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1. 发明申请

US20150126675A1 Polydienes And Diene Copolymers Having Organophosphine Functionality 有权
标题翻译：具有有机膦功能的聚二烯和二烯共聚物
公开(公告)号：US20150126675A1
公开(公告)日：2015-05-07
申请号：US14398644
申请日：2013-05-01
申请人： Terrence E. Hogan , William l. Hergenrother , David M. Roggeman , Bridgestone Corporation
发明人： Terrence E. Hogan , William L. Hergenrother , David M. Roggeman
IPC分类号： C08F236/06 , C08K3/36 , C08K3/04
CPC分类号： C08F236/06 , C08F230/02 , C08F236/04 , C08K3/04 , C08K3/36 , C08L43/02
摘要： Embodiments provide polydienes and diene copolymers having organophosphines functionality. Specific embodiments employ phosphorus-containing organometal initiators and copolymers prepared by anionically polymerizing conjugated diene monomer and vinyl organophosphine.
摘要翻译：实施方案提供具有有机膦功能性的聚二烯和二烯共聚物。具体实施方案使用含磷有机金属引发剂和通过阴离子聚合共轭二烯单体和乙烯基有机膦制备的共聚物。

2. 发明授权

US09868805B2 Polydienes and diene copolymers having organophosphine functionality 有权
公开(公告)号：US09868805B2
公开(公告)日：2018-01-16
申请号：US14398644
申请日：2013-05-01
申请人： Bridgestone Corporation , Terrence E. Hogan , William L. Hergenrother , David M. Roggeman
发明人： Terrence E. Hogan , William L. Hergenrother , David M. Roggeman
IPC分类号： C08F130/02 , C08F236/06 , C08F236/04 , C08K3/04 , C08K3/36 , C08F230/02
CPC分类号： C08F236/06 , C08F230/02 , C08F236/04 , C08K3/04 , C08K3/36 , C08L43/02
摘要： Embodiments provide polydienes and diene copolymers having organophosphines functionality. Specific embodiments employ phosphorus-containing organometal initiators and copolymers prepared by anionically polymerizing conjugated diene monomer and vinyl organophosphine.

3. 发明授权

US09884923B2 Aminosilane initiators and functionalized polymers prepared therefrom 有权
公开(公告)号：US09884923B2
公开(公告)日：2018-02-06
申请号：US13519603
申请日：2010-12-30
申请人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
发明人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
IPC分类号： C08F4/48 , C08F4/58 , C08F4/618 , C07F7/10 , C08F236/10 , C08F136/06 , C08L9/06 , B60C1/00 , C08F297/02 , C08F297/04 , C08F290/04 , C08F212/08
CPC分类号： C08F4/486 , B60C1/00 , B60C1/0008 , B60C1/0016 , B60C1/0025 , B60C2001/0033 , B60C2001/005 , B60C2001/0058 , B60C2001/0066 , B60C2001/0075 , B60C2001/0083 , B60C2001/0091 , C07F7/10 , C08F4/48 , C08F4/58 , C08F4/6185 , C08F4/6186 , C08F136/06 , C08F212/08 , C08F236/10 , C08F290/044 , C08F290/048 , C08F297/02 , C08F297/04 , C08F297/042 , C08F297/044 , C08K3/06 , C08K3/22 , C08K3/36 , C08K5/09 , C08L7/00 , C08L9/06 , C08L91/00 , C08L91/06 , Y02T10/862
摘要： Metallated aminosilane compounds for use as functional initiators in anionic polymerizations and processes for producing an aminosilane-functionalized polymer using the metallated aminosilane compounds to initiate anionic polymerization of at least one type of anionically polymerizable monomer. Preferred use of the metallated aminosilane compounds results in rubber compositions for use in tires comprising an aminosilane functionalized polymer.

