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1. 发明授权

US07741419B2 Process for producing olefin polymers 有权
标题翻译：生产烯烃聚合物的方法
公开(公告)号：US07741419B2
公开(公告)日：2010-06-22
申请号：US10550021
申请日：2005-03-30
申请人： Yasushi Tohi , Kenji Sugimura , Toshiyuki Tsutsui
发明人： Yasushi Tohi , Kenji Sugimura , Toshiyuki Tsutsui
IPC分类号： C08F4/642 , C08F4/6592 , B01J31/22
CPC分类号： C08F10/00 , C08F4/65912 , Y10S526/943 , C08F4/65927 , C08F2/06 , C08F210/16 , C08F210/14 , C08F2500/12 , C08F2500/08
摘要： A process for producing an olefin polymer is provided, in which ethylene and at least one kind or more of monomers selected from α-olefins are polymerized by a high temperature solution polymerization in a temperature range between 120 and 300° C., in the presence of an olefin polymerization catalyst composed of a bridged metallocene compound represented by general formula [I] described below and at least one kind or more compounds (B) selected from (b-1) an organoaluminum oxy-compound, (b-2) a compound capable of forming an ion pair in a reaction with the bridged metallocene compound mentioned above, and (b-3) an organoaluminum compound. According to the high temperature solution polymerization of the present invention, it has become possible to obtain a polymer having a high molecular weight with high polymerization activity that was so far unattainable, and when the polymer is a copolymer, it is a process for producing a high molecular weight olefin polymer with a large comonomer content, a narrow composition distribution, and a narrow molecular weight distribution.
摘要翻译：提供了一种制备烯烃聚合物的方法，其中乙烯和至少一种或多种选自α-烯烃的单体通过高温溶液聚合在120-300℃的温度范围内聚合，的由下述通式[I]表示的桥连金属茂化合物和至少一种以上选自（b-1）有机铝氧化合物，（b-2）a 能够与上述桥连茂金属化合物反应形成离子对的化合物和（b-3）有机铝化合物。根据本发明的高温溶液聚合，可以获得迄今为止无法实现的具有高聚合活性的高分子量聚合物，并且当聚合物是共聚物时，它是制备具有大的共聚单体含量的高分子量烯烃聚合物，组成分布窄，分子量分布窄。

2. 发明授权

US07563849B2 Ethylene (co) polymer and its use 有权
标题翻译：乙烯（共）聚合物及其用途
公开(公告)号：US07563849B2
公开(公告)日：2009-07-21
申请号：US11211845
申请日：2005-08-26
申请人： Mamoru Takahashi , Tetsuji Kasai , Junji Saito , Naoto Matsukawa , Kazutaka Tsuru , Makoto Mitani , Terunori Fujita , Shiro Otsuzuki , Tetsuhiro Matsumoto , Toshiyuki Tsutsui
发明人： Mamoru Takahashi , Tetsuji Kasai , Junji Saito , Naoto Matsukawa , Kazutaka Tsuru , Makoto Mitani , Terunori Fujita , Shiro Otsuzuki , Tetsuhiro Matsumoto , Toshiyuki Tsutsui
IPC分类号： C08F267/04
CPC分类号： C08F255/02 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , C08L23/04 , C08L23/0815 , C08L2205/02 , C08L2205/025 , C08F4/64048 , C08L2666/04 , C08F2500/10 , C08F2500/17 , C08F2500/12 , C08F2500/03 , C08F2500/07 , C08F2500/11 , C08F2500/14 , C08F210/14 , C08F210/08
摘要： An ethylene (co)polymer of the present invention is a (co)polymer with excellent moldability and mechanical properties and either an ethylene homopolymer or a copolymer of ethylene and an α-olefin of 4 to 20 carbon atoms. The (co)polymer has methyl branches measured by 13C-NMR less than 0.1 in number per 1,000 carbon atoms and Mw/Mn measured by GPC not lower than 1.8 and lower than 4.5. The (co)polymer is either an ethylene homopolymer or a copolymer of ethylene and an α-olefin of 3 to 20 carbon atoms. The melt tension (MT) and the swell ratio (SR) satisfy the relation; log(MT)>12.9−7.15×SR; and the intrinsic viscosity ([η]) and the melt flow rate (MFR) satisfy the relation; [η]>1.85×MFR−0.192 in the case of MFR 1.85×MFR−0.213 in the case of MFR≧1. Such an ethylene (co)polymer can be usable for various molding applications and especially suitable for pipes.
摘要翻译：本发明的乙烯（共）聚合物是具有优异的成型性和机械性能（乙烯均聚物或乙烯与4-20个碳原子的α-烯烃的共聚物）的（共）聚合物。（共）聚合物具有通过13 C-NMR测量的甲基支链，每1000个碳原子数小于0.1，GPC测得的Mw / Mn不低于1.8，低于4.5。（共）聚合物是乙烯均聚物或乙烯与3-20个碳原子的α-烯烃的共聚物。熔体张力（MT）和溶胀比（SR）满足关系; log（MT）> 12.9-7.15xSR; 特性粘度（η）和熔体流动速率（MFR）满足关系; 在MFR <1的情况下，η> 1.85×MFR-0.192和关系; 在MFR> = 1的情况下，η> 1.85×MFR-0.213。这种乙烯（共）聚合物可用于各种模塑应用，特别适用于管道。

