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1. 发明授权

US07745565B2 Azetidine derivatives, method for producing said derivatives and use thereof 失效
标题翻译：氮杂环丁烷衍生物，所述衍生物的制备方法及其用途
公开(公告)号：US07745565B2
公开(公告)日：2010-06-29
申请号：US10581624
申请日：2004-12-02
申请人： Stefan Ingrisch , Alois Maier , Thomas Pfeuffer , Norbert Steidl , Herbert Winkelmann , Andrea Gantner, legal representative
发明人： Stefan Ingrisch , Alois Maier , Thomas Pfeuffer , Norbert Steidl , Herbert Winkelmann
IPC分类号： C07D205/04
CPC分类号： C08F8/30 , C07D205/06
摘要： A description is given of azetidine derivatives and methods for producing them, and of their use as a latent curing component for resins having functional groups which are reactive toward amino groups. The particular advantages of the curing component proposed in accordance with the invention, such as effective producibility, high environmental friendliness, and excellent storage stability of the resin/curing agent mixtures, make these azetidine derivatives outstandingly suitable for one-component, moisture-hardening polymer compositions, which are of special interest in particular for the production of (floor) coatings, sealants, and adhesives.
摘要翻译：给出了氮杂环丁烷衍生物及其生产方法及其作为具有对氨基具有反应性的官能团的树脂的潜在固化组分的用途的描述。根据本发明提出的固化组分的特别优点，例如有效的可生产性，高环境友好性和优异的树脂/固化剂混合物的储存稳定性，使得这些氮杂环丁烷衍生物显着地适用于单组分，湿固化聚合物特别是用于生产（地板）涂料，密封剂和粘合剂的组合物。

2. 发明申请

US20080045690A1 Azetidine Derivatives, Method for Producing Said Derivatives and Use Thereof 失效
标题翻译：氮杂环丁烷衍生物，生产所述衍生物的方法及其用途
公开(公告)号：US20080045690A1
公开(公告)日：2008-02-21
申请号：US10581624
申请日：2004-12-02
申请人： Stefan Ingrisch , Alois Maier , Thomas Pfeuffer , Norbert Steidl , Andrea Gantner , Herbert Winkelmann
发明人： Stefan Ingrisch , Alois Maier , Thomas Pfeuffer , Norbert Steidl , Andrea Gantner , Herbert Winkelmann
IPC分类号： C07D205/04 , C08F8/32 , C08J3/24 , C08K5/3412
CPC分类号： C08F8/30 , C07D205/06
摘要： A description is given of azetidine derivatives and methods for producing them, and of their use as a latent curing component for resins having functional groups which are reactive toward amino groups. The particular advantages of the curing component proposed in accordance with the invention, such as effective producibility, high environmental friendliness, and excellent storage stability of the resin/curing agent mixtures, make these azetidine derivatives outstandingly suitable for one-component, moisture-hardening polymer compositions, which are of special interest in particular for the production of (floor) coatings, sealants, and adhesives.
摘要翻译：给出了氮杂环丁烷衍生物及其生产方法及其作为具有对氨基具有反应性的官能团的树脂的潜在固化组分的用途的描述。根据本发明提出的固化组分的特别优点，例如有效的可生产性，高环境友好性和优异的树脂/固化剂混合物的储存稳定性，使得这些氮杂环丁烷衍生物显着地适用于单组分，湿固化聚合物特别是用于生产（地板）涂料，密封剂和粘合剂的组合物。

