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1. 发明授权

US06245920B1 Metal raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：金属催化剂和氢化化合物的制备
公开(公告)号：US06245920B1
公开(公告)日：2001-06-12
申请号：US09451145
申请日：1999-11-30
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07D30702
CPC分类号： B01J25/00
摘要： Noble metal, particularly ruthenium, Raney catalysts which can hydrogenate (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，可加氢氢化（1）芳香性显示有机化合物的环部分的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧酸或其酯基在具有这种环部分的化合物和羧酸或其酯部分中，和（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

2. 发明授权

US5693832A Hydroformylation of allyl alcohol 失效
标题翻译：烯丙醇的加氢甲酰化
公开(公告)号：US5693832A
公开(公告)日：1997-12-02
申请号：US266268
申请日：1994-06-27
申请人： Tetsuro Fujita , Kenichiro Maki , Kuniomi Marumo
发明人： Tetsuro Fujita , Kenichiro Maki , Kuniomi Marumo
IPC分类号： C07C45/49 , C07D307/20
CPC分类号： C07D307/20 , C07C45/49
摘要： A process for the hydroformylation of allyl alcohol is disclosed, which comprises reacting allyl alcohol with carbon monoxide and hydrogen in the presence of a rhodium compound and a diphosphine compound represented by formula (I) or (II) ##STR1## wherein R.sup.1 represents an alkyl group or a substituted or unsubstituted aryl group; and R.sup.2 and R.sup.3 each represents an alkyl group or a hydrogen atom.
摘要翻译：公开了烯丙醇加氢甲酰化的方法，其包括在铑化合物和由式（I）或（II）表示的二膦化合物存在下使烯丙醇与一氧化碳和氢反应。 >（II）其中R1表示烷基或取代或未取代的芳基; R2和R3各自表示烷基或氢原子。

3. 发明授权

US4959451A Novel diallyl terephthalate prepolymer and method for preparing it 失效
标题翻译：新型对苯二甲酸二烯丙酯预聚物及其制备方法
公开(公告)号：US4959451A
公开(公告)日：1990-09-25
申请号：US422727
申请日：1989-10-17
申请人： Hiroshi Uchida , Kuniomi Marumo , Shigehiro Chaen
发明人： Hiroshi Uchida , Kuniomi Marumo , Shigehiro Chaen
IPC分类号： C07C69/83 , C08F283/01 , C08F290/00 , C08F291/02 , C08F299/04 , C08G63/21 , C08G63/52 , C08G63/547 , C08L67/06
CPC分类号： C08G63/547 , C08F291/02 , C08F299/0478 , C08F299/0485 , C08L67/06
摘要： A diallyl terephthalate prepolymer is here disclosed which essentially has the following structureCH.sub.2 .dbd.CHCH.sub.2 O(COArCOOBO).sub.n COArCOOCH.sub.2 CH.dbd.CH.sub.2wherein B is a divalent organic residue derived from a diol having 2 to 20 carbon atoms, Ar is a 1,4-phenylene group, and n is a value of 1 to 100, and having an unsaturation in a range of 20 to 100, as represented by an iodine value determine by the Wijs method, and there is also disclosed a method for preparing the diallyl terephthalate prepolymer.The method of the present invention permits obtaining the allyl prepolymer having excellent physical properties from inexpensive raw materials with less labor.Since this prepolymer has a double bond suitably, it can be mixed with unsaturated polyester resin or diallyl phthalate resin, when used. Moreover, the prepolymer can be also used as a crosslinking agent for EPR, elaslene, synthetic rubber and the like.
摘要翻译：此处公开了二烯丙基对苯二酸酯预聚物，其基本上具有以下结构CH 2 = CHCH 2 O（COArCOOBO）n COArCOOCH 2 CH = CH 2其中B是衍生自具有2至20个碳原子的二醇的二价有机残基，Ar是1,4-亚苯基， n为1〜100，不饱和度为20〜100，以由Wijs法测定的碘值表示，并且还公开了对苯二甲酸二烯丙酯预聚物的制备方法。本发明的方法可以从较便宜的原料获得具有优异物理性能的烯丙基预聚物，而且劳动力少。由于该预聚物适当地具有双键，因此可以在使用时与不饱和聚酯树脂或邻苯二甲酸二烯丙酯树脂混合。此外，预聚物也可以用作EPR，金刚石，合成橡胶等的交联剂。

