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1. 发明授权

US4664936A Aromatic polyamide fiber-based composite prepreg 失效
标题翻译：芳香族聚酰胺纤维复合预浸料
公开(公告)号：US4664936A
公开(公告)日：1987-05-12
申请号：US816309
申请日：1986-01-06
申请人： Susumu Ueno , Shigehiro Hoshida , Hirokazu Nomura
发明人： Susumu Ueno , Shigehiro Hoshida , Hirokazu Nomura
IPC分类号： B29B15/08 , B29C59/14 , C08J5/06 , D06M10/02 , B05D3/06
CPC分类号： B29B15/08 , B29C59/14 , C08J5/06 , D06M10/025 , B29K2105/08 , B29K2277/00 , D06M2101/36 , D06M2200/50
摘要： The resin-impregnated composite prepreg based on a fabric material of an aromatic polyamide fiber is prepared by exposing the fabric material to low temperature plasma generated in an atmosphere of an inorganic gas, which is preferably oxygen or an oxygen-containing gaseous mixture, under a pressure of 0.5 to 5 Torr to such an extent that ruggedness of 0.01 to 0.5 .mu.m is formed on the surface and then impregnating the fabric material with an organic resinous binder. The adhesive bonding strength between the binder and the fiber surface can further be increased when the plasma-treated fabric material is brought into contact with an unsaturated compound polymerizable by free radical polymerization without contacting with air so as to form a graft-polymerized layer on the fiber surface.
摘要翻译：基于芳族聚酰胺纤维的织物材料的树脂浸渍的复合预浸料通过将织物材料暴露于无机气体（其优选为氧或含氧气体混合物）的气氛中产生的低温等离子体来制备，压力为0.5〜5托，至表面形成0.01〜0.5微米的凹凸，然后用有机树脂粘合剂浸渍织物。当等离子体处理的织物材料与通过自由基聚合可聚合的不饱和化合物接触而不与空气接触以在粘合剂和纤维表面之间形成接枝聚合层时，可以进一步增加粘合剂和纤维表面之间的粘合强度纤维表面。

2. 发明授权

US4824717A Mesh screen of polyester filaments for screen printing 失效
标题翻译：涤丝丝网丝网印花
公开(公告)号：US4824717A
公开(公告)日：1989-04-25
申请号：US137321
申请日：1987-12-23
申请人： Toru Nakanishi , Shigehiro Hoshida , Susumu Ueno
发明人： Toru Nakanishi , Shigehiro Hoshida , Susumu Ueno
IPC分类号： B29C59/14 , B41N1/24 , B32B7/00
CPC分类号： B29C59/14 , B41N1/247 , Y10T428/2938 , Y10T428/2969 , Y10T428/2978 , Y10T428/31 , Y10T442/183 , Y10T442/3976
摘要： A mesh screen of polyester filaments for screen printing is subjected to a treatment with low temperature plasma in an atmosphere of a non-oxidizing inorganic gas to such an extent that a crosslinked layer having a thickness of 0.001 to 0.1 .mu.m is formed on the surface of the polyester filaments and the surface of the filaments is provided with protrusions and concavities having a diameter of 0.01 to 0.1 .mu.m in a distribution density of 1000 to 6000 per .mu.m.sup.2 of the surface area of the filament. The thus treated mesh screen is advantageously improved, with no adverse influences on the mechanical strength, in respect of the adhesion between the filament surface and a photosensitive resin composition applied to the mesh screen for photolithographic patterning. The plasmatreated mesh screen is also advantageous in respect of the decreased resistance against transfer of a printing ink through open meshes.
摘要翻译：用于丝网印刷的聚酯长丝的筛网在非氧化性无机气体的气氛中用低温等离子体进行处理，使得在表面上形成厚度为0.001〜0.1μm的交联层的聚酯长丝和长丝的表面在细丝的表面积的分布密度为1000〜6000 /μm的情况下，设置有直径为0.01〜0.1μm的突起和凹部。有利地，这样处理的筛网有利地提高了对于在丝网表面和施加到用于光刻图案的网筛之间的感光性树脂组合物之间的粘合力对机械强度没有不利影响。等离子体处理的筛网对于通过开放的网孔转印印刷油墨的抗性降低也是有利的。