3. 发明申请

US20060194931A1 Use of diazepine derivatives as latent hardening components 审中-公开
标题翻译：二氮杂衍生物作为潜在硬化组分的使用
公开(公告)号：US20060194931A1
公开(公告)日：2006-08-31
申请号：US10555775
申请日：2004-05-05
申请人： Stefan Ingrisch , Alois Maier , Thomas Pfeuffer , Norbert Steidl , Herbert Winkelmann , Fleix Gantner , Andrea Gantner
发明人： Stefan Ingrisch , Alois Maier , Thomas Pfeuffer , Norbert Steidl , Herbert Winkelmann , Fleix Gantner , Andrea Gantner
IPC分类号： C08L63/00 , C08L75/04 , B32B27/00
CPC分类号： C08G18/10 , C08G18/3848 , C08G59/5073 , C08K5/3442 , C08L75/04
摘要： The invention relates to the use of diazepine derivates of general formula (I) and/or (II), wherein R1, R2, R3 and R5 independently represent H, C1-C20-alkyl, C3-C8-cycloakyl, C6-C10-aryl or alkylaryl comprising C1-C4-alkyl and C6-C10-aryl groups, R4═H, C1-C6-alkyl(iden), as latent hardening components for resinous substances comprising functional groups which can react with amines. Based on the particular advantages of the inventive hardening components, such as good producibility, environmentally friendly and having an excellent shelf life of the resin/hardening mixture, said diazepine derivatives are outstanding for single-componented, moisture-hardening polymer masses, which are particularly useful in the production of sealing materials, adhesives and coating materials.
摘要翻译：本发明涉及通式（I）和/或（II）的二氮杂衍生物的用途，其中R 1，R 2，R 3， SUP＆gt;和R 5独立地表示H，C 1 -C 20 - 烷基，C 3 -C 包括C 1 -C 4 - 环烷基，C 6 -C 10 - 芳基或包括C 1 -C 4 - C 1 -C 6烷基和C 6 -C 10 - 芳基，R 4 -H，C 1〜 -C 6 - 烷基（iden），作为包含可与胺反应的官能团的树脂状物质的潜在硬化成分。基于本发明的硬化组分的特别优点，例如良好的可生产性，环境友好并且具有优异的树脂/硬化混合物的保存期限，所述二氮杂衍生物对于单组分，湿润固化的聚合物质量是显着的，特别是可用于生产密封材料，粘合剂和涂料。

4. 发明授权

US07265178B2 Polyurethane-polymer hybrid-dispersion with enhanced surface properties, method for the production and utilization thereof 失效
标题翻译：具有增强表面性能的聚氨酯 - 聚合物杂化分散体，其生产和利用方法
公开(公告)号：US07265178B2
公开(公告)日：2007-09-04
申请号：US10563903
申请日：2004-07-09
申请人： Alois Maier , Stefan Ingrisch , Norbert Steidl , Frank Weinelt
发明人： Alois Maier , Stefan Ingrisch , Norbert Steidl , Frank Weinelt
IPC分类号： C08J3/00 , C08K3/20 , C08L75/00 , C08L83/00 , C08F8/30
CPC分类号： C09D151/08 , C08F283/00 , C08F283/006 , C08F289/00 , C08G18/0819 , C08G18/2885 , C08L51/08 , C08L2666/02 , C09D175/04 , C09J151/08 , Y10T428/31551
摘要： A description is given of an optionally fluorinated polyurethane-polymer hybrid dispersion with enhanced surface properties (low critical surface tensions γc and very high contact angles θ) which is obtainable by a) preparing a dispersion component (binder) based on an aqueous solution or dispersion of an optionally hydroxy- and/or amino-functional polyurethane-polymer hybrid having optionally fluorinated side chains and, if desired, b) subsequently reacting the dispersion component from stage a) with a crosslinker component (D). The polyurethane-polymer hybrid dispersion of the invention can be prepared in solvent-free or low-solvent fashion and with high solids content and requires only a very low level of stabilizing groups.
摘要翻译：给出了具有增强的表面性质（低临界表面张力γ和非常高的接触角θ）的任选氟化的聚氨酯 - 聚合物混合分散体的描述，其可通过以下步骤获得：a）制备分散体组分）基于具有任选氟化侧链的任选羟基和/或氨基官能的聚氨酯 - 聚合物杂化物的水溶液或分散体，如果需要，b）随后使来自a）步的分散体组分与交联剂组分（D ）。本发明的聚氨酯 - 聚合物混合分散体可以以无溶剂或低溶剂方式制备并具有高固体含量，并且仅需要非常低水平的稳定基团。