3. 发明申请

US20090069515A1 Solid Titanium Catalyst Component, Catalyst for Polymerization of Olefin and Process for Producing Olefin Polymer 审中-公开
标题翻译：固体钛催化剂组分，烯烃聚合催化剂和生产烯烃聚合物的方法
公开(公告)号：US20090069515A1
公开(公告)日：2009-03-12
申请号：US11795504
申请日：2006-01-19
申请人： Kazuhisa Matsunaga , Hisao Hashida , Toshiyuki Tsutsui , Kunio Yamamoto , Atsushi Shibahara , Tetsunori Shinozaki
发明人： Kazuhisa Matsunaga , Hisao Hashida , Toshiyuki Tsutsui , Kunio Yamamoto , Atsushi Shibahara , Tetsunori Shinozaki
IPC分类号： C08F4/76 , B01J31/04
CPC分类号： B01J31/0209 , B01J31/0212 , B01J31/128 , B01J31/143 , B01J31/38 , C08F10/00 , C08F110/06 , C08F110/08 , C08F110/14 , C08F210/06 , C08F4/6543 , C08F4/651 , C08F2500/04 , C08F2500/18 , C08F210/16 , C08F4/6465
摘要： A solid titanium catalyst component (I) of the present invention is characterized in that it contains titanium, magnesium, halogen, and a cyclic ester compound (a) represented by the following formula (1): wherein n is an integer of 5 to 10; R2 and R3 are each independently COOR1 or R, and at least one of R2 and R3 is COOR1; a single bond (excluding Ca—Ca bonds, and a Ca—Cb bond in the case where R3 is R) in the cyclic backbone may be replaced with a double bond; a plurality of R1's are each independently a monovalent hydrocarbon group having 1 to 20 carbon atoms; and a plurality of R's are each independently a hydrogen atom or a substituent, but at least one of R's is not a hydrogen atom. When using this solid titanium catalyst component (I), an olefin polymer having a broad molecular weight distribution can be produced.
摘要翻译：本发明的固体钛催化剂组分（I）的特征在于它含有钛，镁，卤素和由下式（1）表示的环酯化合物（a）：其中n是5至10的整数 ; R2和R3各自独立地是COOR1或R，R2和R3中的至少一个是COOR1; 环状骨架中的单键（不包括Ca-Ca键，在R3为R的情况下为Ca-Cb键）可以被双键取代; 多个R 1各自独立地为具有1〜20个碳原子的一价烃基; 并且多个R各自独立地为氢原子或取代基，但R中的至少一个不是氢原子。当使用该固体钛催化剂组分（I）时，可以生产具有宽分子量分布的烯烃聚合物。

4. 发明授权

US07220696B2 Solid titanium catalyst component for olefin polymerization, catalyst for olefin polymerization, and process for olefin polymerization 有权
标题翻译：用于烯烃聚合的固体钛催化剂组分，用于烯烃聚合的催化剂和烯烃聚合方法
公开(公告)号：US07220696B2
公开(公告)日：2007-05-22
申请号：US10501888
申请日：2003-04-03
申请人： Kazuhisa Matsunaga , Masao Nagano , Masaaki Ohgizawa , Toshiyuki Tsutsui
发明人： Kazuhisa Matsunaga , Masao Nagano , Masaaki Ohgizawa , Toshiyuki Tsutsui
IPC分类号： B01J31/00
CPC分类号： C08F110/06 , C08F10/00 , C08F4/6492 , C08F4/651 , C08F4/6545 , C08F2500/18 , C08F2500/15 , C08F2500/12
摘要： Disclosed is a catalyst for olefin polymerization comprising [I] a solid titanium catalyst component [S] comprising titanium, magnesium, halogen and an electron donor (b), which is obtained by bringing a solid adduct consisting of a magnesium compound and an electron donor (a) into contact with an electron donor (b) and a liquid titanium compound by at least one method selected from (A) a method of contacting the materials in a suspended state in the coexistence of an inert hydrocarbon solvent and (B) a method of contacting the material plural times individed portions and [II] an organometallic compound catalyst component [M] containing a metal selected from the groups I to III in the periodic table.
摘要翻译：公开了一种用于烯烃聚合的催化剂，其包含[I]包含钛，镁，卤素和电子给体（b）的固体钛催化剂组分[S]，其通过使由镁化合物和电子给体（a）通过选自以下的至少一种方法与电子给体（b）和液体钛化合物接触：（A）在惰性烃溶剂共存下使悬浮状态的材料接触的方法和（B）将该材料多次接触的方法和[II]含有选自元素周期表中I〜III族的金属的有机金属化合物催化剂组分[M]。