3. 发明授权

US4722816A Method for the preparation of shaped articles of a vinyl chloride-based resin having improved surface properties 失效
标题翻译：用于制备具有改善的表面性质的氯乙烯基树脂的成形制品的方法
公开(公告)号：US4722816A
公开(公告)日：1988-02-02
申请号：US865474
申请日：1986-05-21
申请人： Susumu Ueno , Shigehiro Hoshida , Kouiti Kuroda , Kenji Fushimi
发明人： Susumu Ueno , Shigehiro Hoshida , Kouiti Kuroda , Kenji Fushimi
IPC分类号： B29C59/00 , B29C59/14 , B29C71/04 , B29K27/06 , C08J7/00 , C08K9/00 , C08K9/04 , C08K9/06 , C08L1/00 , C08L27/00 , C08L27/06 , C08L33/00 , C08L33/02 , C08L63/00
CPC分类号： C08K9/04 , B29C59/005 , C08K9/06 , B29C59/14 , B29K2027/06
摘要： A vinyl chloride-based resin is compounded with a filler, e.g. calcium carbonate, having been treated on the surface with an epoxy compound such as 3-glycidyloxypropyl trimethoxy silane in advance and the resin composition is shaped into an article which is then subjected to a low temperature plasma treatment. The thus obtained shaped article is imparted with remarkably improved surface properties such as decrease in the phenomenon of plasticizer bleeding and the effect is very durable even after prolonged outdoor exposure of the article.
摘要翻译：氯乙烯类树脂与填料混合，例如预先用诸如3-缩水甘油氧基丙基三甲氧基硅烷的环氧化合物在表面上处理过的碳酸钙，并将树脂组合物成形为制品，然后进行低温等离子体处理。如此得到的成形制品被赋予显着改善的表面性能，例如增塑剂渗色现象的降低，并且即使在长时间的室外暴露于制品之后，效果也非常耐用。

4. 发明授权

US5210158A Suspension polymerization of vinyl chloride with heating of reactor surfaces 失效
标题翻译：乙烯基氯化锂与反应器表面加热的悬浮聚合
公开(公告)号：US5210158A
公开(公告)日：1993-05-11
申请号：US741652
申请日：1991-08-07
申请人： Tadashi Amano , Shigehiro Hoshida , Yoshihiro Shirota
发明人： Tadashi Amano , Shigehiro Hoshida , Yoshihiro Shirota
IPC分类号： C08F2/00 , C08F2/18 , C08F2/20 , C08F14/00 , C08F14/06
CPC分类号： C08F2/002 , C08F14/06
摘要： An improvement is proposed in the process of suspension polymerizatiopn of vinyl chloride monomer in an aqueous polymerization medium, by which a resin product of high quality relative to the contents of foamy resin and fish-eyes can be produced in a high efficiency with little deposition of polymer scale on the reactor walls. The improvment comprises heating and keeping the surfaces of the polymerization reactor and accessory equipment coming into contact with the gaseous phase above the polymerization mixture at a temperature of 55.degree. C. or higher during a period starting from a moment when the temperature of the polymerization mixture under temperature elevation up to the polymerization temperature is still 45.degree. C. or lower to a moment when conversion of the monomer into polymer is at least 10% so that foaming on the polymerization mixture can be greatly reduced.

5. 发明授权

US5118741A Vinyl chloride resin compositions used for food containers and food packing materials 失效
标题翻译：用于食品容器和食品包装材料的氯乙烯树脂组合物
公开(公告)号：US5118741A
公开(公告)日：1992-06-02
申请号：US755608
申请日：1991-09-05
申请人： Tadashi Amano , Shigehiro Hoshida
发明人： Tadashi Amano , Shigehiro Hoshida
IPC分类号： C08F14/06 , C08L9/06 , C08L25/10 , C08L27/06 , C08L51/04
CPC分类号： C08F14/06 , C08L27/06 , C08K5/57 , C08K5/58 , C08L29/04 , C08L51/04
摘要： Such food packing materials as heat shrinkable films or such formed containers for food as bottles are manufatured by forming resin compositions of the following compostions: (a) 100 weight parts of vinyl chloride based resin obtained by adding 0.005 to 0.5 weight parts of partially saponified polyvinyl alcohol, degree of saponification 20-55 mol %, means degree of polymerization 150-600, to 100 weight parts of loaded vinyl chloride monomer or a mixture of vinyl based monomer with vinyl chloride as main, during suspension-polymerizing in an aqueous medium under the existence of 0.03-0.08 weight parts of partially saponified polyvinyl alcohol, degree of saponification 65-80 mol %, means degree of polymerization 600-1000, or else in slurry after completion of the suspension-polymerizing: (b) 0.3 to 5 weight parts of non-toxic stabilizer for food which is a liquid composite stabilizer; and (c) 4 to 15 weigth parts of butadiene-styrene based copolymer resin. The food packing materials are resistant to whitening of their surface caused either by contact with water, alcohol, aqueous water of alcohol or incubation for prolonged time under a high temperature and high humidity atmosphere, thus enabling an improvement in their quality.
摘要翻译：通过形成以下组合物的树脂组合物来制造作为热收缩膜或这种用于食品的瓶子形成的容器的食品包装材料：（a）将100重量份的氯乙烯基树脂通过加入0.005至0.5重量份的部分皂化的聚乙烯酒精，皂化度20-55mol％，指聚合度150-600至100重量份负载的氯乙烯单体或乙烯基单体与氯乙烯的混合物，在悬浮聚合过程中在水性介质中存在0.03-0.08重量份的部分皂化聚乙烯醇，皂化度为65-80摩尔％，意味着聚合度600-1000，或者在悬浮聚合完成后的浆料中：（b）0.3-5重量份作为液体复合稳定剂的食品无毒稳定剂的一部分; 和（c）丁二烯 - 苯乙烯基共聚物树脂的4至15重量份。食品包装材料通过与水，酒精，酒精水溶液接触或者在高温高湿气氛下长时间孵育，可以抵抗其表面的美白，从而能够提高其质量。