5. 发明申请

US20060167206A1 Fluorine-modified polyurethane resins containing one or two constituents, method for the production thereof, and use of the same 审中-公开
标题翻译：含有一种或两种成分的氟改性聚氨酯树脂，其制备方法及其用途
公开(公告)号：US20060167206A1
公开(公告)日：2006-07-27
申请号：US10563539
申请日：2004-07-06
申请人： Alois Maier , Norbert Steidl , Stefan Ingrisch , Frank Weinelt
发明人： Alois Maier , Norbert Steidl , Stefan Ingrisch , Frank Weinelt
IPC分类号： C08G18/00
CPC分类号： C08G18/6225 , C08G18/2885 , C08G18/3275 , C08G18/3812 , C08G18/718 , C09D175/04
摘要： A description is given of a fluorine-modified one- or two-component polyurethane resin having improved surface properties, which is obtainable by a) preparing a fluorine-modified polyurethane prepolymer having free isocyanate groups or free amino and/or hydroxyl groups, or a fluorine-modified polyol mixture having free hydroxyl groups (binder), and by b) preparing a fluorine-modified polyurethane resin having a polymer-bonded fluorine content of 1% to 4% by weight in the system as a whole by reacting the fluorine-modified polyurethane prepolymer from stage a3) in the case of a one-component application with atmospheric moisture, or reacting the fluorine-modified polyurethane prepolymer or polyol mixture (binder) in the case of a two-component application with a crosslinker component (D) (curing agent), with a formulating component (F)(ii) in the presence if desired of a solvent component (L)(iii) and also of a catalyst. Through the use of suitable fluorinated macromonomers in the one- or two-component polyurethane resins of the invention it is possible to produce hard coating systems and/or surfaces having very low surface tensions and very high contact angles. Furthermore, the dirt pickup tendency of these polyurethane resins is also significantly reduced as compared with the known prior art.
摘要翻译：对具有改善的表面性质的氟改性单组分或双组分聚氨酯树脂进行描述，其可通过以下步骤获得：a）制备具有游离异氰酸酯基或游离氨基和/或羟基的氟改性聚氨酯预聚物，或具有游离羟基的氟改性多元醇混合物（粘合剂），以及b）通过使该氟改性多元醇混合物中的氟 - 在具有大气湿度的单组分施用的情况下，或者在双组分的情况下使氟改性的聚氨酯预聚物或多元醇混合物（粘合剂）反应，从阶段a 3阶段的改性聚氨酯预聚物）在需要溶剂组分（L）（iii）和催化剂的情况下，用交联剂组分（D）（固化剂）与配制组分（F）（ii）的应用。通过在本发明的单组分或双组分聚氨酯树脂中使用合适的氟化大分子单体，可以生产具有非常低的表面张力和非常高的接触角的硬涂层体系和/或表面。此外，与已知的现有技术相比，这些聚氨酯树脂的污垢吸收趋势也显着降低。

6. 发明申请

US20060189750A1 Polyurethane-polymer hybrid-dispersion with enhanced surface properties, method for the production and utilization thereof 失效
标题翻译：具有增强表面性能的聚氨酯 - 聚合物杂化分散体，其生产和利用方法
公开(公告)号：US20060189750A1
公开(公告)日：2006-08-24
申请号：US10563903
申请日：2004-07-09
申请人： Alois Maier , Stefan Ingrisch , Norbert Steidl , Frank Weinelt
发明人： Alois Maier , Stefan Ingrisch , Norbert Steidl , Frank Weinelt
IPC分类号： C08G18/08
CPC分类号： C09D151/08 , C08F283/00 , C08F283/006 , C08F289/00 , C08G18/0819 , C08G18/2885 , C08L51/08 , C08L2666/02 , C09D175/04 , C09J151/08 , Y10T428/31551
摘要： A description is given of an optionally fluorinated polyurethane-polymer hybrid dispersion with enhanced surface properties (low critical surface tensions γc and very high contact angles θ) which is obtainable by a) preparing a dispersion component (binder) based on an aqueous solution or dispersion of an optionally hydroxy- and/or amino-functional polyurethane-polymer hybrid having optionally fluorinated side chains and, if desired, b) subsequently reacting the dispersion component from stage a) with a crosslinker component (D). The polyurethane-polymer hybrid dispersion of the invention can be prepared in solvent-free or low-solvent fashion and with high solids content and requires only a very low level of stabilizing groups.
摘要翻译：给出了具有增强的表面性质（低临界表面张力γ和非常高的接触角θ）的任选氟化的聚氨酯 - 聚合物混合分散体的描述，其可通过以下步骤获得：a）制备分散体组分）基于具有任选氟化侧链的任选羟基和/或氨基官能的聚氨酯 - 聚合物杂化物的水溶液或分散体，如果需要，b）随后使来自a）步的分散体组分与交联剂组分（D ）。本发明的聚氨酯 - 聚合物混合分散体可以以无溶剂或低溶剂方式制备并具有高固体含量，并且仅需要非常低水平的稳定基团。

