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1. 发明授权

US06309997B1 Olefin polymerization catalysts, transition metal compounds, processes for olefin polymerization, and &agr;-olefin/conjugated diene copolymers 失效
标题翻译：烯烃聚合催化剂，过渡金属化合物，烯烃聚合方法和α-烯烃/共轭二烯共聚物
公开(公告)号：US06309997B1
公开(公告)日：2001-10-30
申请号：US09065593
申请日：1998-04-24
申请人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
发明人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
IPC分类号： B01J2106
CPC分类号： C08F210/02 , C07F7/003 , C07F7/0803 , C07F9/005 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F2500/17 , C08F2500/01 , C08F2500/03 , C08F236/06 , C08F210/06 , C08F4/64189 , C08F4/64048 , C08F4/7022 , C08F4/6812
摘要： The invention provides olefin polymerization catalyst exhibiting excellent polymerization activities, a process for olefin polymerization using the catalyst, a novel transition metal compound useful for the catalyst, and an &agr;-olefin/conjugated diene copolymer having specific properties. The olefin polymerization catalyst of the invention comprises (A) a transition metal compound of formula (I) or (II), and (B) an organometallic compound, an oranoaluminum oxy-compound or an ionizing ionic compound. The novel transition metal compound of the invention is a compound of formula (I) wherein M is a transition meal atom of Group 3 or 4 of the periodic table; m is an integer of 1 to 3; R1 is a hydrocarbon group, etc.; R2 to R5 are each H, a halogen, a hydrocarbon group, etc.; R6 is a halogen, a hydrocarbon group, etc.; n is a number satisfying a valence of M; and X is a halogen, a hydrocarbon group, etc.
摘要翻译：本发明提供了表现出优异聚合活性的烯烃聚合催化剂，使用该催化剂的烯烃聚合方法，用于催化剂的新型过渡金属化合物和具有特定性能的α-烯烃/共轭二烯共聚物。本发明的烯烃聚合催化剂包含（A）式（I）或（II）的过渡金属化合物和（B）有机金属化合物，或者是含有氧化铝的氧化合物或离子化离子化合物。本发明的新型过渡金属化合物是式（I）的化合物，其中M是周期表第3或4族的过渡膳食原子; m为1〜3的整数。 R1是烃基等; R2至R5各自为H，卤素，烃基等; R6是卤素，烃基等; n是满足M价的数; X为卤素，烃基等

2. 发明申请

US20050124771A1 Olefin polymerization catalysts, transition metal compounds, processes for olefin polymerization, and alpha-olefin/conjugated diene copolymers 有权
标题翻译：烯烃聚合催化剂，过渡金属化合物，烯烃聚合方法和α-烯烃/共轭二烯共聚物
公开(公告)号：US20050124771A1
公开(公告)日：2005-06-09
申请号：US11028923
申请日：2005-01-05
申请人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
发明人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
IPC分类号： C08F210/04 , C07F7/00 , C07F7/08 , C07F9/00 , C08F4/602 , C08F110/02 , C08F110/06 , C08F210/02 , C08F210/12 , C08F210/16 , C08F4/44
CPC分类号： C08F210/02 , C07F7/003 , C07F7/0803 , C07F9/005 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F2500/17 , C08F2500/01 , C08F2500/03 , C08F236/06 , C08F210/06 , C08F4/64189 , C08F4/64048 , C08F4/7022 , C08F4/6812
摘要： The invention provides a process using olefin polymerization catalysts exhibiting excellent polymerization activities. The olefin polymerization catalysts of the invention contain a transition metal compound of and at least one of an organometallic compound, an organoaluminum oxy-compound or a compound which reacts with said transition metal compound to form an ion pair. The process using the inventive catalysts is useful in producing α-olefin/conjugated diene copolymers having specific properties.
摘要翻译：本发明提供一种使用显示优异聚合活性的烯烃聚合催化剂的方法。本发明的烯烃聚合催化剂含有有机金属化合物，有机铝氧化合物或与所述过渡金属化合物反应形成离子对的化合物中的至少一种的过渡金属化合物。使用本发明催化剂的方法可用于制备具有特定性质的α-烯烃/共轭二烯共聚物。

