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1. 发明授权

US06630535B1 Rubber compositions & vulcanizates including comb polymers 失效
标题翻译：橡胶组合物和硫化胶，包括梳形聚合物
公开(公告)号：US06630535B1
公开(公告)日：2003-10-07
申请号：US09642497
申请日：2000-08-18
申请人： Terrence E. Hogan , James A. Krom , James E. Hall , Xiaorong Wang , Peyman Pakdel , William L. Hergenrother
发明人： Terrence E. Hogan , James A. Krom , James E. Hall , Xiaorong Wang , Peyman Pakdel , William L. Hergenrother
IPC分类号： C08L5100
CPC分类号： C08L51/003 , C08L51/04 , C08L2666/02 , C08L2666/04
摘要： A composition comprising an elastomer, a filler, and a comb-like polymer, the comb-like polymer comprising a backbone and a plurality of side chains, the backbone having a length greater than or equal to the entanglement length, the side chains having a length greater than about 33% of the entanglement length, the backbone including at least one side chain per entanglement length, and the comb-like polymer having a Tg of less than −5° C.
摘要翻译：包含弹性体，填料和梳状聚合物的组合物，所述梳状聚合物包含骨架和多个侧链，主链具有大于或等于缠结长度的长度，侧链具有长度大于缠结长度的约33％，骨架包括每个缠结长度的至少一个侧链，并且梳状聚合物的Tg小于-5℃。

2. 发明授权

US06194485B1 Compounding process for achieving uniform, fine particle size dispersion of curing agents with minimal use of solvents 失效
标题翻译：用最少使用溶剂实现固化剂均匀，细粒度分散的复合方法
公开(公告)号：US06194485B1
公开(公告)日：2001-02-27
申请号：US09285198
申请日：1999-04-01
申请人： Terrence E. Hogan , Xiaorong Wang , William L. Hergenrother , Georg G. A. Bohm
发明人： Terrence E. Hogan , Xiaorong Wang , William L. Hergenrother , Georg G. A. Bohm
IPC分类号： B29C7300
CPC分类号： H04M3/42034 , C08J3/2053 , C08J2321/00 , C08K5/33 , C08L2666/02 , C08L2666/36 , C09J121/00 , C09J123/16 , C08L21/00
摘要： Rubber curing agents such as quinoids are compounded to achieve a uniform or homogeneous distribution thereof in a rubber composition. The quinoid curing agents are initially solubilized in an organic polar solvent and then mixed with the rubber or rubber masterbatch. The organic polar solvent is then removed. A uniform fine distribution of the curing agent results in improved physical properties. The process is an improvement in that it does not require the rubber masterbatch be dissolved in a nonpolar solvent. The present invention is particularly suitable as a sealant composition for tires.
摘要翻译：复合橡胶固化剂如醌类以在橡胶组合物中达到均匀或均匀的分布。醌类固化剂最初溶解在有机极性溶剂中，然后与橡胶或橡胶母料混合。然后除去有机极性溶剂。固化剂的均匀精细分布导致改善的物理性能。该方法的改进在于不需要将橡胶母料溶解在非极性溶剂中。本发明特别适用于轮胎用密封剂组合物。

3. 发明授权

US06573412B1 Chain-coupled polymeric alkoxide compounds having controlled viscosity 有权
标题翻译：具有受控粘度的链偶联聚合物醇盐化合物
公开(公告)号：US06573412B1
公开(公告)日：2003-06-03
申请号：US09570578
申请日：2000-05-12
申请人： Terrence E. Hogan , William L. Hergenrother , James E. Hall
发明人： Terrence E. Hogan , William L. Hergenrother , James E. Hall
IPC分类号： C07C4311
CPC分类号： C08C19/44 , C08F8/42 , C08F2810/40 , C08J5/18 , C08F8/00 , C08F297/04
摘要： The invention provides chain-coupled polymeric alkoxide compounds for use as the elastomeric component in vulcanizable elastomeric compositions comprising silica, carbon black or mixtures thereof. In particular, the invention provides anionically polymerized polymers having polymer chain living ends that are functionalized with alkoxide groups and coupled together by a metal or nonmetal atom. The polymeric alkoxide compounds have an initial high viscosity for ease of handling prior to compounding, a stable viscosity during storage, and a decreased compound viscosity for better filler dispersion and improved mixing efficiency. The invention further provides a pneumatic tire having at least one component produced from the vulcanizable elastomeric composition of the invention.
摘要翻译：本发明提供了用作可硫化弹性体组合物中的弹性体组分的链偶联聚合物醇盐化合物，其包含二氧化硅，炭黑或其混合物。特别地，本发明提供具有聚合物链活性末端的阴离子聚合聚合物，该末端用烷氧基基团官能化并通过金属或非金属原子偶联在一起。聚合物醇盐化合物具有初始高粘度，以便在配混之前易于处理，在储存期间稳定的粘度，以及降低的化合物粘度以获得更好的填料分散和改善的混合效率。本发明还提供一种充气轮胎，其具有由本发明的可硫化弹性体组合物制成的至少一种组分。