7. 发明授权

US06787596B1 Solvent-free polyrethane-polymer-hybrid-dispersion and use thereof 失效
标题翻译：无溶剂聚氨酯 - 聚合物 - 杂化分散体及其用途
公开(公告)号：US06787596B1
公开(公告)日：2004-09-07
申请号：US10110446
申请日：2002-04-11
申请人： Alois Maier , Stefan Ingrisch , Herbert Winkelmann , Franz Wolfertstetter , Alfred Kern , Werner Temme , Ralph Bergs
发明人： Alois Maier , Stefan Ingrisch , Herbert Winkelmann , Franz Wolfertstetter , Alfred Kern , Werner Temme , Ralph Bergs
IPC分类号： C08J300
CPC分类号： C09D175/04 , C08F283/006 , C08G18/0823 , C08G18/12 , C08G18/6692 , C08L51/08 , C09D151/08 , C08G18/3228
摘要： A solvent-free polyurethane-polymer hybrid dispersion having a high solids content of polymer or formulation constituents is described, which is obtainable by a) the multistage preparation of a polyurethane base dispersion and b) by the subsequent preparation of a polyurethane-polymer hybrid dispersion. This polyurethane-polymer hybrid dispersion not only is distinguished by complete freedom from solvents and high solids contents in combination with low viscosity and a technically simple preparation process but also has excellent mechanical properties and, owing to the low hydrophilicity, high water resistance. The polyurethane-polymer hybrid dispersion proposed according to the invention can be used in an outstanding manner in formulations for sport floor coverings, said dispersion being suitable in particular as a binder for resilient coats, as a spray or leveling coating on resilient or rigid substrates, as an adhesion promoter or primer, as filling compounds for sealing pores, as adhesive for the adhesive bonding of prefabricated resilient layers or for the sealing of sport floor coverings.
摘要翻译：描述了具有高固体含量的聚合物或配制成分的无溶剂的聚氨酯 - 聚合物混合分散体，其可通过以下方式获得：a）通过随后制备聚氨酯 - 聚合物混合分散体的聚氨酯基分散体的多阶段制备和b）。聚氨酯 - 聚合物混合分散体不仅通过完全不含溶剂和高固体含量与低粘度和技术上简单的制备方法相结合，而且具有优异的机械性能，并且由于亲水性低，耐水性高。根据本发明提出的聚氨酯 - 聚合物混合分散体可以以优异的方式用于运动地板覆盖物的配方中，所述分散体特别适用于弹性涂层的粘合剂，作为弹性或刚性基材上的喷涂或流平涂层，作为粘合促进剂或底漆，作为用于密封孔的填充化合物，作为用于预制弹性层的粘合剂粘合剂或用于运动地板覆盖物的密封的粘合剂。

