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1. 发明授权

US06245920B1 Metal raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：金属催化剂和氢化化合物的制备
公开(公告)号：US06245920B1
公开(公告)日：2001-06-12
申请号：US09451145
申请日：1999-11-30
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07D30702
CPC分类号： B01J25/00
摘要： Noble metal, particularly ruthenium, Raney catalysts which can hydrogenate (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，可加氢氢化（1）芳香性显示有机化合物的环部分的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧酸或其酯基在具有这种环部分的化合物和羧酸或其酯部分中，和（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

2. 发明授权

US06018048A Noble metal Raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：贵金属阮内催化剂及其氢化化合物的制备
公开(公告)号：US06018048A
公开(公告)日：2000-01-25
申请号：US989157
申请日：1997-12-11
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07D251/04 , B01J25/00 , C07B61/00 , C07C5/10 , C07C29/19 , C07C29/20 , C07C31/13 , C07C31/27 , C07C35/21 , C07C51/36 , C07C51/367 , C07C61/09 , C07C67/31 , C07C209/48 , C07C209/72 , C07C211/46 , C07C211/50 , C07D211/02 , C07D215/02 , C07D217/02 , C07D237/30 , C07D239/74 , C07D241/42 , C07D295/02 , C07D475/00 , C07C5/02
CPC分类号： C07C29/20 , B01J25/00 , C07C209/48 , C07C51/36 , C07C51/367 , C07C67/31 , C07D211/02 , C07C2101/14 , C07C2102/28
摘要： Noble metal, particularly ruthenium, Raney catalysts having the property of catalyzing the hydrogenation of (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，具有催化（1）有机化合物的芳香性显示环部分的氢化的性质的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧基酸或其酯基，以及（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

3. 发明授权

US06215030B1 Noble metal raney catalysts and preparation of hydrogenated compounds therewith 失效
标题翻译：贵金属催化剂和氢化化合物的制备
公开(公告)号：US06215030B1
公开(公告)日：2001-04-10
申请号：US09451146
申请日：1999-11-30
申请人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
发明人： Kouhei Morikawa , Shuuji Hirayama , Yoshimasa Ishimura , Yuseki Suyama , Tsutomu Nozawa , Hiroyuki Monzen , Motoo Miura , Kuniomi Marumo , Taketoshi Naito
IPC分类号： C07C2704
CPC分类号： C07C29/20 , B01J25/00 , C07C51/36 , C07C51/367 , C07C67/31 , C07C209/48 , C07C2601/14 , C07C2602/28 , C07D211/02 , C07C35/21 , C07C31/276 , C07C31/20 , C07C35/08 , C07C31/1355 , C07C61/08 , C07C59/01 , C07C69/675
摘要： Noble metal, particularly ruthenium, Raney catalysts which can hydrogenate (1) aromaticity-exhibiting ring portions of organic compounds, (2) carboxylic acids and their ester portions (carbonyl ester groups), (3) ring portions and carboxylic acid or their ester groups in compounds having such ring portions and carboxylic acid or their ester portions, and (4) ring portions and nitrile groups of aromatic nitrile compounds and methods for the preparation of corresponding hydrogenated compounds. The methods allow preparation of hydrogenated compounds having hydrogenated aromatic ring portions, hydrogenated carbonyl ester groups, hydrogenated aromatic ring and carbonyl ester groups, or hydrogenated aromatic rings and nitrile groups under milder hydrogen pressure and temperature conditions than the conventional catalysts.
摘要翻译：贵金属，特别是钌，可加氢氢化（1）芳香性显示有机化合物的环部分的阮内催化剂，（2）羧酸及其酯部分（羰基酯基），（3）环部分和羧酸或其酯基在具有这种环部分的化合物和羧酸或其酯部分中，和（4）芳族腈化合物的环部分和腈基以及制备相应的氢化化合物的方法。该方法允许在比常规催化剂更温和的氢气压力和温度条件下，制备具有氢化芳环部分，氢化羰基酯基，氢化芳环和羰基酯基，或氢化芳环和腈基的氢化化合物。

4. 发明授权

US5693832A Hydroformylation of allyl alcohol 失效
标题翻译：烯丙醇的加氢甲酰化
公开(公告)号：US5693832A
公开(公告)日：1997-12-02
申请号：US266268
申请日：1994-06-27
申请人： Tetsuro Fujita , Kenichiro Maki , Kuniomi Marumo
发明人： Tetsuro Fujita , Kenichiro Maki , Kuniomi Marumo
IPC分类号： C07C45/49 , C07D307/20
CPC分类号： C07D307/20 , C07C45/49
摘要： A process for the hydroformylation of allyl alcohol is disclosed, which comprises reacting allyl alcohol with carbon monoxide and hydrogen in the presence of a rhodium compound and a diphosphine compound represented by formula (I) or (II) ##STR1## wherein R.sup.1 represents an alkyl group or a substituted or unsubstituted aryl group; and R.sup.2 and R.sup.3 each represents an alkyl group or a hydrogen atom.
摘要翻译：公开了烯丙醇加氢甲酰化的方法，其包括在铑化合物和由式（I）或（II）表示的二膦化合物存在下使烯丙醇与一氧化碳和氢反应。 >（II）其中R1表示烷基或取代或未取代的芳基; R2和R3各自表示烷基或氢原子。

