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1. 发明授权

US5565601A Process for producing phosphoric esters 失效
标题翻译：磷酸酯的制备方法
公开(公告)号：US5565601A
公开(公告)日：1996-10-15
申请号：US498697
申请日：1995-07-03
申请人： Takeshi Ihara , Shinji Yano , Katsumi Kita
发明人： Takeshi Ihara , Shinji Yano , Katsumi Kita
IPC分类号： C07F9/09
CPC分类号： C07F9/09
摘要： Phosphoric esters (mono-, di- or triester) is useful as, for example, a cleaner, an emulsifier, an antistatic agent, metal-chelating agent and a lubricant for fibers. It is produced at a high yield while completely trapping the hydrogen chloride gas formed as a by-product. The reaction between a phosphorus oxyhalide and an organic hydroxyl compound to produce a phosphoric ester is effected in the presence of a metal salt of an acid having a pKa of from -5 to 13.
摘要翻译：磷酸酯（单 - ，二 - 或三酯）可用作例如清洁剂，乳化剂，抗静电剂，金属螯合剂和纤维润滑剂。以高产率生产，同时完全捕获作为副产物形成的氯化氢气体。在产生磷酸酯的磷卤化物和有机羟基化合物之间的反应在pKa为-5至13的酸的金属盐存在下进行。

2. 发明授权

US5872272A Polyvalent metal salts of phosphoric diester and organo(poly)siloxanes modified with polyvalent metal salt of phosphoric diester 失效
标题翻译：磷酸二酯的多价金属盐和用磷酸二酯的多价金属盐改性的有机（聚）硅氧烷
公开(公告)号：US5872272A
公开(公告)日：1999-02-16
申请号：US454181
申请日：1995-06-15
申请人： Shinji Yano , Junichi Fukasawa , Hironori Kawasaki , Munehisa Okutsu , Takeshi Ihara , Katsumi Kita , Yoshiaki Fujikura , Akira Akaogi
发明人： Shinji Yano , Junichi Fukasawa , Hironori Kawasaki , Munehisa Okutsu , Takeshi Ihara , Katsumi Kita , Yoshiaki Fujikura , Akira Akaogi
IPC分类号： A61K8/55 , A61K8/893 , A61K8/896 , A61Q1/02 , A61Q17/04 , A61Q19/00 , A61Q19/10 , C07F7/08 , C07F9/09 , C07F9/6596 , C08G77/30 , C08G77/395 , C08G77/48 , C08G79/04
CPC分类号： C08G77/48 , A61K8/55 , A61K8/896 , A61Q19/00 , C07F9/091 , C07F9/092 , C07F9/6596 , C08G77/395 , A61Q1/02 , A61Q17/04
摘要： The present invention relates to polyvalent metal salts of a phosphoric diester represented by formula (1) and organo(poly)siloxanes modified with a polyvalent metal salt of a phosphoric diester having the structural units represented by formulae (9) and (10): ##STR1## wherein R.sup.1 represents a C1 to C20 linear or branched alkyl group, R.sup.2 and R.sup.4 are the same or different and independently represent a C2 to C3 linear or branched alkylene group, R.sup.3 represents a C3 to C20 linear or C5 to C20 branched alkylene group, A represents a group --COO-- or --O--, x and y are the same or different from each other and independently represent an integer of 0 to 10, L represents a C1 to C40 linear or branched alkyl group or a group, R.sup.1 --(OR.sup.2).sub.x --A--R.sup.3 (OR.sup.4).sub.y -- wherein R.sup.1, R.sup.2, R.sup.3, R.sup.4, A, x and y have the same meaning as defined herein before, M represents a divalent or polyvalent metal atom, and m represents the same value as the valence of M.
摘要翻译： PCT No.PCT / JP93 / 01924 Sec。 371日期：1995年6月15日 102（e）日期1995年6月15日PCT 1993年12月28日PCT PCT。公开号WO94 / 14822 日期：1994年7月7日本发明涉及由式（1）表示的磷酸二酯的多价金属盐和由具有式（9）所示的结构单元的磷酸二酯的多价金属盐改性的有机（聚）硅氧烷，（10）：其中R1表示C1〜C20直链或支链烷基，R2和R4相同或不同，并且独立地表示C2〜C3直链或支链亚烷基，R3表示C3〜C20 线性或C5至C20支链亚烷基，A表示基团-COO-或-O-，x和y彼此相同或不同，并且独立地表示0至10的整数，L表示C1至C40直链或支化烷基或基团，R1-（OR2）xA-R3（OR4）y-，其中R1，R2，R3，R4，A，x和y具有如前所定义的相同含义，M表示二价或多价金属原子，m表示与M的化合价相同的值。