3. 发明授权

US06875718B2 Olefin polymerization catalysts, transition metal compounds, processes for olefin polymerization, and α-olefin/conjugated diene copolymers 有权
标题翻译：烯烃聚合催化剂，过渡金属化合物，烯烃聚合方法和α-烯烃/共轭二烯共聚物
公开(公告)号：US06875718B2
公开(公告)日：2005-04-05
申请号：US09942706
申请日：2001-08-31
申请人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
发明人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
IPC分类号： C08F210/04 , C07F7/00 , C07F7/08 , C07F9/00 , C08F4/602 , C08F110/02 , C08F110/06 , C08F210/02 , C08F210/12 , C08F210/16 , B01J31/00 , B01J37/00 , C08F4/02 , C08F4/60 , C08F4/44
CPC分类号： C08F210/02 , C07F7/003 , C07F7/0803 , C07F9/005 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F2500/17 , C08F2500/01 , C08F2500/03 , C08F236/06 , C08F210/06 , C08F4/64189 , C08F4/64048 , C08F4/7022 , C08F4/6812
摘要： The invention provides olefin polymerization catalysts exhibiting excellent polymerization activities, a process for olefin polymerization using the catalysts, a novel transition metal compound useful for the catalysts, and α-olefin/conjugated diene copolymers having specific properties. The olefin polymerization catalysts of the invention contain (A) a transition metal compound of formula (I), and (B) an organometallic compound, an organoaluminum oxy-compound or an ionizing ionic compound. The novel transition metal compounds of the invention are compounds of formula (I) wherein M is a transition metal atom of Group 3 or 4 of the periodic table; R1 is a hydrocarbon group, etc.; R2 to R5 are each H, a halogen, a hydrocarbon group, etc.; R6 is a halogen, a hydrocarbon group, etc.; n is a number satisfying a valence of M; and X is a halogen, a hydrocarbon group, etc
摘要翻译：本发明提供了表现出优异聚合活性的烯烃聚合催化剂，使用该催化剂的烯烃聚合方法，用于该催化剂的新型过渡金属化合物和具有特定性质的α-烯烃/共轭二烯共聚物。本发明的烯烃聚合催化剂含有（A）式（I）的过渡金属化合物和（B）有机金属化合物，有机铝氧化合物或离子化离子化合物。本发明的新型过渡金属化合物是式（I）的化合物，其中M是周期表第3或4族的过渡金属原子; R 1是烃基等; R 2〜R 5各自为H，卤素，烃基等; R 6是卤素，烃基等; n是满足M价的数; X为卤素，烃基等

4. 发明授权

US07300903B2 Olefin polymerization catalysts, transition metal compounds, processes for olefin polymerization, and α-olefin/conjugated diene copolymers 有权
标题翻译：烯烃聚合催化剂，过渡金属化合物，烯烃聚合方法和α-烯烃/共轭二烯共聚物
公开(公告)号：US07300903B2
公开(公告)日：2007-11-27
申请号：US11028923
申请日：2005-01-05
申请人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
发明人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
IPC分类号： B01J31/00 , C08F4/06 , C08F4/44
CPC分类号： C08F210/02 , C07F7/003 , C07F7/0803 , C07F9/005 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F2500/17 , C08F2500/01 , C08F2500/03 , C08F236/06 , C08F210/06 , C08F4/64189 , C08F4/64048 , C08F4/7022 , C08F4/6812
摘要： The invention provides a process using olefin polymerization catalysts exhibiting excellent polymerization activities. The olefin polymerization catalysts of the invention contain a transition metal compound typified by formula (I) and at least one of an organometallic compound, an organoaluminum oxy-compound or a compound which reacts with said transition metal compound to form an ion pair. The process using the inventive catalysts is useful in producing α-olefin/conjugated diene copolymers having specific properties
摘要翻译：本发明提供一种使用显示优异聚合活性的烯烃聚合催化剂的方法。本发明的烯烃聚合催化剂含有式（I）代表的过渡金属化合物和有机金属化合物，有机铝氧化合物或与所述过渡金属化合物反应形成离子对的化合物中的至少一种。使用本发明催化剂的方法可用于制备具有特定性质的α-烯烃/共轭二烯共聚物

