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1. 发明授权

US07438958B2 Sealant composition for liquid crystal and process for producing liquid-crystal display panel with the same 有权
标题翻译：用于液晶的密封剂组合物和用于制备具有该液晶显示面板的液晶显示面板的方法
公开(公告)号：US07438958B2
公开(公告)日：2008-10-21
申请号：US10531279
申请日：2003-10-24
申请人： Takahisa Miyawaki , Kenichi Yashiro , Kei Nagata
发明人： Takahisa Miyawaki , Kenichi Yashiro , Kei Nagata
IPC分类号： C09K19/54 , G02F1/1339 , C08G59/14 , C08L63/10 , C08L83/06
CPC分类号： C08G59/3254 , C08G59/306 , G02F1/1339 , G02F2202/025 , Y10T428/10 , Y10T428/1059 , Y10T428/1073
摘要： The present invention provides a liquid crystal sealing composition and a liquid crystal display panel excellent in adhesion, moisture permeation resistance and heat resistance and superior for use in a sheet press heating bonding system. The liquid crystal sealing composition comprises (1) an alkoxysilyl group-containing modified epoxy resin obtained by de-alcohol condensation reaction of (a) an epoxy resin having at least one hydroxyl group in one molecule and (b) an alkoxysilyl group-containing compound, (2) a heat latent epoxy curing agent, (3) a filler having an average particle diameter of 0.1 to 10 μm, and if necessary (4) an epoxy resin having at least 1.2 epoxy groups on average in one molecule, (5) an aprotic solvent having a boiling point in the range of 140 to 220° C., compatible with epoxy resin and inert to an epoxy group, and (6) other additives.
摘要翻译：本发明提供一种液晶密封组合物和粘合性，耐透湿性和耐热性优异的液晶显示面板，并且优于用于片材加压粘合体系的液晶显示面板。液晶密封组合物包含（1）通过（a）在一个分子中具有至少一个羟基的环氧树脂和（b）含烷氧基甲硅烷基的化合物的脱醇缩合反应获得的含烷氧基甲硅烷基的改性环氧树脂，（2）热潜环氧固化剂，（3）平均粒径为0.1〜10μm的填料，必要时（4）一分子中平均具有至少1.2个环氧基的环氧树脂（5 ）沸点在140-220℃范围内的非质子溶剂，与环氧树脂相容并且与环氧基惰性，和（6）其它添加剂。

2. 发明申请

US20070096056A1 One component resin composition curable with combination of light and heat and use of the same 审中-公开
标题翻译：通过光和热的组合可固化的单组分树脂组合物及其用途
公开(公告)号：US20070096056A1
公开(公告)日：2007-05-03
申请号：US10580852
申请日：2004-11-25
申请人： Fumito Takeuchi , Takahisa Miyawaki , Kenji Itou , Kenichi Yashiro , Kei Nagata , Souta Itou , Tazo Ikeguchi , Nobuo Sasaki , Makoto Nakahara
发明人： Fumito Takeuchi , Takahisa Miyawaki , Kenji Itou , Kenichi Yashiro , Kei Nagata , Souta Itou , Tazo Ikeguchi , Nobuo Sasaki , Makoto Nakahara
IPC分类号： C09K19/52
CPC分类号： C08F283/10 , C08G59/18 , C08L51/08 , G03F7/0007 , G03F7/027 , G03F7/038 , C08L2666/02
摘要： A one component resin composition curable with a combination of light and heat, which comprises (1) an epoxy resin, (2) an acrylic ester monomer and/or methacrylic ester monomer, or an oligomer thereof, (3) a latent epoxy curing agent, (4) a photo radical initiator, and (5) a compound having two or more thiol groups per molecule, wherein the ingredient (5) is contained in an amount of 0.001 to 5.0 parts by weight per 100 parts by weight of this resin composition. According to the present invention, a one component resin composition curable with a combination of light and heat, which has excellent curability especially in a light-shielded area can be provided. Also, a liquid crystal sealant composition curable with a combination of light and heat, which is applicable to the one-drop-fill method and has excellent curability in light-shielded areas and adhesion reliability, especially high-temperature and high-humidity adhesion reliability, can be provided.
摘要翻译：包含（1）环氧树脂，（2）丙烯酸酯单体和/或甲基丙烯酸酯单体或其低聚物的可光聚合组合的单组分树脂组合物，（3）潜在环氧固化剂，（4）光自由基引发剂，和（5）每分子具有两个以上硫醇基的化合物，其中成分（5）的含量相对于该树脂100重量份为0.001〜5.0重量份组成。根据本发明，可以提供特别是在遮光区域中具有优异固化性的组合可热固化的单组分树脂组合物。另外，适用于一滴填充法而且在遮光区域具有优异的固化性和粘合可靠性，尤其是高温高湿粘合可靠性的光和热组合可固化的液晶密封剂组合物，可以提供。

