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    • 1. 发明授权
    • Field emission electron gun system
    • 场发射电子枪系统
    • US4945247A
    • 1990-07-31
    • US365827
    • 1989-06-14
    • Takeshi KawasakiJunji EndoShigeto IsakozawaMasahiro TomitaAkira Tonomura
    • Takeshi KawasakiJunji EndoShigeto IsakozawaMasahiro TomitaAkira Tonomura
    • H01J29/48H01J37/073H01J37/145
    • H01J37/073
    • In a field emission electron gun system with a multi-stage acceleration tube comprising a field emission electron source, a field emission electrode for extracting the electrons, a magnetic lens having a magnetic gap between the field emission electron source and the field emission electrode or a magnetic lens having a magnetic pole which also serves as the field emission electrode, and at least two-stages of acceleration electrodes for accelerating the electrons, a magnetization current I for the magnetic lens is changed interlocking with a field emission voltage V.sub.1 applied between the field emission electron source and the field emission electrode so that IN/.sqroot.V.sub.1 (N: the number of windings of the magnetic lens) takes a predetermined value and a first acceleration voltage V.sub.2 applied between the field emission electron source and the first-stage acceleration electrode is changed interlocking with the field emission voltage V.sub.1 so that V.sub.2 /V.sub.1 takes a predetermined value.
    • 在具有包括场发射电子源的多级加速管的场发射电子枪系统中,用于提取电子的场发射电极,在场发射电子源和场发射电极之间具有磁隙的磁透镜或 具有也用作场发射电极的磁极的磁性透镜以及用于加速电子的至少两级的加速电极,用于磁性透镜的磁化电流I与施加在磁场之间的场致发射电压V1互锁地变化 发射电子源和场发射电极,使得IN / 2ROOT V1(N:磁性透镜的绕组数)取预定值,施加在场发射电子源和第一级加速电极之间的第一加速电压V2 与场致发射电压V1互锁,使得V2 / V1取规定值。
    • 5. 发明授权
    • Electron microscope
    • 电子显微镜
    • US5552602A
    • 1996-09-03
    • US398684
    • 1995-03-06
    • Hiroshi KakibayashiYasuhiro MitsuiHideo TadokoroKatsuhiro KurodaMasanari KoguchiKazutaka TsujiTatsuo MakishimaMikio IchihashiShigeto Isakozawa
    • Hiroshi KakibayashiYasuhiro MitsuiHideo TadokoroKatsuhiro KurodaMasanari KoguchiKazutaka TsujiTatsuo MakishimaMikio IchihashiShigeto Isakozawa
    • G01N23/04G01R31/305H01J37/26
    • G01R31/305G01N23/046G01N2223/419H01J2237/226
    • 3-dimensional observation on the atomic arrangement and atomic species in a thin-film specimen as well as conventional electron microscope observations is carried out at high speed and accuracy by an electron microscope which measures electrons emitted at high angle from the specimen. For that purpose, the present invention provides a scanning transmission electron microscope having an electron detection device comprising a scintillator converting electrons detected thereby to photons, a photoconductive-film converting photons from the scintillator detected thereby to c.a. 1000 times as many electron-hole pairs as these photons (i.d. avalanche multiplication), an electron gun emitting an electron beam toward the photoconductive-film to detect the holes generated therein, and electron deflector electrodes deflecting the electron beam on the photoconductive-film. Avalanche multiplication in the photoconductive-film amplifies the signal of these photons at so high signal-to-noise ratio that the electron microscope in this invention can detect such weak electrons as emitted at high angle from the specimen at high sensitivity and resolution. Therefore this invention enables a scanning transmission electron microscope to obtain for example 3-dimensional image of point defects and impurity elements existing in joint interfaces and contacts in a ULSI device rapidly and accurately.
    • 通过电子显微镜以高速和准确的方式对薄膜样品中的原子排列和原子种类进行3维观察,以及常规的电子显微镜观察,测量从样品以高角度发射的电子。 为此目的,本发明提供了一种具有电子检测装置的扫描透射电子显微镜,该电子检测装置包括将由此检测的电子转化为光子的闪烁体,从其检测的闪烁体的光电导膜转换光子至c.a. 与这些光子(i.d.雪崩乘法)一样多的电子 - 空穴对的1000倍,向光电导膜发射电子束以检测其中产生的空穴的电子枪以及偏转电子束在光电导膜上的电子偏转器电极。 光电导膜中的雪崩乘法以如此高的信噪比放大了这些光子的信号,使得本发明的电子显微镜能够以高灵敏度和分辨率从样品中以高角度检测出这样的弱电子。 因此,本发明能够使扫描透射电子显微镜能够快速,准确地获得例如存在于ULSI装置的接合界面和触点中的点缺陷和杂质元素的3维图像。
    • 7. 发明授权
    • Element mapping unit, scanning transmission electron microscope, and element mapping method
    • 元素映射单元,扫描透射电子显微镜和元素映射方法
    • US07928376B2
    • 2011-04-19
    • US11232964
    • 2005-09-23
    • Kazutoshi KajiKazuhiro UedaKoji KimotoTakashi AoyamaShunroku TayaShigeto Isakozawa
    • Kazutoshi KajiKazuhiro UedaKoji KimotoTakashi AoyamaShunroku TayaShigeto Isakozawa
    • H01J47/00
    • H01J37/256
    • There is provided an element mapping unit, scanning transmission electron microscope, and element mapping method that enable to acquire an element mapping image very easily. On the scanning transmission electron microscope, the electron beam transmitted through an object to be analyzed enters into the element mapping unit. The electron beam is analyzed of its energy into spectrum by an electron spectrometer and an electron energy loss spectrum is acquired. Because the acceleration voltage data for each element and window data for 2-window method, 3-window method or contrast tuning method are already stored in a database and accordingly the spectrum measurement is carried out immediately even when an element to be analyzed is changed to another, the operator can confirm a two-dimensional element distribution map immediately. Besides, because every electron beam that enters into an energy filter passes through the object point, aberration strain in the electron spectrometer can be minimized and higher energy stability can be achieved. As a result, drift of the electron energy loss spectrum acquired by analyzing the electron beam into spectrum can be minimized and element distribution with higher accuracy can be acquired.