4. 发明授权

US06476117B1 Grafted near-gelation polymers having high damping properties 失效
标题翻译：具有高阻尼性能的接枝近胶凝聚合物
公开(公告)号：US06476117B1
公开(公告)日：2002-11-05
申请号：US09586873
申请日：2000-06-05
申请人： Xiaorong Wang , Victor J. Foltz , Terrence E. Hogan , James E. Hall
发明人： Xiaorong Wang , Victor J. Foltz , Terrence E. Hogan , James E. Hall
IPC分类号： C08L2326
CPC分类号： C08F8/00 , C08F297/00
摘要： Thermoplastic elastomers containing hard segments formed from polyalkylenes and soft segments formed from elastomeric polymers near their gelation point are formed. Compositions containing these materials are elastomeric and exhibit excellent damping capabilities over a wide range of temperatures and frequencies.
摘要翻译：形成包含由聚烯烃形成的硬链段和在其凝胶化点附近由弹性体聚合物形成的软链段的热塑性弹性体。含有这些材料的组合物是弹性体，并且在宽范围的温度和频率下表现出优异的阻尼能力。

5. 发明授权

US08822620B2 Method for making alkoxy-modified silsesquioxanes 有权
标题翻译：制备烷氧基改性倍半硅氧烷的方法
公开(公告)号：US08822620B2
公开(公告)日：2014-09-02
申请号：US13030611
申请日：2011-02-18
申请人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： C08G77/08
CPC分类号： C08G77/08 , B60C1/00 , C08G77/18 , C08G77/28 , C08K3/013 , C08L9/00 , C08L21/00 , C08L83/06 , C08L83/08 , Y02P20/584 , C08L83/00
摘要： A method is presented for making alkoxy-modified silsesquioxanes (AMS) or co-alkoxy-modified silsesquioxanes (co-AMS,) comprising the steps of (a) combining as a reaction mixture (i) water, (ii) an acid-stable solvent for the water, (iii) a solid strong cationic hydrolysis and condensation catalyst, and (iv) a trialkoxysilane compound, (b) allowing the reaction mixture to react for about 0.5 hours to about 200 hours to form the alkoxy-modified silsesquioxanes; and (c) recovering the alkoxy-modified silsesquioxanes from the reaction mixture. The use of solid strong cationic catalysts in this reaction system is advantageous because they remain as solids throughout the reaction, allowing simplified separation of the solid catalyst from the soluble AMS or co-AMS products, resulting in total or near total recovery of the AMS or co-AMS products, the products being free of, or substantially free of residual acid catalyst, as well as virtual total recovery of the catalyst for recycling. The improved AMS and co-AMS compounds, vulcanizable rubber compounds containing them, and a pneumatic tire having a component made from the vulcanized rubber compounds are also presented.
摘要翻译：提出了制备烷氧基改性倍半硅氧烷（AMS）或共 - 烷氧基改性倍半硅氧烷（co-AMS）的方法，该方法包括以下步骤：（a）将反应混合物（i）和（ii）酸稳定溶剂，（iii）固体强阳离子水解和缩合催化剂，和（iv）三烷氧基硅烷化合物，（b）使反应混合物反应约0.5小时至约200小时以形成烷氧基改性倍半硅氧烷; 和（c）从反应混合物中回收烷氧基改性的倍半硅氧烷。在该反应系统中使用固体强阳离子催化剂是有利的，因为它们在整个反应中保持固体，允许固体催化剂与可溶性AMS或共AMS产物的简单分离，导致AMS或共AMS产品，产品没有或基本上没有残留的酸催化剂，以及用于再循环的催化剂的虚拟总回收。还提出了改进的AMS和共AMS化合物，含有它们的可硫化橡胶化合物和具有由硫化橡胶化合物制成的组分的充气轮胎。

6. 发明授权

US08513371B2 Amino alkoxy-modified silsesquioxanes and method of preparation 有权
标题翻译：氨基烷氧基改性倍半硅氧烷及其制备方法
公开(公告)号：US08513371B2
公开(公告)日：2013-08-20
申请号：US12346994
申请日：2008-12-31
申请人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
发明人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
IPC分类号： C08G77/26
CPC分类号： C08K5/544 , C08G77/26 , C08G77/28 , C08K5/548 , C09D183/08 , Y02T10/862 , Y10T152/10 , Y10T152/10495 , Y10T428/2991 , Y10T428/2995
摘要： An amino alkoxy-modified silsesquioxane (AMS) comprising one or more compounds selected from the group consisting of an amino AMS, an amino/mercaptan co-AMS, an amino/blocked mercaptan co-AMS, mixtures thereof, and a weak acid-neutralized solid or aqueous solution thereof, and a method of making the amino AMS, are presented. The compounds are useful in compounding, processing, cure and storage of silica-reinforced rubbers because they contain low levels of volatile organic compounds (VOC).
摘要翻译：包含一种或多种选自氨基AMS，氨基/硫醇共-AMS，氨基/封端的硫醇共-AMS，及其混合物和弱酸中和的氨基烷氧基改性倍半硅氧烷（AMS）提供其固体或水溶液，以及制备氨基AMS的方法。该化合物可用于二氧化硅增强橡胶的混合，加工，固化和储存，因为它们含有低水平的挥发性有机化合物（VOC）。

