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1. 发明申请

US20130281590A1 Rubber Composition With Improved Bis-Silane Reinforcement 有权
标题翻译：改善双硅烷增强橡胶组合物
公开(公告)号：US20130281590A1
公开(公告)日：2013-10-24
申请号：US13976217
申请日：2011-12-21
申请人： Chenchy J. Lin , Atsushi Fukushima , Christopher G. Robertson , William L. Hergenrother , Yaohong Chen
发明人： Chenchy J. Lin , Atsushi Fukushima , Christopher G. Robertson , William L. Hergenrother , Yaohong Chen
IPC分类号： C08K3/36 , C08K5/5419 , C08K5/548
CPC分类号： C08K3/36 , B60C1/00 , C08K5/5419 , C08K5/548 , C08K2201/014 , C08L7/00 , C08L9/00 , C08L9/06
摘要： The present disclosure is directed to tire rubber compositions containing at least one rubbery polymer (with 10 to 100 weight percent of monomer units derived from conjugated diene monomer having between 4 and 8 carbon atoms and 0 to 90 weight percent of monomer units derived from vinyl aromatic monomer); 0.5 to 100 phr of silica filler; 0.05 to 20 phr of a bi-functional silica coupling agent; and 1 to 30 phr of a non-elastomer reactive filler reinforcing agent capable of interacting with at least two silica particles. The bi-functional silica coupling agent and the filler reinforcing agent are utilized in a weight ratio of from 1:100 to 1:0.2. Also disclosed are methods for preparing the tire rubber compositions.
摘要翻译：本公开涉及含有至少一种橡胶状聚合物（10至100重量％的衍生自具有4至8个碳原子的共轭二烯单体的单体单元和0至90重量％衍生自乙烯基芳族化合物的单体单元的轮胎橡胶组合物）单体）; 0.5〜100phr二氧化硅填料; 0.05〜20phr双功能二氧化硅偶联剂; 和1至30phr的能够与至少两种二氧化硅颗粒相互作用的非弹性体反应性填料增强剂。二官能二氧化硅偶联剂和填料增强剂以1:100至1:0.2的重量比使用。还公开了制备轮胎橡胶组合物的方法。

2. 发明授权

US08501895B2 Method for making alkoxy-modified silsesquioxanes and amino alkoxy-modified silsesquioxanes 有权
标题翻译：制备烷氧基改性倍半硅氧烷和氨基烷氧基改性倍半硅氧烷的方法
公开(公告)号：US08501895B2
公开(公告)日：2013-08-06
申请号：US12347047
申请日：2008-12-31
申请人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： C08G77/26
CPC分类号： C08G77/28 , C08G77/26 , Y02P20/584
摘要： A method is presented for making an amino alkoxy-modified silsesquioxane (amino AMS) comprising one or more compounds selected from the group consisting of an amino-AMS, an amino/mercaptan co-AMS, an amino/blocked mercaptan co-AMS, and mixtures of these. The use of solid strong cationic catalysts in this reaction system is advantageous because the catalyst remains as a solid throughout the reaction, allowing simplified separation of the solid catalyst from the soluble amino AMS or amino co-AMS products, resulting in total or near total recovery of the amino AMS or amino co-AMS products, as well as virtual total recovery of the catalyst for recycling. The use of the solid strong cationic catalysts is advantageous because it results in amino AMS products that are free of, or substantially free of, residual acid catalyst.
摘要翻译：提出了一种制备氨基烷氧基改性倍半硅氧烷（氨基AMS）的方法，其包含一种或多种选自氨基AMS，氨基/硫醇共-AMS，氨基/封端的硫醇共-AMS的化合物和这些的混合物。在该反应体系中使用固体强阳离子催化剂是有利的，因为催化剂在整个反应中保持固体，使固体催化剂与可溶性氨基AMS或氨基共聚AMS产物的分离更简单，导致总的或接近总的回收的氨基AMS或氨基共AMS产物，以及用于再循环的催化剂的虚拟总回收率。使用固体强阳离子催化剂是有利的，因为其导致氨基AMS产物不含或基本上不含残留的酸催化剂。