4. 发明授权

US06433211B1 Process for producing cyanobenzoic acid derivatives 失效
标题翻译：制备氰基苯甲酸衍生物的方法
公开(公告)号：US06433211B1
公开(公告)日：2002-08-13
申请号：US09404362
申请日：1999-09-24
申请人： Hiroshi Yasuda , Haruaki Ito , Takashi Tani , Kimitaka Ohshiro , Makoto Saito , Sumio Soya , Kuniomi Marumo
发明人： Hiroshi Yasuda , Haruaki Ito , Takashi Tani , Kimitaka Ohshiro , Makoto Saito , Sumio Soya , Kuniomi Marumo
IPC分类号： C07C25500
CPC分类号： C07C253/30 , C07C255/57
摘要： A process for producing a cyanobenzoic acid compound, a cyanobenzamide compound, an alkyl cyanobenzoate compound, and a cyanobenzoyl chloride compound, which are useful intermediates for a variety of chemicals such as pharmaceuticals, agrochemicals, liquid crystals, and monomers for functional polymers. One nitrile group of an easily available phthalonitrile compound is selectively hydrolyzed to thereby produce a cyanobenzamide compound with high selectivity and yield. The cyanobenzamide compound thus-produced is transformed under acidic conditions into a cyanobenzoic acid compound and a cyanobenzoate ester compound without the cyano group of the benzene ring being damaged.
摘要翻译：用于制备用于各种化学品如药物，农业化学品，液晶和功能性聚合物的单体的有用的中间体的氰基苯甲酸化合物，氰基苯甲酰胺化合物，烷基氰基苯甲酸酯化合物和氰基苯甲酰氯化合物的方法。选择性地水解一种容易获得的邻苯二腈化合物的腈基，从而以高选择性和收率产生氰基苯甲酰胺化合物。将由此制得的氰基苯甲酰胺化合物在酸性条件下转化成氰基苯甲酸化合物和氰基苯甲酸酯化合物，而苯环的氰基不被损坏。

5. 发明授权

US06018048A Noble metal Raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：贵金属阮内催化剂及其氢化化合物的制备
公开(公告)号：US06018048A
公开(公告)日：2000-01-25
申请号：US989157
申请日：1997-12-11
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07D251/04 , B01J25/00 , C07B61/00 , C07C5/10 , C07C29/19 , C07C29/20 , C07C31/13 , C07C31/27 , C07C35/21 , C07C51/36 , C07C51/367 , C07C61/09 , C07C67/31 , C07C209/48 , C07C209/72 , C07C211/46 , C07C211/50 , C07D211/02 , C07D215/02 , C07D217/02 , C07D237/30 , C07D239/74 , C07D241/42 , C07D295/02 , C07D475/00 , C07C5/02
CPC分类号： C07C29/20 , B01J25/00 , C07C209/48 , C07C51/36 , C07C51/367 , C07C67/31 , C07D211/02 , C07C2101/14 , C07C2102/28
摘要： Noble metal, particularly ruthenium, Raney catalysts having the property of catalyzing the hydrogenation of (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，具有催化（1）有机化合物的芳香性显示环部分的氢化的性质的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧基酸或其酯基，以及（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