5. 发明申请

US20060226220A1 Sales office system 审中-公开
标题翻译：销售办公系统
公开(公告)号：US20060226220A1
公开(公告)日：2006-10-12
申请号：US11271769
申请日：2005-11-14
申请人： Atsushi Hasegawa , Akihito Itou , Masahiro Abe , Kazuma Kurata , Masataka Itakura , Toshiyuki Tsutsui , Takeshi Minemoto
发明人： Atsushi Hasegawa , Akihito Itou , Masahiro Abe , Kazuma Kurata , Masataka Itakura , Toshiyuki Tsutsui , Takeshi Minemoto
IPC分类号： G06K15/00
CPC分类号： G06Q30/06
摘要： A sales office system acquires information about a customer's attention to financial commodities without demanding special operations from the customer and provides effective information matching the acquired customer's attention. In the sales office system that connects with plural information processors via networks, a sales office system server includes a part that cooperates with an Internet banking server, a part that cooperates with a customer management server, a part that acquires dealing statuses, a part that acquires consultation reservation information, a part that acquires commodity information, a part that determines valuable information by valuable information criteria, and a part that holds customers' operation histories, and effective sales are performed for customers by flexibly and effectively using information about purchasers of a variety of commodities.
摘要翻译：销售办公系统从客户那里获取关于顾客关注金融商品的信息，而不需要客户的特殊操作，并提供与获取的客户关注的有效信息。在通过网络与多个信息处理器连接的销售处系统中，销售处系统服务器包括与网上银行服务器协作的部分，与客户管理服务器协作的部分，获取交易状态的部分，获取咨询预约信息，获取商品信息的部分，通过有价值信息标准确定有价值信息的部分，以及持有客户运营历史的部分，并且通过灵活有效地使用关于购买者的购买者的信息来为客户执行有效销售各种商品。

6. 发明申请

US20060097045A1 Sales shop system 有权
标题翻译：销售店系统
公开(公告)号：US20060097045A1
公开(公告)日：2006-05-11
申请号：US11259260
申请日：2005-10-27
申请人： Toshiyuki Tsutsui , Masataka Itakura , Tomohiro Hamada , Akihito Itou , Kazuma Kurata
发明人： Toshiyuki Tsutsui , Masataka Itakura , Tomohiro Hamada , Akihito Itou , Kazuma Kurata
IPC分类号： G06K15/00 , G07F19/00
CPC分类号： G06Q20/40 , G06Q20/4014 , G06Q20/40145 , G06Q30/02
摘要： Conventionally, to acquire specific information of a customer, acquisition of the information is only possible by using information such as a bank account number owned by the customer, and further it is not possible to present information beneficial to the customer unless information owned by the customer is acquired from the customer. More specifically, there is a problem in that much time is necessary for a customer or a system operator to input such information. To solve the above-stated problem, the present invention outputs information associated with a customer by using biometric information including a face image. More specifically, biometric information is acquired from a user of a first terminal unit included in a plurality of terminal units, and information associated with an operation made by the user is identified. Then, when the user is going to use a second terminal unit (or when the second terminal unit executes processing of information on the user based on inputs by a third party, etc.), biometric information is acquired from the user, and information that is identified by an operation made on the first terminal unit is retrieved for output by using the biometric information.
摘要翻译：通常，为了获取客户的具体信息，只能通过使用客户拥有的银行帐号等信息来获取信息，而且除了客户所拥有的信息之外，还不可能提供有益于客户的信息是从客户那里获得的。更具体地说，存在客户或系统操作员输入这样的信息需要很多时间的问题。为了解决上述问题，本发明通过使用包括脸部图像的生物信息来输出与顾客相关联的信息。更具体地，从包括在多个终端单元中的第一终端单元的用户获取生物特征信息，并且识别与由用户进行的操作相关联的信息。然后，当用户要使用第二终端单元（或者当第二终端单元基于第三方的输入来执行对用户的信息的处理等）时，从用户获取生物特征信息，以及信息通过在第一终端单元上进行的操作来识别，通过使用生物特征信息被检索以输出。