3. 发明授权

US08399562B2 Amine-containing alkoxysilyl-functionalized polymers 有权
标题翻译：含胺的烷氧基甲硅烷基官能化聚合物
公开(公告)号：US08399562B2
公开(公告)日：2013-03-19
申请号：US13406714
申请日：2012-02-28
申请人： Terrence E. Hogan , William L. Hergenrother , Maria Tallman
发明人： Terrence E. Hogan , William L. Hergenrother , Maria Tallman
IPC分类号： C08G77/26
CPC分类号： C08C19/22 , B60C1/00 , B60C1/0016 , B60C1/0025 , C08C19/25 , C08C19/44 , C08F8/32 , C08F8/42 , C08L15/00
摘要： An amine-containing alkoxysilyl-functionalized polymer, a method of preparing a reactive polymer functionalized with an alkoxysilane functionalizing agent and further reacted with an amino alcohol, the resulting polymer, and vulcanizates thereof.
摘要翻译：含胺的烷氧基甲硅烷基官能化聚合物，制备用烷氧基硅烷官能化剂官能化的反应性聚合物的方法，并进一步与氨基醇反应，得到的聚合物和硫化产物。

4. 发明授权

US08344049B2 Modified asphalt binders and asphalt paving compositions 失效
标题翻译：改性沥青结合料和沥青铺路料
公开(公告)号：US08344049B2
公开(公告)日：2013-01-01
申请号：US12881791
申请日：2010-09-14
申请人： William L. Hergenrother , Peter W. Boerner , Christine Rademacher , Daniel F. Graves , Timothy P. Reece , Herbert L. Wissel
发明人： William L. Hergenrother , Peter W. Boerner , Christine Rademacher , Daniel F. Graves , Timothy P. Reece , Herbert L. Wissel
IPC分类号： C08L95/00
CPC分类号： C08L95/00 , C08L25/10 , C08L53/02 , C08L2666/74 , C08L53/00 , C08L2666/24 , C08L2666/04
摘要： A modified asphalt binder composition prepared by combining asphalt binder, phosphorus pentasulfide, and less than 2.5 parts by weight unsaturated polymer, per 100 parts by weight asphalt binder, to thereby produce a modified asphalt binder composition characterized by an elongation recovery at 25° C., as determined according to AASHTO T301, of greater than 75%.
摘要翻译：通过将沥青粘合剂，五硫化二磷和小于2.5重量份的不饱和聚合物相对于100重量份的沥青粘合剂混合制备的改性沥青粘合剂组合物，由此制备改性沥青粘合剂组合物，其特征在于在25℃下的伸长率恢复，根据AASHTO T301确定，大于75％。

5. 发明授权

US08329297B2 Rubber compositions containing non-sulfur silica coupling agents bound to diene rubbers 有权
标题翻译：含有与二烯橡胶结合的非硫二氧化硅偶联剂的橡胶组合物
公开(公告)号：US08329297B2
公开(公告)日：2012-12-11
申请号：US12628527
申请日：2009-12-01
申请人： William L. Hergenrother , Chenchy Jeffrey Lin , Yaohong Chen
发明人： William L. Hergenrother , Chenchy Jeffrey Lin , Yaohong Chen
IPC分类号： B32B5/16 , B60C5/00 , C08G18/08 , C08G73/10
CPC分类号： C08L9/06 , B60C1/00 , C08K3/013 , C08K5/5419 , C08K5/544 , Y10T152/10495 , Y10T428/2995 , C08L21/00
摘要： The invention provides vulcanizable rubber compound having improved tensile mechanical and dynamic viscoelastic properties. The compounds are formed by mixing an elastomer, containing unsaturated carbon-carbon bonds in its molecular structure, with a reinforcing inorganic filler silica in the presence of an alkyl alkoxysilane and a non-sulfur coupling agent that binds to the rubber backbone with an “ene” linkage or a 1,3 dipolar addition linkage. In particular, the coupling agent and the alkyl alkoxysilane are present in the compound in a weight ratio of about 0.0001:1 to about 1:1.
摘要翻译：本发明提供具有改进的拉伸机械和动态粘弹性的硫化橡胶化合物。该化合物通过在烷基烷氧基硅烷和非硫偶联剂存在下，将具有分子结构中含有不饱和碳 - 碳键的弹性体与增强无机填料二氧化硅混合而形成，所述烷基烷氧基硅烷和非硫偶联剂与烯键连接在橡胶骨架上或1,3-偶极加成键。特别地，偶联剂和烷基烷氧基硅烷以约0.0001:1至约1:1的重量比存在于化合物中。