6. 发明授权

US5100988A Initiated scale-free formation of vinyl chloride polymers using washing liquid at temperature affecting initiator half-life 失效
标题翻译：使用洗涤液在温度影响发动机半衰期的情况下自动形成乙烯基氯化聚合物
公开(公告)号：US5100988A
公开(公告)日：1992-03-31
申请号：US494325
申请日：1990-03-16
申请人： Tadashi Amano , Shigehiro Hoshida
发明人： Tadashi Amano , Shigehiro Hoshida
IPC分类号： C08F14/06
CPC分类号： C08F14/06
摘要： A method for preparing vinyl chloride polymers which comprises polymerizing vinyl chloride monomer or a vinylic monomer mixture mainly composed of vinyl chloride in an aqueous medium in the presence of a polymerization initiator, characterized by washing a piping and an opening of a polymerizer, for charging the polymerization initiator into the polymerizer, with water, steam or a washing liquid capable of lowering the half-life of the polymerization initiator to not more than 30 minutes after introducing the initiator into the polymerizer. The method makes it possible to eliminate the formation of polymer scales on the piping and the opening for charging the polymerization initiator into a polymerizer and, therefore, the yield of the vinyl chloride polymers can greatly improved and the production cost can be substantially saved. Moreover, the polymer product does not include any materials used for washing said portions and thus polymer product of high quality can be provided in a high yield.
摘要翻译：一种制备氯乙烯聚合物的方法，其包括在聚合引发剂存在下，在水性介质中聚合氯乙烯单体或主要由氯乙烯组成的乙烯基单体混合物，其特征在于，清洗管道和聚合反应器的开口，将聚合引发剂引入聚合反应器中，与引入剂引入聚合反应器中的水，蒸汽或能够将聚合引发剂的半衰期降至不超过30分钟的洗涤液。该方法可以消除管道上的聚合物垢的形成和将聚合引发剂加入聚合反应器的开口，从而可大大提高氯乙烯聚合物的收率，并且可以显着节省生产成本。此外，聚合物产品不包括用于洗涤所述部分的任何材料，因此可以高产率提供高质量的聚合物产品。

7. 发明授权

US5064917A Process of polymerizing vinyl chloride with washing of charging passage 失效
标题翻译：洗涤充电通道聚合氯乙烯的工艺
公开(公告)号：US5064917A
公开(公告)日：1991-11-12
申请号：US462972
申请日：1990-01-05
申请人： Tadashi Amano , Shigehiro Hoshida
发明人： Tadashi Amano , Shigehiro Hoshida
IPC分类号： C08F2/00 , C08F2/20 , C08F14/00 , C08F14/06
CPC分类号： C08F14/06
摘要： A process of preparing a vinyl chloride polymer in a polymerization vessel comprising the steps of:charging a polymerization initiator through a charging passage communicating with the inside of the polymerization vessel, andpolymerizing vinyl chloride or a vinyl monomer mixture containing vinyl chloride in an aqueous medium,wherein after said polymerization initiator has been charged into the polymerization vessel, said charging passage is washed with a cleaning fluid containing a polymerization inhibitor. This process can effectively prevent scale formation in the charging passage and produce a vinyl chloride polymer of high quality.
摘要翻译：一种在聚合容器中制备氯乙烯聚合物的方法，包括以下步骤：通过与聚合容器内部连通的加料通道加入聚合引发剂，并在含水介质中聚合氯乙烯或含有氯乙烯的乙烯基单体混合物其中在所述聚合引发剂已经装入聚合容器中之后，用含有阻聚剂的清洗液洗涤所述充电通道。该方法可以有效地防止充电通道中的结垢形成并产生高质量的氯乙烯聚合物。