6. 发明授权

US5344655A External application base or auxiliary agent and external application composition for human being or animal containing the same 失效
标题翻译：外用施用基或辅助剂和外用施用组合物，用于含有其的人或动物
公开(公告)号：US5344655A
公开(公告)日：1994-09-06
申请号：US32100
申请日：1993-03-17
申请人： Yasuyuki Sakai , Noriyuki Suzuki , Tetsuo Kudo , Kuniomi Marumo , Toshiyuki Aizawa , Kunio Imamura , Shuichi Sugita , Kazuo Kanbayashi
发明人： Yasuyuki Sakai , Noriyuki Suzuki , Tetsuo Kudo , Kuniomi Marumo , Toshiyuki Aizawa , Kunio Imamura , Shuichi Sugita , Kazuo Kanbayashi
IPC分类号： A61K9/06 , A61K9/00 , A61K9/70 , A61K47/32 , A61L15/58
CPC分类号： A61K9/7053 , A61K47/32 , A61K9/0014 , A61K9/7023 , A61K9/7061
摘要： A (co)polymer suitable for bases or auxiliary agents for external application (for example, hydrophilic gels, adhesives, thickeners or excipients) to be coated or plastered onto the skin or mucosa of a human being or animal, such as ointment agents (ointment, hydrogel, jelly or cream), plastering agents (molded poultice, tape agent or plaster agent), sticky bandages (sticky bandage, strap, wound strap, surgical tape, taping material, supporter), and to preparations for external application containing same.
摘要翻译：适用于外用（例如，亲水性凝胶，粘合剂，增稠剂或赋形剂）的底物或助剂的（共）聚合物，其被涂覆或涂抹在人或动物的皮肤或粘膜上，例如软膏剂，水凝胶，果冻或奶油），抹灰剂（成型的泥敷剂，胶带剂或石膏剂），粘性绷带（粘性绷带，皮带，缠绕带，手术胶带，胶带材料，支持物）以及用于包含其的外部应用的制剂。

7. 发明授权

US4997984A Process for preparation of N-(.alpha.-alkoxyethyl)-carboxylic acid amide 失效
标题翻译：制备N-（α-烷氧基乙基） - 羧酸酰胺的方法
公开(公告)号：US4997984A
公开(公告)日：1991-03-05
申请号：US452936
申请日：1989-12-19
申请人： Shuichi Sugita , Tetsuo Kudo , Kuniomi Marumo
发明人： Shuichi Sugita , Tetsuo Kudo , Kuniomi Marumo
IPC分类号： C07C231/12
CPC分类号： C07C231/12 , Y02P20/582
摘要： A process for the preparation of an N-(.alpha.-alkoxyethyl)carboxylic acid amide represented by the following formula [I]: ##STR1## wherein R stands for a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a benzyl group or an aryl group, and R.sup.1 stands for an alkyl group having 1 to 10 carbon atoms or a cycloalkyl group,which comprises reacting an ethylidene-bisamide represented by the following formula [II]:CH.sub.3 CH(NHCOR).sub.2 [II]wherein R stands for a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a benzyl group or an aryl group,with an alkanol in the presence of an acid catalyst. According to this process, a high-purity N-(.alpha.-alkoxyethyl)carboxylic acid amide, which is valuable as an intermediate for the production of an N-vinylcarboxylic acid amide and the like, can be easily prepared from cheap and easily available starting materials.
摘要翻译：由下式[I]表示的制备N-（α-烷氧基乙基）羧酸酰胺的方法：其中R代表氢原子，具有1至6个碳原子的烷基，苄基或芳基，R1表示碳原子数1〜10的烷基或环烷基，其包括使下式[II]表示的亚乙基双酰胺与CH 3 CH（NHCOR）2 [II] 其中R代表氢原子，具有1至6个碳原子的烷基，苄基或芳基，与烷基醇在酸催化剂存在下反应。根据该方法，可以从便宜且容易获得的起始物中容易地制备作为制备N-乙烯基羧酸酰胺等的中间体有价值的高纯度N-（α-烷氧基乙基）羧酸酰胺材料