3. 发明申请

US20100022745A1 ONE COMPONENT RESIN COMPOSITION CURABLE WITH COMBINATION OF LIGHT AND HEAT AND USE OF THE SAME 审中-公开
标题翻译：一种组分树脂组合物，可与光和热的组合固化并使用它们
公开(公告)号：US20100022745A1
公开(公告)日：2010-01-28
申请号：US12572420
申请日：2009-10-02
申请人： Fumito Takeuchi , Takahisa Miyawaki , Kenji Itou , Kenichi Yashiro , Kei Nagata , Souta Itou , Tazo Ikeguchi , Nobuo Sasaki , Makoto Nakahara
发明人： Fumito Takeuchi , Takahisa Miyawaki , Kenji Itou , Kenichi Yashiro , Kei Nagata , Souta Itou , Tazo Ikeguchi , Nobuo Sasaki , Makoto Nakahara
IPC分类号： C08G65/04
CPC分类号： C08F283/10 , C08G59/18 , C08L51/08 , G03F7/0007 , G03F7/027 , G03F7/038 , C08L2666/02
摘要： A one component resin composition curable with a combination of light and heat, which comprises (1) an epoxy resin, (2) an acrylic ester monomer and/or methacrylic ester monomer, or an oligomer thereof, (3) a latent epoxy curing agent, (4) a photo radical initiator, and (5) a compound having two or more thiol groups per molecule, wherein the ingredient (5) is contained in an amount of 0.001 to 5.0 parts by weight per 100 parts by weight of this resin composition. According to the present invention, a one component resin composition curable with a combination of light and heat, which has excellent curability especially in a light-shielded area can be provided. Also, a liquid crystal sealant composition curable with a combination of light and heat, which is applicable to the one-drop-fill method and has excellent curability in light-shielded areas and adhesion reliability, especially high-temperature and high-humidity adhesion reliability, can be provided.
摘要翻译：包含（1）环氧树脂，（2）丙烯酸酯单体和/或甲基丙烯酸酯单体或其低聚物的可光聚合组合的单组分树脂组合物，（3）潜在环氧固化剂，（4）光自由基引发剂，和（5）每分子具有两个以上硫醇基的化合物，其中成分（5）的含量相对于该树脂100重量份为0.001〜5.0重量份组成。根据本发明，可以提供特别是在遮光区域中具有优异固化性的组合可热固化的单组分树脂组合物。另外，可以适用于一滴填充法并且在遮光区域中具有优异的固化性和粘合可靠性，特别是高温高湿附着可靠性的光和热组合可固化的液晶密封剂组合物，可以提供。