8. 发明授权

US07524394B2 Flame retardant adhesive composition, and adhesive sheet, coverlay film and flexible copper-clad laminate using same 失效
标题翻译：阻燃粘合剂组合物，粘合片，覆盖膜和使用其的柔性覆铜层压板
公开(公告)号：US07524394B2
公开(公告)日：2009-04-28
申请号：US11401854
申请日：2006-04-12
申请人： Toru Nakanishi , Kazunori Kondo , Shigehiro Hoshida , Tadashi Amano
发明人： Toru Nakanishi , Kazunori Kondo , Shigehiro Hoshida , Tadashi Amano
IPC分类号： B32B37/12 , B32B27/38 , C08L63/00 , C09J163/00
CPC分类号： H05K3/386 , B32B7/12 , B32B15/06 , B32B15/092 , B32B15/16 , B32B15/20 , B32B25/08 , B32B25/16 , B32B27/08 , B32B27/18 , B32B27/26 , B32B27/38 , B32B2264/104 , B32B2274/00 , B32B2307/202 , B32B2307/306 , B32B2307/3065 , B32B2307/5825 , B32B2405/00 , B32B2457/00 , C08J5/125 , C08K5/3462 , C08K5/34922 , C08K5/5205 , C08L33/08 , C08L33/20 , C08L55/02 , C08L63/00 , C08L2666/02 , C08L2666/14 , C09J7/10 , C09J11/06 , C09J113/00 , C09J133/08 , C09J133/20 , C09J155/02 , C09J163/00 , C09J2205/102 , C09J2433/00 , C09J2455/00 , C09J2461/00 , C09J2463/00 , C09J2467/00 , C09K21/12 , H05K1/0346 , H05K1/0393 , H05K2201/012 , H05K2201/0133 , H05K2203/122 , Y10T428/24917 , Y10T428/2804 , Y10T428/31511 , Y10T428/31515 , Y10T428/31522 , Y10T428/31529 , Y10T428/31721
摘要： Provided is a flame retardant adhesive composition including (A) a halogen-free epoxy resin, (B) a thermoplastic resin and/or a synthetic rubber, (C) a curing agent, (D) a nitrogen-containing polyphosphate compound, and (E) a curing accelerator. Also provided are an adhesive sheet having a layer including the above composition, and a protective layer for covering the layer including the composition; a coverlay film having an electrically insulating film, and a layer including the above composition provided on top of the film; a flexible copper-clad laminate having an electrically insulating film, a layer including the above composition provided on top of the film, and copper foil; and a method of bonding two substrates, including the steps of sandwiching the above adhesive sheet between two substrates, and curing the adhesive sheet. Further provided are a process for producing the adhesive sheet, a process for producing the coverlay film, and a process for producing the flexible copper-clad laminate. The halogen-free adhesive composition yields a cured product, on curing, that exhibits excellent flame retardancy and anti-migration properties. The composition can be used for producing an adhesive sheet, a coverlay film, and a flexible copper-clad laminate. The adhesive sheet can be used for a method of bonding two substrates.
摘要翻译：本发明提供阻燃性粘合剂组合物，其包含（A）无卤环氧树脂，（B）热塑性树脂和/或合成橡胶，（C）固化剂，（D）含氮多磷酸盐化合物和（ E）固化促进剂。还提供了具有包含上述组合物的层的粘合片和用于覆盖包含该组合物的层的保护层; 具有电绝缘膜的覆盖层膜和设置在膜顶部的包含上述组合物的层; 具有电绝缘膜的柔性覆铜层压板，设置在膜顶部的上述组成的层和铜箔; 以及将两个基板接合的方法，包括将上述粘合片夹在两个基板之间并固化粘合片的步骤。还提供了粘合片的制造方法，覆盖膜的制造方法以及制造柔性覆铜层压体的方法。无卤粘合剂组合物在固化时产生固化产物，其显示出优异的阻燃性和抗迁移性能。该组合物可用于生产粘合片，覆盖膜和柔性覆铜层压板。粘合片可以用于粘合两个基底的方法。