5. 发明授权

US06770723B2 &agr;-olefin/conjugated diene copolymers 有权
标题翻译： α-烯烃/共轭二烯共聚物
公开(公告)号：US06770723B2
公开(公告)日：2004-08-03
申请号：US09942636
申请日：2001-08-31
申请人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
发明人： Terunori Fujita , Yasushi Tohi , Makoto Mitani , Shigekazu Matsui , Junji Saito , Masatoshi Nitabaru , Kiyoaki Sugi , Haruyuki Makio , Toshiyuki Tsutsui
IPC分类号： C08F23604
CPC分类号： C08F210/02 , C07F7/003 , C07F7/0803 , C07F9/005 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F2500/17 , C08F2500/01 , C08F2500/03 , C08F236/06 , C08F210/06 , C08F4/64189 , C08F4/64048 , C08F4/7022 , C08F4/6812
摘要： The invention provides olefin polymerization catalyst exhibiting excellent polymerization activities, a process for olefin polymerization using the catalyst, a novel transition metal compound useful for the catalyst, and an &agr;-olefin/conjugated diene copolymer having specific properties. The olefin polymerization catalyst of the invention comprises (A) a transition metal compound of formula (I) or (II), and (B) an organometallic compound, an oranoaluminum oxy-compound or an ionizing ionic compound. The novel transition metal compound of the invention is a compound of formula (I) wherein M is a transition meal atom of Group 3 or 4 of the periodic table; m is an integer of 1 to 3; R1 is a hydrocarbon group, etc.; R2 to R5 are each H, a halogen, a hydrocarbon group, etc.; R6 is a halogen, a hydrocarbon group, etc.; n is a number satisfying a valence of M; and X is a halogen, a hydrocarbon group, etc.
摘要翻译：本发明提供了表现出优异聚合活性的烯烃聚合催化剂，使用该催化剂的烯烃聚合方法，用于催化剂的新型过渡金属化合物和具有特定性能的α-烯烃/共轭二烯共聚物。本发明的烯烃聚合催化剂包含（A）式（I）或（II）的过渡金属化合物和（B）有机金属化合物，或者是含有氧化铝的氧化合物或离子化离子化合物。本发明的新型过渡金属化合物是式（I）的化合物，其中M是周期表第3或4族的过渡膳食原子; m为1〜3的整数。 R 1是烃基等; R 2〜R 5各自为H，卤素，烃基等; R 6是卤素，烃基等; n是满足M价的数; X为卤素，烃基等

6. 发明授权

US06222072B1 Process for producing optically active amine 失效
标题翻译：光学活性胺的制备方法
公开(公告)号：US06222072B1
公开(公告)日：2001-04-24
申请号：US09186626
申请日：1998-11-06
申请人： Teruaki Mukaiyama , Kiyoaki Sugi , Takushi Nagata , Toru Yamada
发明人： Teruaki Mukaiyama , Kiyoaki Sugi , Takushi Nagata , Toru Yamada
IPC分类号： C07B5700
CPC分类号： B01J31/2243 , B01J31/1805 , B01J2231/643 , B01J2531/0252 , B01J2531/845 , C07B53/00 , C07B2200/07 , C07C209/52 , C07C303/40 , C07D217/04 , C07F9/36 , C07F9/65522 , C07C211/27 , C07C311/20
摘要： A novel process for producing an optically active amine is provided. The optically active amine is adapted for use as an intermediate in synthesizing physiologically active compounds such as pharmaceuticals and agricultural chemicals, as a functional material such as a liquid crystal, and as a starting material in synthesizing fine chemicals. The process comprises the step of reacting an imine with a hydride reagent in the presence of an optically active metal compound and an alcohol compound and/or carboxylic acid compound.
摘要翻译：提供了一种制备光学活性胺的新方法。光学活性胺适合用作合成诸如药物和农药之类的生理活性化合物的中间体，作为液晶等功能材料，以及作为合成精细化学品的原料。该方法包括在光学活性金属化合物和醇化合物和/或羧酸化合物的存在下使亚胺与氢化物试剂反应的步骤。