4. 发明授权

US07566377B2 Liquid crystal sealing agent composition and manufacturing method of liquid crystal display panel using the same 有权
标题翻译：液晶密封剂组成及其制造方法采用液晶显示面板
公开(公告)号：US07566377B2
公开(公告)日：2009-07-28
申请号：US10528196
申请日：2003-09-19
申请人： Takahisa Miyawaki , Yasushi Mizuta , Fumito Takeuchi , Kenji Itou , Tadashi Kitamura , Hiroyuki Asakura , Kenichi Yashiro , Kei Nagata
发明人： Takahisa Miyawaki , Yasushi Mizuta , Fumito Takeuchi , Kenji Itou , Tadashi Kitamura , Hiroyuki Asakura , Kenichi Yashiro , Kei Nagata
IPC分类号： B32B38/04 , C08L63/00
CPC分类号： C08G59/18 , C08F283/10 , G02F1/1339
摘要： A liquid crystal sealing agent composition that is a one-component light and heat-curable resin composition containing: (1) a solid epoxy resin having a ring and ball method softening temperature of 40° C. or above; (2) an acrylate monomer and/or a methacrylate monomer, or an oligomer thereof; (3) a thermoplastic polymer having a ring and ball method softening temperature of 50 to 120° C., the thermoplastic polymer being obtained by copolymerizing an acrylate monomer and/or a methacrylate monomer with a monomer copolymerizable therewith; (4) a light-activated radical polymerization initiator; and (5) a latent epoxy curing agent. The light and heat curable liquid crystal sealing agent composition is employable in one drop fill, is excellent in properties of a cured product particularly after first-stage light curing, achieves stable cell gap after cell gap formation, permits prevention of contamination of the liquid crystal in second-stage heat curing, is excellent in curing properties in shaded area, and shows superior bonding reliability.
摘要翻译：一种液晶密封剂组合物，其是单组分的光热可固化树脂组合物，其包含：（1）环球法软化温度为40℃以上的固体环氧树脂; （2）丙烯酸酯单体和/或甲基丙烯酸酯单体或其低聚物; （3）具有环球法软化温度为50〜120℃的热塑性聚合物，所述热塑性聚合物通过使丙烯酸酯单体和/或甲基丙烯酸酯单体与可共聚合的单体共聚而得到; （4）光活化自由基聚合引发剂; 和（5）潜在环氧固化剂。光热固化型液晶密封剂组合物可以在一个滴液填充中使用，特别是在第一阶段光固化之后，固化产物的性能优异，在电池间隙形成之后实现稳定的电池间隙，可以防止液晶的污染在第二阶段热固化中，阴影区域的固化性优异，粘接可靠性优异。

5. 发明申请

US20060009579A1 Sealing composition for liquid crystal displays and process for production of liquid crystal display panels 有权
标题翻译：用于液晶显示器的密封组合物和制造液晶显示面板的方法
公开(公告)号：US20060009579A1
公开(公告)日：2006-01-12
申请号：US10528196
申请日：2003-09-19
申请人： Takahisa Miyawaki , Yasushi Mizuta , Fumito Takeuchi , Kenji Itou , Tadashi Kitamura , Hiroyuki Asakura , Kenichi yashiro , Kei Nagata
发明人： Takahisa Miyawaki , Yasushi Mizuta , Fumito Takeuchi , Kenji Itou , Tadashi Kitamura , Hiroyuki Asakura , Kenichi yashiro , Kei Nagata
IPC分类号： C08G59/00 , B32B37/00
CPC分类号： C08G59/18 , C08F283/10 , G02F1/1339
摘要： A liquid crystal sealing agent composition that is a one-component light and heat-curable resin composition containing: (1) a solid epoxy resin having a ring and ball method softening temperature of 40° C. or above; (2) an acrylate monomer and/or a methacrylate monomer, or an oligomer thereof; (3) a thermoplastic polymer having a ring and ball method softening temperature of 50 to 120° C., the thermoplastic polymer being obtained by copolymerizing an acrylate monomer and/or a methacrylate monomer with a monomer copolymerizable therewith; (4) a light-activated radical polymerization initiator; and (5) a latent epoxy curing agent. The light and heat curable liquid crystal sealing agent composition is employable in one drop fill, is excellent in properties of a cured product particularly after first-stage light curing, achieves stable cell gap after cell gap formation, permits prevention of contamination of the liquid crystal in second-stage heat curing, is excellent in curing properties in shaded area, and shows superior bonding reliability.
摘要翻译：一种液晶密封剂组合物，其是单组分的光热可固化树脂组合物，其包含：（1）环球法软化温度为40℃以上的固体环氧树脂; （2）丙烯酸酯单体和/或甲基丙烯酸酯单体或其低聚物; （3）具有环球法软化温度为50〜120℃的热塑性聚合物，所述热塑性聚合物通过使丙烯酸酯单体和/或甲基丙烯酸酯单体与可共聚合的单体共聚而得到; （4）光活化自由基聚合引发剂; 和（5）潜在环氧固化剂。光热固化型液晶密封剂组合物可以在一个滴液填充中使用，特别是在第一阶段光固化之后，固化产物的性能优异，在电池间隙形成之后实现稳定的电池间隙，可以防止液晶的污染在第二阶段热固化中，阴影区域的固化性优异，粘接可靠性优异。