6. 发明申请

US20120077922A1 Amino Alkoxy-Modified Silsesquioxane Adhesives For Improved Metal Adhesion And Metal Adhesion Retention To Cured Rubber 有权
标题翻译：用于改善金属粘附性和固化橡胶金属粘附保持性的氨基烷氧基改性倍半硅氧烷粘合剂
公开(公告)号：US20120077922A1
公开(公告)日：2012-03-29
申请号：US13174129
申请日：2011-06-30
申请人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan , Zhong-Ren Chen
发明人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan , Zhong-Ren Chen
IPC分类号： C08K3/08
CPC分类号： C08K3/08 , C08G77/26 , C08K5/544 , C09J183/08 , C08L21/00
摘要： Amino alkoxy-modified silsesquioxanes (amino AMS), and/or amino co-AMS compounds that also comprise a mercaptosilane or a blocked mercaptosilane, are excellent adhesives for coating plated or unplated metal wire for adherence of the wire to a rubber stock. The amino AMS and/or the amino/mercaptan co-AMS adhesives can be used with all types of rubber and there is no requirement for the use of special adhesive additives to the rubber vulcanizates, such as, but not limited to, cobalt, resins and high sulfur levels. In particular, the use of amino AMS and/or amino/mercaptan co-AMS compounds as adhesives for bonding wire to rubber also improves the adherence performance of the reinforcements to obtain sufficient bonding that is resistant to degradation over the course of time, especially resistance to thermal aging and/or thermo-oxidizing aging, in particular corrosion in the presence of water. Vulcanized rubber compositions that contain an amino AMS and/or amino/mercaptan co-AMS compound also have improved adhesion to embedded uncoated steel after humidity aging compared with vulcanized rubber compositions not containing the amino alkoxy-modified silsesquioxane.
摘要翻译：还包含巯基硅烷或封端巯基硅烷的氨基烷氧基改性倍半硅氧烷（氨基AMS）和/或氨基共-MSMS化合物是用于涂覆电镀或未镀覆金属丝的优良粘合剂，用于将线粘附到橡胶原料上。氨基AMS和/或氨基/硫醇共-AMS粘合剂可以与所有类型的橡胶一起使用，并且不需要对橡胶硫化橡胶使用特殊的粘合剂添加剂，例如但不限于钴，树脂和高硫含量。特别地，使用氨基AMS和/或氨基/硫醇共-AMS化合物作为用于将线接合到橡胶上的粘合剂也提高了增强材料的粘附性能，以获得足够的粘合，其耐受在时间上的劣化，特别是电阻热老化和/或热氧化老化，特别是在水存在下的腐蚀。与不含氨基烷氧基改性的倍半硅氧烷的硫化橡胶组合物相比，含有氨基AMS和/或氨基/硫醇共-AMS化合物的硫化橡胶组合物在湿度老化后也具有改善的对包埋未涂层钢的粘附性。

7. 发明授权

US08124677B2 Modified asphalt binders and asphalt paving compositions 有权
标题翻译：改性沥青结合料和沥青铺路料
公开(公告)号：US08124677B2
公开(公告)日：2012-02-28
申请号：US12881768
申请日：2010-09-14
申请人： William L. Hergenrother , Peter W. Boerner , Daniel F. Graves , Christine Rademacher , Timothy P. Reece , Herbert L. Wissel
发明人： William L. Hergenrother , Peter W. Boerner , Daniel F. Graves , Christine Rademacher , Timothy P. Reece , Herbert L. Wissel
IPC分类号： C08L95/00
CPC分类号： C08L95/00 , C08L53/02 , C08L53/00
摘要： A modified asphalt binder composition prepared by combining asphalt binder, phosphorus pentasulfide, and less than 2.5 parts by weight unsaturated polymer, per 100 parts by weight asphalt binder, to thereby produce a modified asphalt binder composition characterized by an elongation recovery at 25° C., as determined according to AASHTO T301, of greater than 75%, where the phosphorus pentasulfide includes a blend of P4S10 and P4S9.
摘要翻译：通过将沥青粘合剂，五硫化二磷和小于2.5重量份的不饱和聚合物相对于100重量份的沥青粘合剂混合制备的改性沥青粘合剂组合物，由此制备改性沥青粘合剂组合物，其特征在于在25℃下的伸长率恢复，如根据AASHTO T301测定的大于75％，其中五硫化二磷包括P4S10和P4S9的共混物。

