , Nobuyuki Kondo , Haruki Ishigami , Yoshimasa Ishimura
IPC分类号： C01B15/022 , C01B15/029 , C01B15/01
CPC分类号： C01B15/022 , C01B15/029
摘要： A process for producing hydrogen peroxide, comprising the step of producing hydrogen peroxide catalytically from hydrogen and oxygen in a reaction medium, wherein a platinum-group metal catalyst is used which comprises a platinum-group metal and, supported thereon, a niobium oxide, a mixed oxide of niobium, a tantalum oxide, a mixed oxide of tantalum, a molybdenum oxide or a tungsten oxide.
摘要翻译： PCT No.PCT / JP93 / 01678 Sec。 371日期：1994年7月19日 102（e）日期1994年7月19日PCT 1993年11月16日PCT公布。公开号WO94 / 12428 日本6月9日，1994年。一种生产过氧化氢的方法，包括在反应介质中由氢和氧催化生产过氧化氢的步骤，其中使用铂族金属催化剂，其包含铂族金属，并且被负载氧化铌，铌的混合氧化物，氧化钽，钽的混合氧化物，氧化钼或氧化钨。

6. 发明授权

US06215030B1 Noble metal raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：贵金属催化剂和氢化化合物的制备
公开(公告)号：US06215030B1
公开(公告)日：2001-04-10
申请号：US09451146
申请日：1999-11-30
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07C2704
CPC分类号： C07C29/20 , B01J25/00 , C07C51/36 , C07C51/367 , C07C67/31 , C07C209/48 , C07C2601/14 , C07C2602/28 , C07D211/02 , C07C35/21 , C07C31/276 , C07C31/20 , C07C35/08 , C07C31/1355 , C07C61/08 , C07C59/01 , C07C69/675
摘要： Noble metal, particularly ruthenium, Raney catalysts which can hydrogenate (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，可加氢氢化（1）芳香性显示有机化合物的环部分的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧酸或其酯基在具有这种环部分的化合物和羧酸或其酯部分中，和（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

7. 发明授权

US06018048A Noble metal Raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：贵金属阮内催化剂及其氢化化合物的制备
公开(公告)号：US06018048A
公开(公告)日：2000-01-25
申请号：US989157
申请日：1997-12-11
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07D251/04 , B01J25/00 , C07B61/00 , C07C5/10 , C07C29/19 , C07C29/20 , C07C31/13 , C07C31/27 , C07C35/21 , C07C51/36 , C07C51/367 , C07C61/09 , C07C67/31 , C07C209/48 , C07C209/72 , C07C211/46 , C07C211/50 , C07D211/02 , C07D215/02 , C07D217/02 , C07D237/30 , C07D239/74 , C07D241/42 , C07D295/02 , C07D475/00 , C07C5/02
CPC分类号： C07C29/20 , B01J25/00 , C07C209/48 , C07C51/36 , C07C51/367 , C07C67/31 , C07D211/02 , C07C2101/14 , C07C2102/28
摘要： Noble metal, particularly ruthenium, Raney catalysts having the property of catalyzing the hydrogenation of (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，具有催化（1）有机化合物的芳香性显示环部分的氢化的性质的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧基酸或其酯基，以及（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

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