3. 发明授权

US5530084A Organo(poly)siloxane modified with phosphoric ester and process for producing the same 失效
标题翻译：用磷酸酯改性的有机（聚）硅氧烷及其制备方法
公开(公告)号：US5530084A
公开(公告)日：1996-06-25
申请号：US392738
申请日：1995-03-06
申请人： Takeshi Ihara , Shinji Yano , Katsumi Kita , Yoshiaki Fujikura
发明人： Takeshi Ihara , Shinji Yano , Katsumi Kita , Yoshiaki Fujikura
IPC分类号： A61K8/58 , A61K8/893 , A61K8/896 , A61Q5/02 , A61Q5/12 , A61Q19/00 , A61Q19/10 , C07F9/09 , C08G77/30 , C08G77/395 , C08G77/04
CPC分类号： C08G77/395 , A61K8/585 , A61K8/896 , A61Q19/00 , C07F9/091 , C07F9/092 , A61Q19/10 , A61Q5/02 , A61Q5/12
摘要： The present invention relates to organo(poly)siloxanes modified by phosphates (including alkali metal salts thereof or the like) suitable as a component of cosmetics, and to a process for the manufacture of organo(poly)siloxanes modified by phosphates (including alkali metal salts thereof or the like) comprising reacting an organo(poly)siloxane having a group HO--(R.sup.4 O).sub.q --R.sup.5' --OR.sup.6).sub.r -- in its molecular chain, wherein R.sup.4 -R.sup.6 are alkylene groups, with an oxyhalogenated phosphorus; and further reacting it with an alkaline solution. These phosphate-modified organo(poly)siloxanes can stably emulsify silicone oils commonly used as cosmetic raw materials, irrespective of temperatures, and exhibit excellent compatibility with polar components and good foaming capability, so that they are suitable as a component of cosmetics such as skin cosmetics, skin detergents, hair cosmetics, hair detergents, and the like.
摘要翻译： PCT No.PCT / JP93 / 01279 Sec。 371日期：1995年3月6日 102（e）1995年3月6日PCT PCT 1993年9月9日PCT公布。第WO94 / 05720号公报日期：1994年3月17日本发明涉及适用于化妆品成分的磷酸盐（包括其碱金属盐等）改性的有机（聚）硅氧烷，以及制造有机（聚）硅氧烷的方法由磷酸盐（包括其碱金属盐等）修饰，包括在其分子链中使具有基团HO-（R4O）q-R5'-OR6）r-的有机（聚）硅氧烷，其中R 4 -R 6是亚烷基，与卤代磷; 并进一步与碱性溶液反应。这些磷酸酯改性的有机（聚）硅氧烷可以稳定地乳化通常用作化妆品原料的硅油，而不考虑温度，并且与极性组分具有优异的相容性和良好的发泡能力，因此它们适合作为化妆品如皮肤的组分化妆品，皮肤洗涤剂，头发化妆品，毛发洗涤剂等。