6. 发明申请

US20060006362A1 Sealant composition for liquid crystal and process for producing liquid-crystal display panel with the same 有权
标题翻译：用于液晶的密封剂组合物和用于制备具有该液晶显示面板的液晶显示面板的方法
公开(公告)号：US20060006362A1
公开(公告)日：2006-01-12
申请号：US10531279
申请日：2003-10-24
申请人： Takahisa Miyawaki , Kenichi Yashiro , Kei Nagata
发明人： Takahisa Miyawaki , Kenichi Yashiro , Kei Nagata
IPC分类号： C09K19/52 , C09K19/54 , C09K19/00
CPC分类号： C08G59/3254 , C08G59/306 , G02F1/1339 , G02F2202/025 , Y10T428/10 , Y10T428/1059 , Y10T428/1073
摘要： The present invention provides a liquid crystal sealing composition and a liquid crystal display panel excellent in adhesion, moisture permeation resistance and heat resistance and superior for use in a sheet press heating bonding system. The liquid crystal sealing composition comprises (1) an alkoxysilyl group-containing modified epoxy resin obtained by de-alcohol condensation reaction of (a) an epoxy resin having at least one hydroxyl group in one molecule and (b) analkoxysilyl group-containing compound, (2) a heat latent epoxy curing agent, (3) a filler having an average particle diameter of 0.1 to 10 μm, and if necessary (4) an epoxy resin having at least 1.2 epoxy groups on average in one molecule, (5) an aprotic solvent having a boiling point in the range of 140 to 220° C., compatible with epoxy resin and inert to an epoxy group, and (6) other additives.
摘要翻译：本发明提供一种液晶密封组合物和粘合性，耐透湿性和耐热性优异的液晶显示面板，并且优于用于片材加压粘合体系的液晶显示面板。液晶密封组合物包含（1）通过（a）在一分子中具有至少一个羟基的环氧树脂和（b）含有烷氧基甲硅烷基的化合物的脱醇缩合反应获得的含烷氧基甲硅烷基的改性环氧树脂，（2）热潜环氧固化剂，（3）平均粒径为0.1〜10μm的填料，必要时（4）一分子中平均具有至少1.2个环氧基的环氧树脂，（5）沸点在140〜220℃范围内的非质子溶剂，与环氧树脂相容，与环氧基呈惰性，（6）其它添加剂。