8. 发明授权

US06566438B1 Hybrid polyurethane-polymer dispersion with high film hardness, method for the production and the use thereof 失效
标题翻译：具有高膜硬度的混合聚氨酯 - 聚合物分散体，其制备方法和用途
公开(公告)号：US06566438B1
公开(公告)日：2003-05-20
申请号：US09787939
申请日：2001-03-22
申请人： Stefan Ingrisch , Alois Maier , Herbert Winkelmann , Franz Wolfertstetter , Alfred Kern , Josef Weichmann
发明人： Stefan Ingrisch , Alois Maier , Herbert Winkelmann , Franz Wolfertstetter , Alfred Kern , Josef Weichmann
IPC分类号： C08J300
CPC分类号： C08G18/12 , C08G18/0823 , C08G2270/00 , C09D175/06 , C08G18/3228 , C08L33/00
摘要： Described is a polyurethane/polymer hybrid dispersion with high film hardness, which comprises the reaction components (A) from 3 to 25% by weight of a polyol component consisting of (i) from 2 to 20% by weight of a relatively high molecular mass polyol component, (ii) from 0.5 to 5% by weight of a low molecular mass polyol component, (iii) from 0.5 to 3% by weight of a low molecular mass and anionically modifiable polyol component, (B) from 2 to 20% by weight of a polyisocyanate component, (C) if desired, from 0 to 6% by weight of a solvent component consisting of (i) at least one polyisocyanate-inert organic solvent and/or (ii) a polyisocyanate-inert reactive diluent, (D) from 0.15 to 1.5% by weight of a neutralizing component, (E) from 0.1 to 1% by weight of a chain extender component, (F) from 5 to 40% by weight of a monomer component, (G) from 0.01 to 1.5% by weight of an initiator component, and water as the remainder. The advantages of the polyurethane/polymer hybrid dispersion of the invention, such as high hardness coupled with high flexibility of the crack-free films, good chemical resistance, great stability of the dispersion within a wide pH range, good freeze/thaw stability, and the use of inexpensive raw materials, are achieved in a simplified synthesis route, without subsequence chemical crosslinking, with a simultaneously low organic solvent content (≦4% by weight), and with good filming at temperatures ≦+10° C.
摘要翻译：描述了具有高膜硬度的聚氨酯/聚合物混合分散体，其包含3至25重量％的多元醇组分的反应组分（A），其由（i）2至20重量％的较高分子量多元醇组分，（ii）0.5至5重量％的低分子量多元醇组分，（iii）0.5至3重量％的低分子量和阴离子可修饰的多元醇组分，（B）2至20重量％重量的多异氰酸酯组分，（C）如果需要，0至6重量％的由（i）至少一种多异氰酸酯惰性有机溶剂和/或（ii）多异氰酸酯惰性反应性稀释剂组成的溶剂组分，（D）0.15〜1.5重量％的中和成分（E）0.1〜1重量％的增链剂成分（F）5〜40重量％的单体成分（G）来自 0.01〜1.5重量％的引发剂组分，余量为水。本发明的聚氨酯/聚合物混合分散体的优点例如高硬度，无裂纹膜的高柔韧性，良好的耐化学性，在宽的pH范围内的分散体的稳定性，良好的冷冻/融化稳定性和廉价原料的使用，在简化的合成路线，没有亚序列化学交联，同时低有机溶剂含量（<= 4重量％），并且在<= + 10℃的温度下具有良好的成膜性。