7. 发明申请

US20080308204A1 FUNCTIONAL POLYMERS PREPARED WITH SULFUR-CONTAINING INITIATORS 有权
标题翻译：功能性聚合物与含硫装置的制备
公开(公告)号：US20080308204A1
公开(公告)日：2008-12-18
申请号：US12139567
申请日：2008-06-16
申请人： Terrence E. Hogan , William L. Hergenrother
发明人： Terrence E. Hogan , William L. Hergenrother
IPC分类号： B60C1/00 , C07C321/14
CPC分类号： B60C1/0016 , B60C1/00 , B60C1/0025 , C08F36/04 , C08L19/006 , C08F4/48
摘要： A method for forming a polymer including a sulfur-containing functional group, the method comprising introducing a sulfur-containing initiator defined by the formula with conjugated diene monomer and optionally copolymerizable monomer within a polymerization medium and allowing the sulfur-containing initiator to initiate the polymerization of the conjugated diene monomer and the optional copolymerizable monomer, where R1 is a monovalent organic group, R2 is a divalent organic group, R3 is a divalent organic group or a bond, and a is an integer from 1 to about 5.
摘要翻译：一种形成含有含硫官能团的聚合物的方法，所述方法包括将由式表示的含硫起始物与共轭二烯单体和任选的可共聚单体引入聚合介质中，并允许含硫引发剂引发聚合的共轭二烯单体和任选的可共聚单体，其中R 1为一价有机基团，R 2为二价有机基团，R 3为二价有机基团或键，a为1至约5的整数。

8. 发明申请

US20080293858A1 METHOD FOR MAKING ALKOXY-MODIFIED SILSESQUIOXANES 有权
标题翻译：制备改性硅烷氧基硅烷的方法
公开(公告)号：US20080293858A1
公开(公告)日：2008-11-27
申请号：US11752715
申请日：2007-05-23
申请人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , James H. Pawlow , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： B60C1/00 , C07F7/00
CPC分类号： C08G77/08 , B60C1/00 , C08G77/18 , C08G77/28 , C08K3/013 , C08L9/00 , C08L21/00 , C08L83/06 , C08L83/08 , Y02P20/584 , C08L83/00
摘要： A method is presented for making alkoxy-modified silsesquioxanes (AMS) or co-alkoxy-modified silsesquioxanes (co-AMS,) comprising the steps of (a) combining as a reaction mixture (i) water, (ii) an acid-stable solvent for the water, (iii) a solid strong cationic hydrolysis and condensation catalyst, and (iv) a trialkoxysilane compound, (b) allowing the reaction mixture to react for about 0.5 hours to about 200 hours to form the alkoxy-modified silsesquioxanes; and (c) recovering the alkoxy-modified silsesquioxanes from the reaction mixture. The use of solid strong cationic catalysts in this reaction system is advantageous because they remain as solids throughout the reaction, allowing simplified separation of the solid catalyst from the soluble AMS or co-AMS products, resulting in total or near total recovery of the AMS or co-AMS products, the products being free of, or substantially free of residual acid catalyst, as well as virtual total recovery of the catalyst for recycling. The improved AMS and co-AMS compounds, vulcanizable rubber compounds containing them, and a pneumatic tire having a component made from the vulcanized rubber compounds are also presented.
摘要翻译：提出了制备烷氧基改性倍半硅氧烷（AMS）或共 - 烷氧基改性倍半硅氧烷（co-AMS）的方法，该方法包括以下步骤：（a）将反应混合物（i）和（ii）酸稳定溶剂，（iii）固体强阳离子水解和缩合催化剂，和（iv）三烷氧基硅烷化合物，（b）使反应混合物反应约0.5小时至约200小时以形成烷氧基改性倍半硅氧烷; 和（c）从反应混合物中回收烷氧基改性的倍半硅氧烷。在该反应系统中使用固体强阳离子催化剂是有利的，因为它们在整个反应中保持固体，允许固体催化剂与可溶性AMS或共AMS产物的简单分离，导致AMS或共AMS产品，产品没有或基本上没有残留的酸催化剂，以及用于再循环的催化剂的虚拟总回收。还提出了改进的AMS和共AMS化合物，含有它们的可硫化橡胶化合物和具有由硫化橡胶化合物制成的组分的充气轮胎。