4. 发明授权

US08916665B2 Aminosilane initiators and functionalized polymers prepared therefrom 有权
标题翻译：氨基硅烷引发剂和由其制备的官能化聚合物
公开(公告)号：US08916665B2
公开(公告)日：2014-12-23
申请号：US13977296
申请日：2011-06-22
申请人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
发明人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
IPC分类号： C08F4/58 , C08C19/44 , C08F36/06 , C08F36/04 , C08F4/48 , C08L19/00 , C08L15/00 , B60C1/00
CPC分类号： C08C19/25 , B60C1/00 , C08C19/22 , C08C19/44 , C08F4/48 , C08F8/42 , C08F36/04 , C08F36/06 , C08F236/10 , C08L15/00 , C08L19/006 , Y02T10/862
摘要： Metallated aminosilane compounds for use as functional initiators in anionic polymerizations and processes for producing an aminosilane-functionalized polymer using the metallated aminosilane compounds to initiate anionic polymerization of at least one type of anionically polymerizable monomer. Preferred use of the metallated aminosilane compounds results in rubber compositions for use in tires comprising an aminosilane functionalized polymer. A telechelic polymer may result from use of the metallated aminosilane compound as a functional terminator.
摘要翻译：用于阴离子聚合中的官能引发剂的金属化氨基硅烷化合物和使用金属化氨基硅烷化合物制备氨基硅烷官能化聚合物以引发至少一种类型的阴离子聚合单体的阴离子聚合的方法。优选使用金属化的氨基硅烷化合物产生用于包含氨基硅烷官能化聚合物的轮胎的橡胶组合物。使用金属化氨基硅烷化合物作为功能性终止剂可产生遥爪聚合物。

5. 发明申请

US20130281645A1 Aminosilane Initiators And Functionalized Polymers Prepared Therefrom 有权
标题翻译：氨基硅烷引发剂和官能化聚合物
公开(公告)号：US20130281645A1
公开(公告)日：2013-10-24
申请号：US13977296
申请日：2011-06-22
申请人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
发明人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
IPC分类号： C08F36/06
CPC分类号： C08C19/25 , B60C1/00 , C08C19/22 , C08C19/44 , C08F4/48 , C08F8/42 , C08F36/04 , C08F36/06 , C08F236/10 , C08L15/00 , C08L19/006 , Y02T10/862
摘要： Metallated aminosilane compounds for use as functional initiators in anionic polymerizations and processes for producing an aminosilane-functionalized polymer using the metallated aminosilane compounds to initiate anionic polymerization of at least one type of anionically polymerizable monomer. Preferred use of the metallated aminosilane compounds results in rubber compositions for use in tires comprising an aminosilane functionalized polymer. A telechelic polymer may result from use of the metallated aminosilane compound as a functional terminator.
摘要翻译：用于阴离子聚合中的官能引发剂的金属化氨基硅烷化合物和使用金属化氨基硅烷化合物制备氨基硅烷官能化聚合物以引发至少一种类型的阴离子聚合单体的阴离子聚合的方法。优选使用金属化的氨基硅烷化合物产生用于包含氨基硅烷官能化聚合物的轮胎的橡胶组合物。使用金属化氨基硅烷化合物作为功能性终止剂可产生遥爪聚合物。

6. 发明申请

US20130066008A1 AMINOSILANE INITIATORS AND FUNCTIONALIZED POLYMERS PREPARED THEREFROM 有权
标题翻译：氨基甲酸酯起始剂和官能化聚合物
公开(公告)号：US20130066008A1
公开(公告)日：2013-03-14
申请号：US13519603
申请日：2010-12-30
申请人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
发明人： David F. Lawson , Terrence E. Hogan , Christine Rademacher , David M. Roggeman , Fuminori Ota
IPC分类号： C08F236/06 , C08L9/06 , C08K3/36 , C08F236/10 , C08L9/00 , C07F7/10
CPC分类号： C08F4/486 , B60C1/00 , B60C1/0008 , B60C1/0016 , B60C1/0025 , B60C2001/0033 , B60C2001/005 , B60C2001/0058 , B60C2001/0066 , B60C2001/0075 , B60C2001/0083 , B60C2001/0091 , C07F7/10 , C08F4/48 , C08F4/58 , C08F4/6185 , C08F4/6186 , C08F136/06 , C08F212/08 , C08F236/10 , C08F290/044 , C08F290/048 , C08F297/02 , C08F297/04 , C08F297/042 , C08F297/044 , C08K3/06 , C08K3/22 , C08K3/36 , C08K5/09 , C08L7/00 , C08L9/06 , C08L91/00 , C08L91/06 , Y02T10/862
摘要： Metallated aminosilane compounds for use as functional initiators in anionic polymerizations and processes for producing an aminosilane-functionalized polymer using the metallated aminosilane compounds to initiate anionic polymerization of at least one type of anionically polymerizable monomer. Preferred use of the metallated aminosilane compounds results in rubber compositions for use in tires comprising an aminosilane functionalized polymer.
摘要翻译：用于阴离子聚合中的官能引发剂的金属化氨基硅烷化合物和使用金属化氨基硅烷化合物制备氨基硅烷官能化聚合物以引发至少一种类型的阴离子聚合单体的阴离子聚合的方法。优选使用金属化的氨基硅烷化合物产生用于包含氨基硅烷官能化聚合物的轮胎的橡胶组合物。