7. 发明授权

US06333380B1 Thermosetting resin composition for powder paint and thermosetting powder paint composition using the same 有权
标题翻译：用于粉末涂料和热固性粉末涂料组合物的热固性树脂组合物使用该组合物
公开(公告)号：US06333380B1
公开(公告)日：2001-12-25
申请号：US09495895
申请日：2000-02-02
申请人： Hiroyuki Sakayama , Yoshio Kikuta , Mitsuyuki Mizoguchi , Takahisa Miyawaki , Tsuyoshi Matsumoto
发明人： Hiroyuki Sakayama , Yoshio Kikuta , Mitsuyuki Mizoguchi , Takahisa Miyawaki , Tsuyoshi Matsumoto
IPC分类号： C08G6348
CPC分类号： C08G81/021
摘要： There are disclosed a thermosetting resin composition for a powder paint in which a resin composition component (A) is a (block) copolymer obtained by allowing a vinyl-based polymer G (branch) block (component (a-1)) to graft-react with a vinyl-based polymer S (back bone) block (component (a-2)), and if the solubility parameters of the components (a-1) and (a-2) are represented by SPG and SPG, respectively, SPG and SPS satisfy the following numerical formula (I), and a thermosetting powder paint composition comprising a resin composition component (A) and a hardener composition component (B) wherein the component (A) is said thermosetting resin composition for a powder paint. By these compositions, a thermosetting powder paint composition having excellent storage stabilities, appearance properties, physical properties and chemical properties can be provided. Particularly, there can be provided a thermosetting powder paint composition suitably applied to painting of bodies of vehicles such as automobiles and parts of vehicles such as automobiles (aluminum wheel, wiper, pillar, door handle, fender, bonnet, air spoiler, stabilizer, front grill and the like), particularly, to top painting. SPG
摘要翻译：公开了一种粉末涂料用热固性树脂组合物，其中树脂组合物组分（A）是通过使乙烯基类聚合物G（分支）嵌段（组分（a-1））接枝而获得的（嵌段）共聚物，与乙烯基类聚合物S（背面骨）嵌段（成分（a-2））反应，如果成分（a-1）和（a-2）的溶解度参数分别用SPG和SPG表示， SPG和SPS满足以下数值式（I），和包含树脂组合物组分（A）和硬化剂组合物组分（B）的热固性粉末涂料组合物，其中组分（A）是所述粉末涂料用热固性树脂组合物。通过这些组合物，可以提供具有优异的储存稳定性，外观性质，物理性质和化学性质的热固性粉末涂料组合物。特别地，可以提供一种适用于汽车，汽车等车辆（铝轮，刮水器，支柱，门把手，挡泥板，发动机罩，空气扰流板，稳定器，前部等）的车体的涂装的热固性粉末涂料组合物格栅等），特别是顶画。

8. 发明授权

US6121378A Thermosetting powder paint composition 有权
标题翻译：热固性粉末涂料组成
公开(公告)号：US6121378A
公开(公告)日：2000-09-19
申请号：US136290
申请日：1998-08-19
申请人： Takahisa Miyawaki , Yoshio Kikuta , Mitsuyuki Mizoguchi , Hiroyuki Sakayama , Tsuyoshi Matsumoto
发明人： Takahisa Miyawaki , Yoshio Kikuta , Mitsuyuki Mizoguchi , Hiroyuki Sakayama , Tsuyoshi Matsumoto
IPC分类号： C08L83/04 , C09D133/06 , C08F8/00
CPC分类号： C09D133/068 , C08L83/04
摘要： A thermosetting powder paint composition for top coating excellent in weather resistance and storage stability, which comprising 100 parts by weight of an acrylic copolymer (A) having an epoxy group, and 0.01 to 2.0 parts by weight of an organic modified polysiloxane (B) containing at least one functional group, at least two silicon atoms and no radical-polymerizable unsaturated bond wherein the component (B) is contained in the condition that a part or all thereof has reacted and bonded with the component (A) or the component (C), or all thereof has not reacted with them.
摘要翻译：包含100重量份具有环氧基的丙烯酸共聚物（A）和0.01〜2.0重量份含有有机改性聚硅氧烷（B）的耐候性和保存稳定性优异的顶涂层用热固性粉末涂料组合物，其含有至少一个官能团，至少两个硅原子和无自由基聚合性不饱和键，其中组分（B）的一部分或全部与组分（A）或组分（C ），或其全部未与其反应。