9. 发明申请

US20050234191A1 Method for the production of homo-, co- and block copolymers 失效
标题翻译：制备均聚物，共聚物和嵌段共聚物的方法
公开(公告)号：US20050234191A1
公开(公告)日：2005-10-20
申请号：US10515937
申请日：2003-08-01
申请人： Stefan Ingrisch , Maier Alois , Thomas Pfeuffer , Norbert Steidl
发明人： Stefan Ingrisch , Maier Alois , Thomas Pfeuffer , Norbert Steidl
IPC分类号： C08F2/10 , C08F2/38 , C08G63/48 , C08F4/04 , C08G63/91
CPC分类号： C08F2/38 , C08F2/10
摘要： A process is described for producing homo-, co- and block copolymers by controlled radical polymerization in aqueous solution, wherein a monomer component (A) consisting of at least one radically polymerizable monomer, an initiator component (B) consisting of at least one radical initiator, a polysaccharide component (C) consisting of at least one cyclic polysaccharide (derivative) and a regulator component (D) consisting of at least one compound of the general formula (Ia) or/and (Ib) are reacted in the presence of water, in which R1 to R6 can each independently denote hydrogen, an optionally substituted C1-C20 alkyl residue, C3-C8 cycloalkyl residue, C7-C34 aralkyl residue or optionally an aromatic C6-C14 hydrocarbon residue and R2 and R5 can additionally denote polymer residues having an average molecular mass (number average) of 100 to 50,000 Daltons, and at least two but at most four of the residues R1 to R6 represent an aromatic hydrocarbon residue. In this manner it is possible to produce polymers with a very narrow molecular weight distribution. Moreover, due to the much lower amounts of initiator and regulator compared to the prior art, the polymers contain only very small amounts of regulator and initiator decomposition products.
摘要翻译：描述了通过在水溶液中控制自由基聚合制备均聚物，共聚物和嵌段共聚物的方法，其中由至少一种可自由基聚合的单体，由至少一个基团组成的引发剂组分（B）组成的单体组分（A）引发剂，由至少一种环状多糖（衍生物）组成的多糖组分（C）和由至少一种通式（Ia）或/和（Ib）的化合物组成的调节剂组分（D）在存在下反应水，其中R 1至R 6可各自独立地表示氢，任选取代的C 1 -C 20 烷基残基，C 3 -C 8环烷基残基，C 7 -C 34芳烷基残基或任选地芳族C 6 -C 14烃残基和R 2和R 5可另外表示具有平均值的聚合物残基分子量（数均）为100〜50,000道尔顿，并且至少两个但最多四个残基R 1至R 6代表芳烃残基。以这种方式，可以生产具有非常窄的分子量分布的聚合物。此外，由于与现有技术相比，引发剂和调节剂的量低得多，所以聚合物仅含有非常少量的调节剂和引发剂分解产物。

10. 发明授权

US06462127B1 Self-crosslinking polyurethane polymer hybrid dispersion 失效
标题翻译：自交联聚氨酯聚合物混合分散体
公开(公告)号：US06462127B1
公开(公告)日：2002-10-08
申请号：US09743116
申请日：2001-01-05
申请人： Stefan Ingrisch , Alois Maier , Franz Wolfertstetter , Herbert Winkelmann , Alfred Kern , Josef Weichmann
发明人： Stefan Ingrisch , Alois Maier , Franz Wolfertstetter , Herbert Winkelmann , Alfred Kern , Josef Weichmann
IPC分类号： C08J300
CPC分类号： C08G18/12 , C08F283/006 , C08G18/0823 , C08G18/6659 , C09D175/06 , C08G18/3228 , C08L2666/04
摘要： A self-crosslinking polyurethane polymer hybrid dispersion based on oxidatively drying polyols having a high degree of film hardness is described, which is characterized in that it contains the reaction components claimed. The advantages of the polyurethane polymer hybrid dispersion according to the invention, such as a high degree of hardness in combination with high flexibility of the tear-free films, good resistance to chemicals, high stability of the dispersions in a wide pH range, good stability in the freezing and thawing cycle and the use of economical raw materials, are achieved in a simplified synthesis pathway wityout subsequent chemical crosslinking, and simultaneously with a low content of organic solvent (≦4% by weight) and good film formation at temperatures of ≧+10° C.
摘要翻译：描述了一种基于氧化干燥具有高硬度膜的多元醇的自交联聚氨酯聚合物混合分散体，其特征在于其含有所要求的反应组分。根据本发明的聚氨酯聚合物混合分散体的优点，如硬度高，结合无撕裂膜的高柔性，耐化学性好，分散体在宽pH范围内的稳定性高，稳定性好在冷冻和解冻循环中使用经济的原料，在简化的合成途径中实现随后的化学交联，同时具有低含量的有机溶剂（<= 4重量％）和在 > = + 10°C

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