7. 发明授权

US06444603B1 CATALYST COMPONENT FOR ETHYLENICALLY UNSATURATED MONOMER POLYMERIZATION, CATALYST FOR ETHYLENICALLY UNSATURATED MONOMER POLYMERIZATION, AND PROCESS FOR ETHYLENICALLY UNSATURATED MONOMER POLYMERIZATION USING SAID CATALYST 有权
标题翻译：用于乙烯不饱和单体聚合的催化剂组分，用于乙烯单体不饱和单体聚合的催化剂，以及使用所述催化剂进行乙烯单体不饱和单体聚合的方法
公开(公告)号：US06444603B1
公开(公告)日：2002-09-03
申请号：US09216481
申请日：1998-12-21
申请人： Yasushi Tohi , Haruyuki Makio , Terunori Fujita , Toshiyuki Tsutsui
发明人： Yasushi Tohi , Haruyuki Makio , Terunori Fujita , Toshiyuki Tsutsui
IPC分类号： B01J3100
CPC分类号： C08F10/00 , C08F4/65927 , C08F110/02 , C08F4/64072 , C08F4/65912 , C08F2500/17 , C08F4/64048 , C08F4/64079 , C08F4/64186 , C08F4/64068 , C08F4/7006 , C08F4/7027
摘要： The invention relates to a catalyst component which can provide, in combination with a transition metal compound, a catalyst for ethylenically unsaturated monomer polymerization, a catalyst comprising the catalyst component and a transition metal compound, and a process for ethylenically unsaturated monomer polymerization using the catalyst. The catalyst component comprises a compound obtained by the reaction of, in any order, (i) a compound comprising a metal of Group 13 of the periodic table; (ii) a compound capable of reacting with the compound (i) to be bonded to two or more of the Group 13 metal; (iii) a compound capable of reacting the compound (i); and optionally (iv) a hydrocarbon compound or the like.
摘要翻译：本发明涉及一种催化剂组分，其可与过渡金属化合物，烯键式不饱和单体聚合催化剂，含催化剂组分和过渡金属化合物的催化剂和使用该催化剂的烯键式不饱和单体聚合方法。催化剂组分包括通过以任何顺序反应获得的化合物，（i）包含周期表第13族金属的化合物; （ii）能够与要与第13族金属中的两种以上结合的化合物（i）反应的化合物; （iii）能够使化合物（i）反应的化合物; 和（iv）烃化合物等。

8. 发明授权

US06333387B1 Ethylene copolymer composition 有权
标题翻译：乙烯共聚物组成
公开(公告)号：US06333387B1
公开(公告)日：2001-12-25
申请号：US09703665
申请日：2000-11-02
申请人： Mamoru Takahashi , Seiichi Ikeyama , Akira Todo , Toshiyuki Tsutsui , Seiji Ohta , Hajime Inagaki
发明人： Mamoru Takahashi , Seiichi Ikeyama , Akira Todo , Toshiyuki Tsutsui , Seiji Ohta , Hajime Inagaki
IPC分类号： C08L2308
CPC分类号： C08L23/0815 , C08F10/02 , C08F110/02 , C08F210/16 , C08F210/18 , C08L23/06 , C08L23/10 , C08L23/12 , C08L23/14 , C08L23/16 , C08L23/20 , C08L23/22 , C08L51/06 , C08L2205/02 , Y10S526/943 , C08F2/00 , C08L2666/24 , C08L2666/06 , C08F2500/12 , C08F2500/11 , C08F2500/08 , C08F210/14 , C08F210/08 , C08F232/00 , C08F2500/25 , C08L2666/04
摘要： Ethylene/&agr;-olefin copolymer with olefin type elastomer, each having particular properties, including density and melt flow rate, with a density ratio of elastomer to copolymer of less than 1, provide compostions which have excellent moldability and form films having high mechanical strength.
摘要翻译：具有烯烃类弹性体的乙烯/α-烯烃共聚物各自具有特定的性能，包括密度和熔体流动速率，弹性体与共聚物的密度比小于1，提供了具有优异成型性和具有高机械强度的成型膜的组合物。