7. 发明授权

US5756790A Optically active cobalt (II) complexes and method for the preparation of optically active alcohols 失效
标题翻译：光学活性钴（II）配合物和制备光学活性醇的方法
公开(公告)号：US5756790A
公开(公告)日：1998-05-26
申请号：US722561
申请日：1996-09-27
申请人： Teruaki Mukaiyama , Kiyotaka Yorozu , Takushi Nagata , Toru Yamada , Kiyoaki Sugi
发明人： Teruaki Mukaiyama , Kiyotaka Yorozu , Takushi Nagata , Toru Yamada , Kiyoaki Sugi
IPC分类号： C07B53/00 , C07C29/143 , C07C67/31 , C07F15/06 , C07C29/14 , C07F7/00
CPC分类号： C07C29/143 , C07B53/00 , C07C67/31 , C12C11/02 , C07C2102/10
摘要： The invention provides a method for preparing an optically active alcohol comprising the step of reacting a ketone compound with a hydride reagent in the presence of an optically active metal compound. The resulting optically active alcohols are useful as intermediates for the synthesis of physiologically active compounds such as drugs and pesticides, functional materials such as liquid crystals, and raw materials for synthesis in fine chemistry. A novel optically active cobalt (II) complex useful as a catalyst is also provided.
摘要翻译：本发明提供一种制备光学活性醇的方法，其包括在光学活性金属化合物存在下使酮化合物与氢化物试剂反应的步骤。所得光学活性醇可用作合成药物和农药等生理活性化合物，液晶等功能材料和精细化学合成用原料的中间体。还提供了可用作催化剂的新型光学活性钴（II）络合物。

8. 发明授权

US5510511A Process for preparing N,O-dialkylhydroxylamine, its salts or intermediates in their synthesis 失效
标题翻译：在其合成中制备N，O-二烷基羟胺，其盐或中间体的方法
公开(公告)号：US5510511A
公开(公告)日：1996-04-23
申请号：US97225
申请日：1993-07-27
申请人： Satoshi Inoki , Mitsuyuki Takesue , Isao Hashimoto , Noriaki Kihara , Kiyoaki Sugi
发明人： Satoshi Inoki , Mitsuyuki Takesue , Isao Hashimoto , Noriaki Kihara , Kiyoaki Sugi
IPC分类号： C07C239/20 , C07C271/12 , C07C261/00
CPC分类号： C07C271/12 , C07C239/20
摘要： A process for preparing N,O-dialkylhydroxycarbamic acid ester which comprises reacting hydroxylamine or its salt with dihydrocarbyl carbonate in the presence of a basic compound to prepare hydroxycarbamic acid ester and subsequently alkylating this compound with an alkylating agent; a process for recovering N,O-dialkylhydroxycarbamic acid ester which comprises azeotropically distilling the ester with water from a solution containing the ester; a process for preparing N,O-dialkylhydroxylamine which comprises hydrolyzing N,O-dialkylhydroxycarbamic acid ester in an aqueous solution or a hydrous solvent in the presence of an alkali; a process for purifying N,O-dialkylhydroxylamine hydrochloride which comprises adding aldehyde or ketone to a solution of N,O-dialkylhydroxylamine hydrochloride containing O-alkylhydroxylamine hydrochloride as impurities to convert the O-alkylhydroxylamine hydrochloride into O-alkyl aldoxime or O-alkyl ketoxime and subsequently separating the N,O-dialkylhydroxylamine hydrochloride from the reaction system; and a process for separating N,O-dialkylhydroxylamine hydrochloride which comprises (i) adding benzene or alkylated benzene to an aqueous solution containing N,O-dialkylhydroxylamine hydrochloride, azeotropically removing water or a hydrochloride solution, and, subsequently (ii)adding alcohol thereto to obtain N,O-dialkylhydroxylamine hydrochloride in the form of crystal.
摘要翻译：一种制备N，O-二烷基羟基氨基甲酸酯的方法，其包括使羟胺或其盐与二烃基碳酸酯在碱性化合物的存在下反应以制备羟基氨基甲酸酯，随后用烷基化剂烷基化该化合物; 一种回收N，O-二烷基羟基氨基甲酸酯的方法，该方法包括从含有酯的溶液中用水共沸蒸馏该酯; 一种制备N，O-二烷基羟胺的方法，其包括在碱存在下水溶液或含水溶剂中N，O-二烷基羟基氨基甲酸酯水解; 一种纯化N，O-二烷基羟胺盐酸盐的方法，其包括将醛或酮加入到含有O-烷基羟胺盐酸盐的N，O-二烷基羟胺盐酸盐的溶液中作为杂质，以将O-烷基羟胺盐酸盐转化为O-烷基羟基肟或O-烷基酮肟随后从反应体系中分离出N，O-二烷基羟胺盐酸盐; 以及分离N，O-二烷基羟胺盐酸盐的方法，其包括（i）将苯或烷基化苯加入到含有N，O-二烷基羟胺盐酸盐的水溶液中，共沸除去水或盐酸盐溶液，随后（ii）向其中加入醇得到晶体形式的N，O-二烷基羟胺盐酸盐。

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