4. 发明授权

US5505936A Phosphoric diesters which absorb UV rays, method of preparing the same, and cosmetic compositions containing the same 失效
标题翻译：吸收紫外线的磷酸二酯，其制备方法和含有该紫外线的化妆品组合物
公开(公告)号：US5505936A
公开(公告)日：1996-04-09
申请号：US260310
申请日：1994-06-15
申请人： Shinji Yano , Munehisa Okutsu , Katsumi Kita , Yoshiaki Fujikura , Junichi Fukasawa
发明人： Shinji Yano , Munehisa Okutsu , Katsumi Kita , Yoshiaki Fujikura , Junichi Fukasawa
IPC分类号： A61K8/55 , A61Q17/04 , C07F9/09 , A61K7/42
CPC分类号： C07F9/091 , A61K8/55 , A61Q17/04 , Y10S514/844
摘要： Phosphoric diesters having formula (1): ##STR1## wherein R.sup.1 is an acyl group having at least one phenyl group; R.sup.2 is a C.sub.2-12 linear or branched alkylene group which may optionally be inserted with an oxygen atom between carbon atoms thereof; L is a C.sub.2-40 linear or branched alkyl group which may optionally be inserted with an oxygen atom between carbon atoms thereof or the group R.sup.1 -O-R.sup.2 ; M is a hydrogen atom, an alkali metal ion, a metal ion of di- or higher valence, an ammonium group, an alkanolammonium group having 2 to 14 carbon atoms, C.sub.1-14 alkylammonium group; and n is the valence of M are useful UV absorbing compounds. The phosphoric diesters remain on the skin for long periods of time and exhibit lasting UV shielding effects. The compounds and the cosmetic compositions containing the compounds are very safe to the skin.
摘要翻译：具有式（1）的磷酸二酯：一个苯基; R2是可以任选地在其碳原子之间插入氧原子的C2-12直链或支链亚烷基; L是可以任选地在其碳原子之间的氧原子或R1-O-R2基团上插入的C 2-40直链或支链烷基; M是氢原子，碱金属离子，二价或更高价的金属离子，铵基，具有2〜14个碳原子的链烷醇铵基，C 1-14烷基铵基; 并且n是M的化合价是有用的UV吸收化合物。磷酸二酯长时间保留在皮肤上，具有持久的紫外线屏蔽作用。含有这些化合物的化合物和化妆品组合物对皮肤非常安全。

5. 发明授权

US06299887B1 Phosphoric triesters and external compositions containing the same 失效
标题翻译：磷酸三酯和含有它们的外用组合物
公开(公告)号：US06299887B1
公开(公告)日：2001-10-09
申请号：US08606838
申请日：1996-02-26
申请人： Shinji Yano , Takashi Komori , Shinji Ishikawa , Katsumi Kita , Takashi Mizooku
发明人： Shinji Yano , Takashi Komori , Shinji Ishikawa , Katsumi Kita , Takashi Mizooku
IPC分类号： A61K700
CPC分类号： C07F9/09 , A61K8/0212 , A61K8/03 , A61K8/342 , A61K8/375 , A61K8/4926 , A61K8/55 , A61K8/675 , A61Q1/02 , A61Q1/06 , A61Q1/14 , A61Q5/00 , A61Q5/02 , A61Q19/00 , A61Q19/10
摘要： The present invention discloses phosphoric triesters represented by formula (1): wherein R1 represents C12-C24 alkyl or alkenyl, R2 represents C6-C24 alkyl, alkenyl, or aryl, and R3 represents C1-C6 alkyl, C2-C6 alkenyl, or aryl; external compositions containing the phosphoric triesters; and methods for preparing asymmetric phosphoric triesters. The compositions of the present invention have excellent compatibility with the skin, good sensation during use, and a high degree of safety.
摘要翻译：本发明公开了由式（1）表示的磷酸三酯：其中R1表示C12-C24烷基或烯基，R2表示C6-C24烷基，烯基或芳基，R3表示C1-C6烷基，C2-C6烯基或芳基 ; 含有磷酸三酯的外用组合物; 以及制备不对称磷酸三酯的方法。本发明的组合物具有优异的与皮肤的相容性，使用时的良好感觉和高度的安全性。