7. 发明授权

US08822620B2 Method for making alkoxy-modified silsesquioxanes 有权
标题翻译：制备烷氧基改性倍半硅氧烷的方法
公开(公告)号：US08822620B2
公开(公告)日：2014-09-02
申请号：US13030611
申请日：2011-02-18
申请人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： C08G77/08
CPC分类号： C08G77/08 , B60C1/00 , C08G77/18 , C08G77/28 , C08K3/013 , C08L9/00 , C08L21/00 , C08L83/06 , C08L83/08 , Y02P20/584 , C08L83/00
摘要： A method is presented for making alkoxy-modified silsesquioxanes (AMS) or co-alkoxy-modified silsesquioxanes (co-AMS,) comprising the steps of (a) combining as a reaction mixture (i) water, (ii) an acid-stable solvent for the water, (iii) a solid strong cationic hydrolysis and condensation catalyst, and (iv) a trialkoxysilane compound, (b) allowing the reaction mixture to react for about 0.5 hours to about 200 hours to form the alkoxy-modified silsesquioxanes; and (c) recovering the alkoxy-modified silsesquioxanes from the reaction mixture. The use of solid strong cationic catalysts in this reaction system is advantageous because they remain as solids throughout the reaction, allowing simplified separation of the solid catalyst from the soluble AMS or co-AMS products, resulting in total or near total recovery of the AMS or co-AMS products, the products being free of, or substantially free of residual acid catalyst, as well as virtual total recovery of the catalyst for recycling. The improved AMS and co-AMS compounds, vulcanizable rubber compounds containing them, and a pneumatic tire having a component made from the vulcanized rubber compounds are also presented.
摘要翻译：提出了制备烷氧基改性倍半硅氧烷（AMS）或共 - 烷氧基改性倍半硅氧烷（co-AMS）的方法，该方法包括以下步骤：（a）将反应混合物（i）和（ii）酸稳定溶剂，（iii）固体强阳离子水解和缩合催化剂，和（iv）三烷氧基硅烷化合物，（b）使反应混合物反应约0.5小时至约200小时以形成烷氧基改性倍半硅氧烷; 和（c）从反应混合物中回收烷氧基改性的倍半硅氧烷。在该反应系统中使用固体强阳离子催化剂是有利的，因为它们在整个反应中保持固体，允许固体催化剂与可溶性AMS或共AMS产物的简单分离，导致AMS或共AMS产品，产品没有或基本上没有残留的酸催化剂，以及用于再循环的催化剂的虚拟总回收。还提出了改进的AMS和共AMS化合物，含有它们的可硫化橡胶化合物和具有由硫化橡胶化合物制成的组分的充气轮胎。

8. 发明授权

US08513371B2 Amino alkoxy-modified silsesquioxanes and method of preparation 有权
标题翻译：氨基烷氧基改性倍半硅氧烷及其制备方法
公开(公告)号：US08513371B2
公开(公告)日：2013-08-20
申请号：US12346994
申请日：2008-12-31
申请人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
发明人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
IPC分类号： C08G77/26
CPC分类号： C08K5/544 , C08G77/26 , C08G77/28 , C08K5/548 , C09D183/08 , Y02T10/862 , Y10T152/10 , Y10T152/10495 , Y10T428/2991 , Y10T428/2995
摘要： An amino alkoxy-modified silsesquioxane (AMS) comprising one or more compounds selected from the group consisting of an amino AMS, an amino/mercaptan co-AMS, an amino/blocked mercaptan co-AMS, mixtures thereof, and a weak acid-neutralized solid or aqueous solution thereof, and a method of making the amino AMS, are presented. The compounds are useful in compounding, processing, cure and storage of silica-reinforced rubbers because they contain low levels of volatile organic compounds (VOC).
摘要翻译：包含一种或多种选自氨基AMS，氨基/硫醇共-AMS，氨基/封端的硫醇共-AMS，及其混合物和弱酸中和的氨基烷氧基改性倍半硅氧烷（AMS）提供其固体或水溶液，以及制备氨基AMS的方法。该化合物可用于二氧化硅增强橡胶的混合，加工，固化和储存，因为它们含有低水平的挥发性有机化合物（VOC）。