9. 发明申请

US20060042750A1 Preparation of flexible copper foil/polyimide laminate 失效
标题翻译：柔性铜箔/聚酰亚胺层压板的制备
公开(公告)号：US20060042750A1
公开(公告)日：2006-03-02
申请号：US11194606
申请日：2005-08-02
申请人： Masahiro Usuki , Makoto Fujiwara , Shigehiro Hoshida , Michio Aizawa , Tadashi Amano
发明人： Masahiro Usuki , Makoto Fujiwara , Shigehiro Hoshida , Michio Aizawa , Tadashi Amano
IPC分类号： B32B37/00
CPC分类号： B32B7/12 , B32B15/08 , B32B15/20 , B32B27/281 , B32B37/12 , B32B2307/202 , B32B2307/3065 , B32B2309/105 , B32B2311/12 , B32B2379/08 , B32B2457/08 , H05K1/0346 , H05K3/025 , H05K3/386 , H05K2201/0154 , H05K2201/0358 , Y10T428/31681
摘要： A flexible metal foil/polyimide laminate is prepared by applying a polyamic acid varnish onto a very thin copper foil on a carrier, semi-drying the varnish, laminating a polyimide film to the varnish-coated copper foil using a hot roll press, and heat treating the laminate for solvent removal and imidization in an atmosphere having a controlled oxygen concentration. A polyimide adhesive layer resulting from the imidization of polyamic acid has a thickness of up to 6 μm, the sum of the thicknesses of the polyimide film and the polyimide adhesive layer is up to 25 μm. The polyimide adhesive layer has a Tg>400° C.
摘要翻译：通过将聚酰胺酸清漆涂布到载体上的非常薄的铜箔上，半干燥清漆，使用热辊压机将聚酰亚胺膜层压到涂覆有漆膜的铜箔上，制备柔性金属箔/聚酰亚胺层压体在具有受控氧浓度的气氛中处理该层压板用于溶剂去除和酰亚胺化。由聚酰胺酸酰亚胺化得到的聚酰亚胺粘合剂层的厚度最高达6μm，聚酰亚胺膜和聚酰亚胺粘合剂层的厚度之和高达25μm。聚酰亚胺粘合剂层的Tg> 400℃

10. 发明授权

US06854348B2 Method for counting foreign matter particles in vinyl chloride-based resin powder and apparatus system therefor 失效
标题翻译：氯乙烯系树脂粉末中异物颗粒的计数方法及其装置系统
公开(公告)号：US06854348B2
公开(公告)日：2005-02-15
申请号：US10213953
申请日：2002-08-08
申请人： Shigehiro Hoshida , Makoto Suzuki , Hideo Yoshikoshi , Osamu Matsumoto
发明人： Shigehiro Hoshida , Makoto Suzuki , Hideo Yoshikoshi , Osamu Matsumoto
IPC分类号： G01N15/00 , G01N15/14 , G01N33/44 , G01N15/02
CPC分类号： G01N33/442 , G01N2015/0096 , G01N2015/1486
摘要： The invention discloses a method for counting foreign matter particles in a vinyl chloride resin powder comprising the steps of: forming an aqueous dispersion of the resin particles in a vessel having a transparent bottom, allowing the particles to settle forming a layer together with the foreign matter particles and viewing the layer of the deposited particles through the transparent bottom of the vessel to count the foreign matter particles in the deposited layer. The invention also provides an apparatus system for automatically counting foreign matter particles which comprises a vessel having a transparent bottom, a feed means for the resin powder, a water supply means, a stirrer means to form an aqueous dispersion in the vessel, a viewing means such as a CCD camera for recording the bottom image of the deposited layer through the transparent bottom of the vessel, and a control means for bringing the various parts of the system into a sequential linkage motion.
摘要翻译：本发明公开了一种用于计数氯乙烯树脂粉末中的异物颗粒的方法，包括以下步骤：在具有透明底部的容器中形成树脂颗粒的水分散液，使颗粒与异物一起沉降形成层颗粒并通过容器的透明底部观察沉积的颗粒层，以计数沉积层中的异物颗粒。本发明还提供一种用于自动计数异物颗粒的装置系统，其包括具有透明底部的容器，用于树脂粉末的进料装置，供水装置，在容器中形成水分散体的搅拌器装置，观察装置例如用于通过容器的透明底部记录沉积层的底部图像的CCD照相机，以及用于使系统的各个部分进行顺序连动运动的控制装置。

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