5. 发明授权

US4959451A Novel diallyl terephthalate prepolymer and method for preparing it 失效
标题翻译：新型对苯二甲酸二烯丙酯预聚物及其制备方法
公开(公告)号：US4959451A
公开(公告)日：1990-09-25
申请号：US422727
申请日：1989-10-17
申请人： Hiroshi Uchida , Kuniomi Marumo , Shigehiro Chaen
发明人： Hiroshi Uchida , Kuniomi Marumo , Shigehiro Chaen
IPC分类号： C07C69/83 , C08F283/01 , C08F290/00 , C08F291/02 , C08F299/04 , C08G63/21 , C08G63/52 , C08G63/547 , C08L67/06
CPC分类号： C08G63/547 , C08F291/02 , C08F299/0478 , C08F299/0485 , C08L67/06
摘要： A diallyl terephthalate prepolymer is here disclosed which essentially has the following structureCH.sub.2 .dbd.CHCH.sub.2 O(COArCOOBO).sub.n COArCOOCH.sub.2 CH.dbd.CH.sub.2wherein B is a divalent organic residue derived from a diol having 2 to 20 carbon atoms, Ar is a 1,4-phenylene group, and n is a value of 1 to 100, and having an unsaturation in a range of 20 to 100, as represented by an iodine value determine by the Wijs method, and there is also disclosed a method for preparing the diallyl terephthalate prepolymer.The method of the present invention permits obtaining the allyl prepolymer having excellent physical properties from inexpensive raw materials with less labor.Since this prepolymer has a double bond suitably, it can be mixed with unsaturated polyester resin or diallyl phthalate resin, when used. Moreover, the prepolymer can be also used as a crosslinking agent for EPR, elaslene, synthetic rubber and the like.
摘要翻译：此处公开了二烯丙基对苯二酸酯预聚物，其基本上具有以下结构CH 2 = CHCH 2 O（COArCOOBO）n COArCOOCH 2 CH = CH 2其中B是衍生自具有2至20个碳原子的二醇的二价有机残基，Ar是1,4-亚苯基， n为1〜100，不饱和度为20〜100，以由Wijs法测定的碘值表示，并且还公开了对苯二甲酸二烯丙酯预聚物的制备方法。本发明的方法可以从较便宜的原料获得具有优异物理性能的烯丙基预聚物，而且劳动力少。由于该预聚物适当地具有双键，因此可以在使用时与不饱和聚酯树脂或邻苯二甲酸二烯丙酯树脂混合。此外，预聚物也可以用作EPR，金刚石，合成橡胶等的交联剂。

6. 发明授权

US5003020A Diallyl terephthalate prepolymer and process for producing seam 失效
标题翻译：对苯二甲酸二烯丙酯预聚物和生产接缝的方法
公开(公告)号：US5003020A
公开(公告)日：1991-03-26
申请号：US235599
申请日：1988-08-24
申请人： Hiroshi Uchida , Shigehiro Chaen , Kuniomi Marumo
发明人： Hiroshi Uchida , Shigehiro Chaen , Kuniomi Marumo
IPC分类号： C08F18/18
CPC分类号： C08F18/18
摘要： A diallyl terephthalate prepolymer consisting essentially of diallyl terephthalate monomer units, having(a) 10 or less of the monomer units in the carbon-carbon bonded molecular chain portion which is composed of the allyl groups of the monomer units, and either(b) an unsaturation in a range of from 40 to 70, as represented by an iodine value determined by the Wijs method,(c) a number-average molecular weight in a range of from 6,000 to 10,000 as polystyrene, and a weight-average molecular weight in a range of from 10,000 to 70,000 as polystyrene, both being determined by gel permeation chromatography, and(d) a melt viscosity in a range of from 30,000 to 90,000 CP at 170.degree. C., as determined by a Koka flow tester, or(b) an unsaturation in a range of from 50 to 80, as represented by an iodine value determined by the Wijs method,(c) a number-average molecular weight in a range of from 8,000 to 20,000 as polystyrene, and a weight-average molecular weight in a range of from 30,000 to 90,000 as polystyrene, both being determined by gel permeation chromatography, and(d) a melt viscosity in a range of from 20,000 to 90,000 CP at 130.degree. C., as determined by a Koka flow tester.

7. 发明授权

US3957804A Method for the production of nicotinamide and isonicotinamide 失效
标题翻译：生产尼古丁胺和异烟肼的方法
公开(公告)号：US3957804A
公开(公告)日：1976-05-18
申请号：US610406
申请日：1975-09-04
申请人： Ryoji Ishioka , Norio Kametaka , Kuniomi Marumo
发明人： Ryoji Ishioka , Norio Kametaka , Kuniomi Marumo
IPC分类号： C07D213/82 , B01J21/00 , B01J23/00 , B01J23/755 , C07B61/00 , C07D213/81 , C07D213/56
CPC分类号： C07D213/81 , B01J23/755
摘要： A method for the production of nicotinamide or isonicotinamide by catalytically hydrating 3- or 4-cyanopyridine which is characterized in that the hydration reaction is carried out in the presence of a nickel oxide/iron oxide combined catalyst.