6. 发明授权

US6011071A Ether compound and process for producing the same 失效
标题翻译：醚化合物及其制备方法
公开(公告)号：US6011071A
公开(公告)日：2000-01-04
申请号：US952075
申请日：1997-11-17
申请人： Yasuyuki Fujii , Hisakazu Furugaki , Katsumi Kita , Hideharu Morimoto , Mitsuru Uno , Yasushi Kajihara
发明人： Yasuyuki Fujii , Hisakazu Furugaki , Katsumi Kita , Hideharu Morimoto , Mitsuru Uno , Yasushi Kajihara
IPC分类号： A61K8/33 , A61K8/58 , A61K8/81 , A61K31/08 , A61Q1/14 , A61Q19/10 , C07C41/01 , C07C41/05 , C07C43/04 , C07C43/10 , C07C43/11 , C07C43/184
CPC分类号： C07C43/184 , A61K8/33 , A61K8/585 , A61K8/8111 , A61Q1/14 , A61Q19/10 , C07C41/01 , C07C43/04 , C07C43/10 , C07C43/11 , C07C2101/14
摘要： To provide a novel ether compound which is useful such as an oil agent and a surfactant having the formula (I): R.sup.1 --O--(AO).sub.n --R.sup.2, wherein R.sup.1 is an alpha-branched alkyl group or an alkyl group having two or more branched chains or a cycloalkyl having 5 to 7 carbon atoms, R.sup.2 is an alkyl or alkenyl each being either branched or straight, each having 10 to 30 carbon atoms, A is an alkylene having 2 to 12 carbon atoms, n is a number from 0 to 30, A's being same as or different from one another.
摘要翻译： PCT No.PCT / JP96 / 01315 Sec。 371日期：1997年11月17日 102（e）日期1997年11月17日PCT提交1996年5月17日PCT公布。 WO96 / 36583 PCT出版物日期1996年11月21日提供一种有用的新型醚化合物，例如油剂和具有式（I）的表面活性剂：R1-O-（AO）n-R2，其中R1是α-支链烷基或具有2个以上支链或5〜7个碳原子的环烷基的烷基，R 2为分支或直链的烷基或烯基，各自具有10〜30个碳原子，A为碳原子数2〜12的亚烷基，n为0〜30的数，A相同或不同。

7. 发明授权

US06207845B1 Aluminum compounds and use thereof 有权
标题翻译：铝化合物及其用途
公开(公告)号：US06207845B1
公开(公告)日：2001-03-27
申请号：US09403765
申请日：1999-11-01
申请人： Munehisa Okutsu , Tomohito Kitsuki , Katsumi Kita
发明人： Munehisa Okutsu , Tomohito Kitsuki , Katsumi Kita
IPC分类号： C07F506
CPC分类号： B01J31/143 , B01J31/0212 , B01J31/0225 , B01J2231/40 , B01J2231/48 , C07C41/03 , C07C309/04 , C07C309/30 , C07C309/31 , C07C309/35 , C07C309/42 , C07F5/061 , C07F5/069 , C07C43/135 , C07C43/137 , C07C43/13
摘要： An aluminum compounds represented by the following general formula (1): Al(R1—SO3)1(R2)m(R3)n (1) wherein R1 is a hydrocarbon group which may be substituted, R2 is a hydrocarbon group which may be substituted, an aliphatic hydrocarbonoxy group which may be substituted, or a halogen atom, R3 is an aromatic hydrocarbonoxy group which may be substituted, and 1, m and n are independently a number of 0 to 3, with the proviso that 1+m+n equals 3, and 1 is not 0, an acid catalyst comprising the aluminum compound, and a process for producing an ester, acetal, ketal, ether or alkyl glycoside making use of the catalyst. The catalyst is suitable for use in a variety of acid-catalyzed reactions of alcohols, i.e., reactions with carbonyl compounds, such as esterification, transesterification, acetalization and ketalization, etherification, ring-opening reactions of epoxy compounds, etc. in addition to the above-described respective reactions, is not deactivated by alcoholysis, has a sufficient activity, can easily control a reaction catalyzed thereby and scarcely causes side reactions. Consequently, the use of the catalyst permits the production of the intended product at a high yield from starting materials used in an almost equimolar proportion.
摘要翻译：由以下通式（1）表示的铝化合物：其中R1是可被取代的烃基，R2是可被取代的烃基，可被取代的脂族烃氧基或卤素原子，R3是可以被取代的芳族烃氧基，并且1，m和n独立地为0-3的数，条件是1 + m + n等于3，并且1不为0，包含铝化合物的酸催化剂，以及利用催化剂生产酯，缩醛，缩酮，醚或烷基糖苷的方法。该催化剂适用于各种酸催化的醇反应，即与羰基化合物的反应，如酯化，酯交换，缩醛化和缩酮化，醚化，环氧化合物的开环反应等除了上述各自的反应之外，不通过醇解使其失活，具有足够的活性，可以容易地控制ar 因此催化，并且几乎不引起副反应。因此，使用催化剂允许以几乎等摩尔比例使用的起始材料从高产率生产所需产品。