9. 发明授权

US6043325A Process for olefin polymerization 失效
标题翻译：烯烃聚合方法
公开(公告)号：US6043325A
公开(公告)日：2000-03-28
申请号：US978602
申请日：1997-11-26
申请人： Toshiyuki Tsutsui , Ken Yoshitsugu , Masaaki Ohgizawa , Tetsuhiro Matsumoto , Junichi Imuta
发明人： Toshiyuki Tsutsui , Ken Yoshitsugu , Masaaki Ohgizawa , Tetsuhiro Matsumoto , Junichi Imuta
IPC分类号： C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F210/16 , C08F4/64
CPC分类号： C08F10/00 , C08F210/16 , C08F4/65912 , C08F4/65916 , C08F4/6592 , Y10S526/904 , Y10S526/943
摘要： A process for olefin polymerization, including polymerizing or copolymerizing an olefin in the presence of an olefin polymerization catalyst composed of: a fine particle carrier; (A) a transition metal compound of a Group IVB metal of the periodic table, containing a ligand having a cyclopentadienyl skeleton; (B) an aluminoxane compound; and optionally (C) an organoaluminum compound, wherein said aluminoxane compound has an alkyl groups to aluminum ratio of 1.3 to 2.1; said transition metal compound (A) and said organoaluminum oxy-compound (B) and said organoaluminum compound being supported on the fine particle carrier; and said solid catalyst having a bulk density of 0.3 g/cm.sup.3 to 0.5 g/cm.sup.3 and a fluidity index of 45 to 70 and an olefin polymerization process using the olefin polymerization catalyst; and an olefin prepolymerized catalyst obtained by prepolymerizing the catalyst, and an olefin polymerization process using the olefin prepolymerized catalyst. The olefin polymerization process produces a polymer showing excellent particle properties and an olefin polymer which does not stick to the wall of the polymerization reactor.
摘要翻译：一种烯烃聚合方法，包括在烯烃聚合催化剂存在下聚合或共聚烯烃，所述烯烃聚合催化剂由微粒载体构成; （A）周期表第ⅣB族金属的过渡金属化合物，其含有具有环戊二烯基骨架的配位体; （B）铝氧烷化合物; 和任选地（C）有机铝化合物，其中所述铝氧烷化合物具有1.3至2.1的烷基与铝的比率; 所述过渡金属化合物（A）和所述有机铝氧化合物（B）和所述有机铝化合物负载在所述微粒载体上; 所述固体催化剂的体积密度为0.3g / cm 3〜0.5g / cm 3，流动性指数为45〜70，使用该烯烃聚合催化剂的烯烃聚合方法; 和通过使催化剂预聚合获得的烯烃预聚合催化剂和使用烯烃预聚合催化剂的烯烃聚合方法。烯烃聚合方法产生显示出优异的颗粒性能的聚合物和不粘在聚合反应器壁上的烯烃聚合物。

10. 发明授权

US5880056A Olefin polymerization catalyst and process for olefin polymerization 失效
标题翻译：烯烃聚合催化剂和烯烃聚合方法
公开(公告)号：US5880056A
公开(公告)日：1999-03-09
申请号：US954073
申请日：1997-10-20
申请人： Toshiyuki Tsutsui , Masaaki Ohgizawa
发明人： Toshiyuki Tsutsui , Masaaki Ohgizawa
IPC分类号： C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F210/16 , B01J31/00 , B01J37/00 , C08F4/02 , C08F4/60
CPC分类号： C08F10/00 , C08F210/16 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/65925 , Y10S526/943
摘要： Disclosed is an olefin polymerization catalyst comprising (A) a transition metal compound represented by the formula (I) R.sup.1 R.sup.2 MX.sub.2 (wherein M is a transition metal atom, R.sup.1 and R.sup.2 are each a cycloalkadienyl group having an aryl group and a saturated hydrocarbon group as substituents, and X is a halogen atom or the like) and (B) at least one compound selected from (b1) an organoaluminum oxy-compound, (b2) an ionized ionic compound and (b3) an organoaluminum compound. Also disclosed is a process for olefin polymerization comprising polymerizing an olefin in the presence of the above-mentioned catalyst. According to the present invention, an olefin copolymer having a crystallization temperature and a melting point both lower than those of the conventional copolymers can be prepared in the case of that the feeding amount of comonomer is smaller than those conventionally used.
摘要翻译：公开了一种烯烃聚合催化剂，其包含（A）由式（I）表示的过渡金属化合物R 1 R 2 MX 2（其中M是过渡金属原子，R 1和R 2各自是具有芳基和饱和烃基作为取代基的环二烯基 X为卤原子等）和（B）选自（b1）有机铝氧化合物，（b2）离子化离子化合物和（b3）有机铝化合物中的至少一种化合物。还公开了一种烯烃聚合方法，包括在上述催化剂存在下使烯烃聚合。根据本发明，在共聚单体的进料量小于常规使用的情况下，可以制备具有低于常规共聚物的结晶温度和熔点的烯烃共聚物。

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