9. 发明授权

US6084009A Powder paint compositions 失效
标题翻译：粉末涂料组合物
公开(公告)号：US6084009A
公开(公告)日：2000-07-04
申请号：US839104
申请日：1997-04-23
申请人： Mitsuyuki Mizoguchi , Yoshiro Fuseya , Yoshihiro Fujita , Yukiatsu Ishino , Masashi Seki , Takahisa Miyawaki
发明人： Mitsuyuki Mizoguchi , Yoshiro Fuseya , Yoshihiro Fujita , Yukiatsu Ishino , Masashi Seki , Takahisa Miyawaki
IPC分类号： C08L51/04 , C09D133/06 , C08L33/00
CPC分类号： C09D133/068 , C08L51/04 , Y10S524/904 , Y10S525/902 , Y10S525/934
摘要： A thermosetting powder paint composition comprising:(A) a (meth)acrylic copolymer having glycidyl groups;(B) a polybasic carboxylic acid and/or polybasic carboxylic anhydride; and(C) particles having a core/shell structure each comprising a core having Tg of 20.degree. C. or below, the core being covered at least partially with a shell having Tg of 40.degree. C. or above, and said shell having no glycidyl group.The paint composition is excellent in weather resistance as well as in impact resistance and chipping resistance.
摘要翻译：一种热固性粉末涂料组合物，其包含：（A）具有缩水甘油基的（甲基）丙烯酸共聚物; （B）多元羧酸和/或多元羧酸酐; 和（C）具有核/壳结构的颗粒，每个颗粒包含Tg为20℃或更低的芯，所述芯至少部分地被Tg覆盖在40℃以上的壳体上，并且所述壳体没有缩水甘油基。涂料组合物的耐候性以及耐冲击性和耐崩裂性优异。

10. 发明授权

US06388012B1 Thermosetting powder resin composition 有权
标题翻译：热固性粉末树脂组合物
公开(公告)号：US06388012B1
公开(公告)日：2002-05-14
申请号：US09543089
申请日：2000-04-04
申请人： Hiroyuki Sakayama , Yoshio Kikuta , Mitsuyuki Mizoguchi , Takahisa Miyawaki , Tsuyoshi Matsumoto
发明人： Hiroyuki Sakayama , Yoshio Kikuta , Mitsuyuki Mizoguchi , Takahisa Miyawaki , Tsuyoshi Matsumoto
IPC分类号： C08L2300
CPC分类号： C09D5/037
摘要： A thermosetting powder paint composition comprising (A) a resin composition component, (B) a hardener component and (C) a solid flow controlling component, wherein the component (A) contains a resin composition component having reactivity with the component (B), the component (B) contains a hardener having reactivity with the component (A), the component (C) contains a vinyl polymer which is solid at 20° C., and the relation between SPA of the component (A) and SPC of the component (C) satisfies the following numerical formula (1) and the following numerical formula (2) simultaneously. By this constitution, excellent blocking-resistance in storing as the powder paint composition and excellent appearance properties of a paint film formed by coating the powder paint composition can be simultaneously manifested. 8≦SPA≦13 (1) 7≦SPC≦SPA (2).
摘要翻译：一种热固性粉末涂料组合物，其包含（A）树脂组合物组分，（B）固化剂组分和（C）固体流动控制组分，其中组分（A）含有与组分（B）具有反应性的树脂组合物组分，组分（B）含有与组分（A）具有反应性的固化剂，组分（C）含有在20℃下为固体的乙烯基聚合物，组分（A）的SPA与SPC之间的关系组分（C）同时满足以下数学式（1）和以下数值式（2）。通过这种结构，可以同时表现出通过涂覆粉末涂料组合物形成的涂膜作为粉末涂料组合物的优异的耐粘连性和优异的外观性能。

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