9. 发明授权

US06303694B1 Compounding process for achieving uniform, fine particle size dispersion of curing agents in the substantial absence of solvents and a sealant produced thereby 失效
标题翻译：在基本上不存在溶剂的情况下实现固化剂的均匀，细粒度分散的复合方法和由此产生的密封剂
公开(公告)号：US06303694B1
公开(公告)日：2001-10-16
申请号：US09507381
申请日：2000-02-18
申请人： Terrence E. Hogan , William L. Hergenrother , Christine Morehart
发明人： Terrence E. Hogan , William L. Hergenrother , Christine Morehart
IPC分类号： C08F800
CPC分类号： C08J3/226 , C08J2321/00 , C08K5/33 , C08L21/00
摘要： A process for the preparation of a sealant composition by mixing an elastomer in the substantial absence of an organic solvent and separately dispersing a quinoid curing agent in a polymer having a molecular weight below about 5,000 to form a curing agent concentrate. Thereafter, combining the curing agent concentrate with the elastomer to form the sealant composition. The composition is a rubber masterbatch having many applications and is advantageously, substantially free from organic solvents.
摘要翻译：通过在基本上不存在有机溶剂的情况下混合弹性体并且将醌型固化剂单独分散在分子量低于约5,000的聚合物中以形成固化剂浓缩物来制备密封剂组合物的方法。此后，将固化剂浓缩物与弹性体组合以形成密封剂组合物。该组合物是具有许多应用的橡胶母料，并且有利地基本上不含有机溶剂。

10. 发明授权

US09163135B2 Rubber compositions with filler and ketoxime or ketixmo silane 有权
标题翻译：具有填料和酮肟或酮肟硅烷的橡胶组合物
公开(公告)号：US09163135B2
公开(公告)日：2015-10-20
申请号：US13819815
申请日：2011-08-31
申请人： Chenchy J. Lin , Yaohong Chen , Atsushi Fukushima , William L. Hergenrother , Terrence E. Hogan
发明人： Chenchy J. Lin , Yaohong Chen , Atsushi Fukushima , William L. Hergenrother , Terrence E. Hogan
IPC分类号： C08L9/00 , C08K5/5465 , C08K5/548
CPC分类号： C08K5/5465 , C08K3/04 , C08K5/548 , C08L91/00 , C08L21/00
摘要： A composition includes an elastomer and a ketoximo silane or a ketoxime additive. The ketoximo silane corresponds to Formula I: where D is selected from a C1 to C60 hydrocarbyl group, or when A is 0 or 1 a hydrogen, or the structure in Formula III; and wherein n and j are independently 1, 2, or 3, m and q are independently 0 or 1, z and t are independently 0 or 1 and (n+m+z) is equal to 3 and (j+q+t) is equal to 3; A is 0 or greater than or equal to 1; R1 and R2 are independently Ci to C60 divalent organic groups and may optionally include O, N S, Si, and/or P heteroatoms with the proviso that when A is 0 either of R1 and R2 may be a chemical bond; R3, R4, R8 and R9 are independently a hydrogen, or a C1 to C60 hydrocarbyl or alkoxy group optionally including O, N, S, Si and/or P; R5 and R6 are independently hydrogen or C1 to C60 hydrocarbyl groups and may optionally include O, N S, Si, and/or P heteroatoms, and may optionally be bonded together to form a cyclic ring; R10 and R11 are independently hydrogen or C1 to C60 hydrocarbyl groups and may optionally include O, N S, Si, and/or P heteroatoms, and may optionally be bonded together to form a cyclic ring.
摘要翻译：组合物包括弹性体和酮肟基硅烷或酮肟添加剂。酮肟基硅烷对应于式I：其中D选自C1至C60烃基，或当A为0或1时为氢或式III中的结构; 并且其中n和j独立地为1,2或3，m和q独立地为0或1，z和t独立地为0或1，并且（n + m + z）等于3，并且（j + q + t ）等于3; A为0或大于或等于1; R 1和R 2独立地为C 1至C 60二价有机基团，并且可任选地包括O，N S，Si和/或P杂原子，条件是当A为0时，R 1和R 2可以是化学键; R 3，R 4，R 8和R 9独立地为氢或任选包括O，N，S，Si和/或P的C 1至C 60烃基或烷氧基; R 5和R 6独立地是氢或C 1至C 60烃基，并且可任选地包括O，N S，Si和/或P杂原子，并且可以任选地结合在一起形成环状环; R 10和R 11独立地为氢或C 1至C 60烃基，并且可以任选地包括O，N S，Si和/或P杂原子，并且可以任选地结合在一起形成环状环。

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