8. 发明授权

US4278820A Process for preparing monoalkylene glycol monoethers 失效
标题翻译：单亚烷基二醇单醚的制备方法
公开(公告)号：US4278820A
公开(公告)日：1981-07-14
申请号：US81619
申请日：1979-10-03
申请人： Norio Kametaka , Kuniomi Marumo , Tutomu Nozawa
发明人： Norio Kametaka , Kuniomi Marumo , Tutomu Nozawa
IPC分类号： C07C41/02 , B01J21/00 , C07B61/00 , C07C41/00 , C07C41/03 , C07C43/13 , C07C67/00
CPC分类号： C07C41/03
摘要： A monoalkylene glycol monoether is produced with good efficiency and commercial advantage by reacting an alkylene oxide with an alcohol in the presence of a solid catalyst resulting from the exchange of exchangeable cations of a montmorillonite clay with a cation of Al, Cr, Mn, Fe, Sn or Th.
摘要翻译：通过在固体催化剂的存在下使烯化氧与醇反应，通过使蒙脱石粘土的交换性阳离子与Al，Cr，Mn，Fe等阳离子交换而得到，从而生产单亚烷基二醇单醚， Sn或Th。

9. 发明授权

US4260813A Process for the continuous production of ethylene glycol monoethyl ether acetate 失效
标题翻译：连续生产乙二醇单乙醚乙酸酯的方法
公开(公告)号：US4260813A
公开(公告)日：1981-04-07
申请号：US8341
申请日：1979-01-31
申请人： Norio Kametaka , Kuniomi Marumo , Kiyonori Tokuda , Kazuo Sekiguchi
发明人： Norio Kametaka , Kuniomi Marumo , Kiyonori Tokuda , Kazuo Sekiguchi
IPC分类号： C07C67/03 , C07C67/54
CPC分类号： C07C67/03 , Y10S203/20
摘要： Ethyl acetate and an excess of ethylene glycol monoethyl ether are subjected to ester-interchange reaction at a temperature not exceeding 100.degree. C. in the presence of a strongly acidic cation exchange resin as a catalyst. The resulting reaction mixture is distilled to recover the ethylene glycol monoethyl ether acetate formed. The unchanged reactants are recycled to the reaction zone for re-use, and the by-product ethanol is recovered in a highly pure form. This method can be continuously performed easily and effectively without the need to separate the catalyst or to employ complex distilling steps and without involving other difficulties.
摘要翻译：乙酸乙酯和过量的乙二醇单乙醚在强酸性阳离子交换树脂作为催化剂存在下，在不超过100℃的温度下进行酯交换反应。将所得反应混合物蒸馏以回收形成的乙二醇单乙醚乙酸酯。不变的反应物被再循环到反应区以供再利用，并且以高纯度形式回收副产物乙醇。该方法可以容易且有效地连续进行，而不需要分离催化剂或采用复杂的蒸馏步骤而不涉及其它困难。

10. 发明授权

US06433211B1 Process for producing cyanobenzoic acid derivatives 失效
标题翻译：制备氰基苯甲酸衍生物的方法
公开(公告)号：US06433211B1
公开(公告)日：2002-08-13
申请号：US09404362
申请日：1999-09-24
申请人： Hiroshi Yasuda , Haruaki Ito , Takashi Tani , Kimitaka Ohshiro , Makoto Saito , Sumio Soya , Kuniomi Marumo
发明人： Hiroshi Yasuda , Haruaki Ito , Takashi Tani , Kimitaka Ohshiro , Makoto Saito , Sumio Soya , Kuniomi Marumo
IPC分类号： C07C25500
CPC分类号： C07C253/30 , C07C255/57
摘要： A process for producing a cyanobenzoic acid compound, a cyanobenzamide compound, an alkyl cyanobenzoate compound, and a cyanobenzoyl chloride compound, which are useful intermediates for a variety of chemicals such as pharmaceuticals, agrochemicals, liquid crystals, and monomers for functional polymers. One nitrile group of an easily available phthalonitrile compound is selectively hydrolyzed to thereby produce a cyanobenzamide compound with high selectivity and yield. The cyanobenzamide compound thus-produced is transformed under acidic conditions into a cyanobenzoic acid compound and a cyanobenzoate ester compound without the cyano group of the benzene ring being damaged.
摘要翻译：用于制备用于各种化学品如药物，农业化学品，液晶和功能性聚合物的单体的有用的中间体的氰基苯甲酸化合物，氰基苯甲酰胺化合物，烷基氰基苯甲酸酯化合物和氰基苯甲酰氯化合物的方法。选择性地水解一种容易获得的邻苯二腈化合物的腈基，从而以高选择性和收率产生氰基苯甲酰胺化合物。将由此制得的氰基苯甲酰胺化合物在酸性条件下转化成氰基苯甲酸化合物和氰基苯甲酸酯化合物，而苯环的氰基不被损坏。

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