8. 发明授权

US08097674B2 Amino alkoxy-modified silsesquioxanes in silica-filled rubber with low volatile organic chemical evolution 有权
标题翻译：二氧化硅填充橡胶中的氨基烷氧基改性倍半硅氧烷，具有低挥发性有机化学演化
公开(公告)号：US08097674B2
公开(公告)日：2012-01-17
申请号：US12347017
申请日：2008-12-31
申请人： William L. Hergenrother , Chenchy Jeffrey Lin
发明人： William L. Hergenrother , Chenchy Jeffrey Lin
IPC分类号： B60C1/00
CPC分类号： C08K5/544 , C08G77/26 , C08G77/28 , C08K5/548 , C09D183/08 , Y02T10/862 , Y10T152/10 , Y10T152/10495 , Y10T428/2991 , Y10T428/2995
摘要： A vulcanizable rubber composition is presented that comprises an elastomer; a reinforcing filler selected from silica, carbon black, and mixtures thereof, a cure agent; and an amino alkoxy-modified silsesquioxane (AMS) comprising one or more compounds selected from the group consisting of an amino AMS, an amino/mercaptan co-AMS, an amino/blocked mercaptan co-AMS, mixtures thereof, and weak acid-neutralized solid and aqueous solutions thereof. Addition of such compounds to the rubber composition provides improved dynamic viscoelastic and mechanical properties of the vulcanized rubber compound and predict that tire components, especially tread stocks, will provide tires having improved snow traction, lower rolling resistance but equal wet traction, increased rebound, decreased hysteresis, and a general improvement in tire performance.
摘要翻译：提供了一种可硫化的橡胶组合物，其包含弹性体; 选自二氧化硅，炭黑及其混合物的增强填料，固化剂; 和氨基烷氧基改性倍半硅氧烷（AMS），其包含一种或多种选自氨基AMS，氨基/硫醇共-AMS，氨基/封端的硫醇共-AMS，及其混合物和弱酸中和其固体和水溶液。将这些化合物加入到橡胶组合物中提供了硫化橡胶化合物的动态粘弹性和机械性能，并预测轮胎组分，特别是胎面胶料将提供具有改善的雪牵引力，较低滚动阻力但相等的湿牵引力，增加的回弹，降低的轮胎滞后和轮胎性能的普遍改进。

9. 发明授权

US08058357B2 Vulcanizable compositions and tire treads prepared therewith 有权
标题翻译：可硫化组合物和用其制备的轮胎胎面
公开(公告)号：US08058357B2
公开(公告)日：2011-11-15
申请号：US12347762
申请日：2008-12-31
申请人： Amy Randall , Terrence E. Hogan , William L. Hergenrother
发明人： Amy Randall , Terrence E. Hogan , William L. Hergenrother
IPC分类号： C08C19/20 , C08F8/34
CPC分类号： B60C1/0016 , C08C19/44 , C08K5/40 , C08L15/00 , C08L21/00
摘要： A method for preparing a tire tread, the method comprising vulcanizing a vulcanizable composition comprising a rubber component including a functionalized polymer and a cure system, where the cure system includes sulfur and a disulfide compound represented by the formula I R1—S—S—R3—S—S—R2 where R3 represents a divalent organic group and R1 and R2 each independently include a monovalent organic group including a nitrogen atom.
摘要翻译：一种制备轮胎胎面的方法，所述方法包括硫化包含含官能化聚合物和固化体系的橡胶组分的可硫化组合物，其中所述固化体系包括硫和由式I R1-S-S-R3表示的二硫化物 -S-S-R 2，其中R 3表示二价有机基团，并且R 1和R 2各自独立地包括包含氮原子的一价有机基团。

10. 发明授权

US07642302B2 Modified asphalt binders and asphalt paving compositions 失效
公开(公告)号：US07642302B2
公开(公告)日：2010-01-05
申请号：US11820716
申请日：2007-06-20
申请人： William L. Hergenrother , Peter W. Boerner , Daniel F. Graves , Christine Rademacher , Timothy P. Reece , Herbert L. Wissel
发明人： William L. Hergenrother , Peter W. Boerner , Daniel F. Graves , Christine Rademacher , Timothy P. Reece , Herbert L. Wissel
IPC分类号： C08K3/30 , C08K3/32 , C08L95/00
CPC分类号： C08L95/00 , C08L53/02 , C08L53/00
摘要： A process for preparing a modified asphalt binder composition, the process comprising mixing asphalt, an unsaturated polymer, and phosphorus pentasulfide to form a modified asphalt composition.

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