8. 发明授权

US5801270A Amine derivative and detergent composition containing the same 失效
标题翻译：胺衍生物和含有它的洗涤剂组合物
公开(公告)号：US5801270A
公开(公告)日：1998-09-01
申请号：US646338
申请日：1996-06-13
申请人： Mitsuru Uno , Tomohito Kitsuki , Katsumi Kita , Yoshiaki Fujikura , Akiko Okutsu
发明人： Mitsuru Uno , Tomohito Kitsuki , Katsumi Kita , Yoshiaki Fujikura , Akiko Okutsu
IPC分类号： A61K8/00 , A61K8/40 , A61K8/42 , A61K8/44 , A61K8/46 , A61Q5/02 , A61Q5/12 , A61Q19/10 , C07C215/18 , C07C229/16 , C07C233/36 , C07C305/06 , C07C309/14 , C07C309/17 , C10M133/08 , C10N30/04 , C10N40/25 , C11D1/10 , C11D1/18 , C11D1/28 , C11D1/42 , C11D1/90 , C11D1/92 , C07C229/00 , C11D1/04 , C11D1/46
CPC分类号： C11D1/92 , A61K8/44 , A61K8/463 , A61K8/466 , A61Q19/10 , A61Q5/02 , A61Q5/12 , C07C215/18 , C07C233/36 , C07C305/06 , C07C309/17 , C11D1/10 , C11D1/18 , C11D1/28 , C11D1/42 , C11D1/90
摘要： The present invention relates to an amine derivative represented by the following general formula (1): ##STR1## wherein R.sup.2 and R.sup.3 mean individually an alkyl or alkenyl group which may have --OH and has 1-24 carbon atoms, A denotes an alkylene or alkenylene group which may have at least one --OH, --COOH or --SO.sub.3 H and has 1-6 carbon atoms, Y.sup.1 is --COOH, --SO.sub.3 H or --OSO.sub.3 H, Y.sup.2 means --OH, --OSO.sub.3 H or --OCO--A--COOH, n stands for a number of 0 or 1, and p is an integer of 1-8, or a salt or quaternized product thereof, and a detergent composition containing such a compound. This compound is low in irritativeness to the skin and hair and excellent in foamability, and can give a pleasant feeling to the user's skin and the like.
摘要翻译： PCT No.PCT / JP94 / 01923 Sec。 371日期：1996年6月13日 102（e）1996年6月13日PCT 1994年11月14日PCT PCT。出版物WO95 / 16664 日期：1995年6月22日本发明涉及由以下通式（1）表示的胺衍生物：其中R2和R3分别表示可以具有-OH并具有1-24的烷基或烯基碳原子，A表示可以具有至少一个-OH，-COOH或-SO 3 H并且具有1-6个碳原子的亚烷基或亚烯基，Y 1是-COOH，-SO 3 H或-OSO 3 H，Y 2表示-OH，-OSO 3 H 或-OCO-A-COOH，n表示0或1的数，p表示1-8的整数，或其盐或季铵化产物，以及含有该化合物的洗涤剂组合物。该化合物对皮肤和头发的刺激性低，起泡性优异，并且可以给使用者的皮肤等提供愉悦的感觉。