    • 提供了能够非常容易地获取元素映射图像的元素映射单元,扫描透射电子显微镜和元件映射方法。 在扫描透射电子显微镜上,通过待分析物体传输的电子束进入元件映射单元。 电子束通过电子光谱仪将其能量分析成光谱,并获得电子能量损失光谱。 因为用于2窗口方法,3窗口方法或对比度调整方法的每个元素和窗口数据的加速电压数据已经存储在数据库中,因此即使当要分析的元素被改变为 另一方面,操作者可以立即确认二维元素分布图。 此外,由于进入能量过滤器的每个电子束通过物点,所以可以使电子光谱仪中的像差应变最小化并且可以实现更高的能量稳定性。 结果,可以将通过将电子束分析成光谱而获得的电子能量损耗光谱的漂移最小化,并且可以获得具有更高精度的元素分布。
    • 10. 发明授权
    • Ultimate analyzer, scanning transmission electron microscope and ultimate analysis method
    • 终极分析仪,扫描透射电子显微镜和最终分析方法
    • US06794648B2
    • 2004-09-21
    • US10196577
    • 2002-07-17
    • Kazutoshi KajiTakashi AoyamaShunroku TayaHiroyuki TanakaShigeto Isakozawa
    • Kazutoshi KajiTakashi AoyamaShunroku TayaHiroyuki TanakaShigeto Isakozawa
    • H01J3726
    • G01N23/04G01N23/20H01J37/05H01J37/244H01J37/256H01J37/265H01J37/28H01J2237/057H01J2237/24475H01J2237/24485H01J2237/24495H01J2237/2522H01J2237/2802H01J2237/2804H01J2237/2809
    • An object of the present invention is to provide an ultimate analyzer which can display an element distribution image of an object to be analyzed with high contrast to determine the positions of the element distribution with high accuracy, and a scanning transmission electron microscope and a method of analyzing elements using the ultimate analyzer. The present invention exists in an ultimate analyzer comprising a scattered electron beam detector for detecting an electron beam scattered by an object to be analyzed; an electron spectrometer for energy dispersing an electron beam transmitted through the object to be analyzed; an electron beam detector for detecting said dispersed electron beam; and a control unit for analyzing elements of the object to be analyzed based on an output signal of the electron beam detected by the electron beam detector and an output signal of the electron beam detected by the scattered electron beam detector. Further, the present invention exists in a scanning transmission electron microscope comprising the above ultimate analyzer; an electron beam source; an electron beam scanning coil; a scattered electron beam detector; objective lenses; a focusing lens; a magnifying magnetic field lens; and a focus adjusting electromagnetic lens. Furthermore, the ultimate analyzer or the scanning transmission electron microscope may comprises a control unit which makes it possible that both of an image of element distribution and an STEM image detected and formed by the scatted electron beam detector are observed at a time in real time, and the image of element distribution is corrected by the STEM image detected and formed by the scattered electron beam detector.
    • 本发明的目的是提供一种能够以高对比度显示待分析物体的元素分布图像,以高精度地确定元件分布的位置的最终分析器,以及扫描透射电子显微镜和 使用最终分析仪分析元素。 本发明存在于包含用于检测由待分析物体散射的电子束的散射电子束检测器的终极分析仪中; 用于能量分散通过待分析物体的电子束的电子光谱仪; 用于检测所述分散的电子束的电子束检测器; 以及控制单元,用于基于由电子束检测器检测的电子束的输出信号和由散射电子束检测器检测的电子束的输出信号来分析待分析物体的元件。 此外,本发明存在于包含上述极限分析仪的扫描透射电子显微镜中; 电子束源; 电子束扫描线圈; 散射电子束检测器; 物镜; 聚焦镜头; 放大磁场透镜; 和聚焦调整电磁透镜。 此外,最终分析器或扫描透射电子显微镜可以包括控制单元,其使得可以实时地观察由散射电子束检测器检测和形成的元件分布的图像和STEM图像两者, 并且通过由散射电子束检测器检测和形成的STEM图像校正元件分布的图像。