9. 发明申请

US20080308204A1 FUNCTIONAL POLYMERS PREPARED WITH SULFUR-CONTAINING INITIATORS 有权
标题翻译：功能性聚合物与含硫装置的制备
公开(公告)号：US20080308204A1
公开(公告)日：2008-12-18
申请号：US12139567
申请日：2008-06-16
申请人： Terrence E. Hogan , William L. Hergenrother
发明人： Terrence E. Hogan , William L. Hergenrother
IPC分类号： B60C1/00 , C07C321/14
CPC分类号： B60C1/0016 , B60C1/00 , B60C1/0025 , C08F36/04 , C08L19/006 , C08F4/48
摘要： A method for forming a polymer including a sulfur-containing functional group, the method comprising introducing a sulfur-containing initiator defined by the formula with conjugated diene monomer and optionally copolymerizable monomer within a polymerization medium and allowing the sulfur-containing initiator to initiate the polymerization of the conjugated diene monomer and the optional copolymerizable monomer, where R1 is a monovalent organic group, R2 is a divalent organic group, R3 is a divalent organic group or a bond, and a is an integer from 1 to about 5.
摘要翻译：一种形成含有含硫官能团的聚合物的方法，所述方法包括将由式表示的含硫起始物与共轭二烯单体和任选的可共聚单体引入聚合介质中，并允许含硫引发剂引发聚合的共轭二烯单体和任选的可共聚单体，其中R 1为一价有机基团，R 2为二价有机基团，R 3为二价有机基团或键，a为1至约5的整数。

10. 发明申请

US20080293858A1 METHOD FOR MAKING ALKOXY-MODIFIED SILSESQUIOXANES 有权
标题翻译：制备改性硅烷氧基硅烷的方法
公开(公告)号：US20080293858A1
公开(公告)日：2008-11-27
申请号：US11752715
申请日：2007-05-23
申请人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： B60C1/00 , C07F7/00
CPC分类号： C08G77/08 , B60C1/00 , C08G77/18 , C08G77/28 , C08K3/013 , C08L9/00 , C08L21/00 , C08L83/06 , C08L83/08 , Y02P20/584 , C08L83/00
摘要： A method is presented for making alkoxy-modified silsesquioxanes (AMS) or co-alkoxy-modified silsesquioxanes (co-AMS,) comprising the steps of (a) combining as a reaction mixture (i) water, (ii) an acid-stable solvent for the water, (iii) a solid strong cationic hydrolysis and condensation catalyst, and (iv) a trialkoxysilane compound, (b) allowing the reaction mixture to react for about 0.5 hours to about 200 hours to form the alkoxy-modified silsesquioxanes; and (c) recovering the alkoxy-modified silsesquioxanes from the reaction mixture. The use of solid strong cationic catalysts in this reaction system is advantageous because they remain as solids throughout the reaction, allowing simplified separation of the solid catalyst from the soluble AMS or co-AMS products, resulting in total or near total recovery of the AMS or co-AMS products, the products being free of, or substantially free of residual acid catalyst, as well as virtual total recovery of the catalyst for recycling. The improved AMS and co-AMS compounds, vulcanizable rubber compounds containing them, and a pneumatic tire having a component made from the vulcanized rubber compounds are also presented.
摘要翻译：提出了制备烷氧基改性倍半硅氧烷（AMS）或共 - 烷氧基改性倍半硅氧烷（co-AMS）的方法，该方法包括以下步骤：（a）将反应混合物（i）和（ii）酸稳定溶剂，（iii）固体强阳离子水解和缩合催化剂，和（iv）三烷氧基硅烷化合物，（b）使反应混合物反应约0.5小时至约200小时以形成烷氧基改性倍半硅氧烷; 和（c）从反应混合物中回收烷氧基改性的倍半硅氧烷。在该反应系统中使用固体强阳离子催化剂是有利的，因为它们在整个反应中保持固体，允许固体催化剂与可溶性AMS或共AMS产物的简单分离，导致AMS或共AMS产品，产品没有或基本上没有残留的酸催化剂，以及用于再循环的催化剂的虚拟总回收。还提出了改进的AMS和共AMS化合物，含有它们的可硫化橡胶化合物和具有由硫化橡胶化合物制成的组分的充气轮胎。

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