9. 发明授权

US5756784A Amides, method for preparing the amides, and detergent compositions containing the amides 失效
公开(公告)号：US5756784A
公开(公告)日：1998-05-26
申请号：US646767
申请日：1996-05-08
申请人： Mitsuru Uno , Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita
发明人： Mitsuru Uno , Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita
IPC分类号： A61K8/42 , A61Q5/02 , A61Q5/12 , A61Q19/00 , C07C233/05 , C07C233/36 , C07C233/47 , C07C303/22 , C07C303/30 , C07C305/06 , C07C309/15 , C11D1/52 , C11D3/32
CPC分类号： C11D3/32 , A61K8/42 , A61Q19/00 , A61Q19/10 , A61Q5/02 , C07C231/02 , C07C233/36 , C07C233/47 , C07C303/22 , C07C303/24 , C07C303/32 , C07C309/15 , C11D1/528 , A61Q5/12
摘要： An amide represented by the following formula (1): ##STR1## wherein R.sup.1 and R.sup.2 are C1-C24 alkyl, etc.; B is C2-C10 alkylene, etc.; A.sup.1 and A.sup.2 are C1-C6 alkylene, etc.; Y.sup.1 and Y.sup.2 are ##STR2## wherein R.sup.3, R.sup.4, and R.sup.5 are C1-C4 alkyl, etc., and X.sup.1 is halogen; or a salt of the amide and detergent compositions containing the amide or salt are mild to the skin or hair, provide a pleasant sensation to the skin or hair, and have excellent latherability and emulsion stability. These compounds are useful as components of various detergents and cosmetic compositions, emulsifiers, and conditioners.

10. 发明授权

US5429820A Cosmetic composition 失效
标题翻译：化妆品组成
公开(公告)号：US5429820A
公开(公告)日：1995-07-04
申请号：US865179
申请日：1992-04-08
申请人： Hiroshi Kamitani , Katsumi Kita , Yoshiaki Fujikura , Ryuuji Ochiai , Kazuyuki Yahagi
发明人： Hiroshi Kamitani , Katsumi Kita , Yoshiaki Fujikura , Ryuuji Ochiai , Kazuyuki Yahagi
IPC分类号： A61K8/02 , A61Q5/00 , A61Q5/12 , A61Q19/00 , C07C43/11 , C07C43/13 , C07C69/33 , C07H15/04 , C07H15/06 , C08G65/26 , C08G65/28 , C08G65/34 , C09K19/04 , A61K7/42
CPC分类号： A61Q19/00 , A61K8/0295 , C07C43/11 , C07C43/135 , C07C69/33 , C07H15/04 , C07H15/06 , C08G65/2606 , C08G65/34 , C09K19/04 , A61Q5/00 , A61Q5/12
摘要： A cosmetic composition comprises:(A) a nonionic amphipathic compound having in the molecule thereof at least one branched alkyl or alkenyl group having 10-36 carbon atoms and at least three hydroxyl groups, and having a lamellar liquid crystal structure itself at 25.degree. C. and at 50.degree. C. or higher; and(B) a compound represented by formula (1): ##STR1## wherein R.sup.1 is a hydrogen atom, a lower alkyl group or a group ##STR2## R.sup.2 is a hydrogen atom, a methyl group or a methoxy group; R.sup.3 is a direct bond or a saturated or unsaturated divalent hydrocarbon group having 1 to 3 carbon atoms; each Y and each Z are independently hydrogen atoms or hydroxyl groups; and p, q and r are each independently integers of 0 to 5, excepting the case where all of p, q and r are zero and Z is H, and the case where all of p, q and r are zero, R.sup.1 is H and Z is OH.
摘要翻译：化妆品组合物包含：（A）在分子中具有至少一个具有10-36个碳原子和至少三个羟基的支链烷基或烯基的非离子两亲化合物，并且在25℃下本身具有层状液晶结构在50℃以上; 和（B）由式（1）表示的化合物：其中R 1是氢原子，低级烷基或基团R 2是氢原子，甲基或甲氧基; R3是具有1至3个碳原子的直接键或饱和或不饱和的二价烃基; 每个Y和每个Z独立地为氢原子或羟基; p，q和r各自独立地为0〜5的整数，除了p，q和r全部为零，Z为H的情况以外，p，q，r全部为零的情况，R1为H Z是OH。

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