8. 发明授权

US3959297A Process for the preparation of 3-cyanopyridine 失效
标题翻译： 3-氰基吡啶的制备方法
公开(公告)号：US3959297A
公开(公告)日：1976-05-25
申请号：US553627
申请日：1975-02-27
申请人： Ryoji Ishioka , Norio Kametaka , Kuniomi Marumo
发明人： Ryoji Ishioka , Norio Kametaka , Kuniomi Marumo
IPC分类号： B01J23/20 , B01J23/30 , C07D213/84 , C07D213/85 , C07D213/57
CPC分类号： C07D213/84 , B01J23/20 , B01J23/30 , C07D213/85
摘要： A process for preparing 3-cyanopyridine by the ammoxidation of 2-methyl-5-ethylpyridine which comprises reacting 2-methyl-5-ethylpyridine with ammonia and oxygen in the vapor phase at an elevated temperature, using a specific catalyst consisting of a low-area carrier on which has been deposited vanadium oxide and other specific metal oxides, the reaction being carried out in the copresence of steam.
摘要翻译：通过2-甲基-5-乙基吡啶的氨氧化制备3-氰基吡啶的方法，其包括使2-甲基-5-乙基吡啶与氨和氧在气相中在升高的温度下反应，使用由低 - 其上已经沉积有氧化钒和其它特定的金属氧化物的区域载体，反应在蒸汽共存下进行。

9. 发明授权

US5003020A Diallyl terephthalate prepolymer and process for producing seam 失效
标题翻译：对苯二甲酸二烯丙酯预聚物和生产接缝的方法
公开(公告)号：US5003020A
公开(公告)日：1991-03-26
申请号：US235599
申请日：1988-08-24
申请人： Hiroshi Uchida , Shigehiro Chaen , Kuniomi Marumo
发明人： Hiroshi Uchida , Shigehiro Chaen , Kuniomi Marumo
IPC分类号： C08F18/18
CPC分类号： C08F18/18
摘要： A diallyl terephthalate prepolymer consisting essentially of diallyl terephthalate monomer units, having(a) 10 or less of the monomer units in the carbon-carbon bonded molecular chain portion which is composed of the allyl groups of the monomer units, and either(b) an unsaturation in a range of from 40 to 70, as represented by an iodine value determined by the Wijs method,(c) a number-average molecular weight in a range of from 6,000 to 10,000 as polystyrene, and a weight-average molecular weight in a range of from 10,000 to 70,000 as polystyrene, both being determined by gel permeation chromatography, and(d) a melt viscosity in a range of from 30,000 to 90,000 CP at 170.degree. C., as determined by a Koka flow tester, or(b) an unsaturation in a range of from 50 to 80, as represented by an iodine value determined by the Wijs method,(c) a number-average molecular weight in a range of from 8,000 to 20,000 as polystyrene, and a weight-average molecular weight in a range of from 30,000 to 90,000 as polystyrene, both being determined by gel permeation chromatography, and(d) a melt viscosity in a range of from 20,000 to 90,000 CP at 130.degree. C., as determined by a Koka flow tester.

10. 发明授权

US3957804A Method for the production of nicotinamide and isonicotinamide 失效
标题翻译：生产尼古丁胺和异烟肼的方法
公开(公告)号：US3957804A
公开(公告)日：1976-05-18
申请号：US610406
申请日：1975-09-04
申请人： Ryoji Ishioka , Norio Kametaka , Kuniomi Marumo
发明人： Ryoji Ishioka , Norio Kametaka , Kuniomi Marumo
IPC分类号： C07D213/82 , B01J21/00 , B01J23/00 , B01J23/755 , C07B61/00 , C07D213/81 , C07D213/56
CPC分类号： C07D213/81 , B01J23/755
摘要： A method for the production of nicotinamide or isonicotinamide by catalytically hydrating 3- or 4-cyanopyridine which is characterized in that the hydration reaction is carried out in the presence of a nickel oxide/iron oxide combined catalyst.

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