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1. 发明申请

US20050143612A1 Production of alkyl aromatic compounds 有权
标题翻译：烷基芳族化合物的生产
公开(公告)号：US20050143612A1
公开(公告)日：2005-06-30
申请号：US10505787
申请日：2003-02-27
申请人： Shyh-Yuan Hwang , Maruti Bhandarkar , Chung-Ming Chi , Waheed Mukaddam , Frank Demers , Richard Guarino , Dana Johnson
发明人： Shyh-Yuan Hwang , Maruti Bhandarkar , Chung-Ming Chi , Waheed Mukaddam , Frank Demers , Richard Guarino , Dana Johnson
IPC分类号： C07C7/04 , C07B61/00 , C07C2/64 , C07C2/66 , C07C2/70 , C07C7/10 , C07C7/12 , C07C11/04 , C07C11/06 , C07C11/08 , C07C11/09 , C07C15/02 , C07C15/04 , C07C15/06 , C07C15/073 , C07C15/08 , C07C15/085
CPC分类号： C07C2/66 , C07C7/04 , C07C7/10 , C07C7/12 , C07C7/13 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C07C2529/82 , Y02P20/125 , C07C15/085 , C07C11/06 , C07C15/04
摘要： Improved integrated processes for the production of alkyl aromatic compounds are disclosed wherein aromatic compounds which may be treated for removal of deleterious substances are reacted with olefin compounds, which may also be treated for contaminant removal, in the presence of acidic zeolite catalyst(s) to produce the desired alkyl aromatic compound(s). The aromatic and preferably also the olefin feeds are treated substantially to remove contaminants, particularly the nitrogen compounds contained therein, before they are brought together for reaction in the presence of the zeolite catalyst(s). In accordance with the present invention, it has been found that feed pretreatment for removal of nitrogen compounds significantly improves the run length and life of the acidic zeolite catalyst(s). The feed pretreatment of this invention may include the steps of distillation, extraction, and/or adsorption by solid adsorbent, which may be regenerated in accordance with further embodiments of this invention.
摘要翻译：公开了用于生产烷基芳族化合物的改进的一体化方法，其中可以处理去除有害物质的芳族化合物与烯烃化合物反应，烯烃化合物也可以在酸性沸石催化剂存在下进行处理以除去污染物，产生所需的烷基芳族化合物。在沸石催化剂的存在下，芳族化合物和烯烃进料基本上被处理以除去污染物，特别是其中所含的氮化合物，然后将它们聚集在一起进行反应。根据本发明，已经发现用于除去氮化合物的进料预处理显着地改善了酸性沸石催化剂的运行长度和使用寿命。本发明的进料预处理可以包括根据本发明的其它实施方案可以再生的固体吸附剂的蒸馏，萃取和/或吸附的步骤。

2. 发明申请

US20100268008A1 PRODUCTION OF ALKYL AROMATIC COMPOUNDS 审中-公开
标题翻译：生产烷基芳族化合物
公开(公告)号：US20100268008A1
公开(公告)日：2010-10-21
申请号：US12830725
申请日：2010-07-06
申请人： Shyh-Yuan Hwang , Maruti Bhandarkar , Chung-Ming Chi , Waheed Mukaddam , Frank Demers , Richard F. Guarino , Dana E. Johnson
发明人： Shyh-Yuan Hwang , Maruti Bhandarkar , Chung-Ming Chi , Waheed Mukaddam , Frank Demers , Richard F. Guarino , Dana E. Johnson
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C7/04 , C07C7/10 , C07C7/12 , C07C7/13 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C07C2529/82 , Y02P20/125 , C07C15/085 , C07C11/06 , C07C15/04
摘要： Improved integrated processes for the production of alkyl aromatic compounds are disclosed wherein aromatic compounds which may be treated for removal of deleterious substances are reacted with olefin compounds, which may also be treated for contaminant removal, in the presence of acidic zeolite catalyst(s) to produce the desired alkyl aromatic compound(s). The aromatic and preferably also the olefin feeds are treated substantially to remove contaminants, particularly the nitrogen compounds contained therein, before they are brought together for reaction in the presence of the zeolite catalyst(s). In accordance with the present invention, it has been found that feed pretreatment for removal of nitrogen compounds significantly improves the run length and life of the acidic zeolite catalyst(s). The feed pretreatment of this invention may include the steps of distillation, extraction, and/or adsorption by solid adsorbent, which may be regenerated in accordance with further embodiments of this invention.
摘要翻译：公开了用于生产烷基芳族化合物的改进的一体化方法，其中可以处理去除有害物质的芳族化合物与烯烃化合物反应，烯烃化合物也可以在酸性沸石催化剂存在下进行处理以除去污染物，产生所需的烷基芳族化合物。在沸石催化剂的存在下，芳族化合物和烯烃进料基本上被处理以除去污染物，特别是其中所含的氮化合物，然后将它们聚集在一起进行反应。根据本发明，已经发现用于除去氮化合物的进料预处理显着地改善了酸性沸石催化剂的运行长度和使用寿命。本发明的进料预处理可以包括根据本发明的其它实施方案可以再生的固体吸附剂的蒸馏，萃取和/或吸附的步骤。

3. 发明授权

US07777086B2 Production of alkyl aromatic compounds 有权
标题翻译：烷基芳族化合物的生产
公开(公告)号：US07777086B2
公开(公告)日：2010-08-17
申请号：US10505787
申请日：2003-02-27
申请人： Shyh-Yuan Hwang , Maruti Bhandarkar , Chung-Ming Chi , Waheed Mukaddam , Frank Demers , Richard F. Guarino , Dana E Johnson
发明人： Shyh-Yuan Hwang , Maruti Bhandarkar , Chung-Ming Chi , Waheed Mukaddam , Frank Demers , Richard F. Guarino , Dana E Johnson
IPC分类号： C07C2/66 , C07C7/04
CPC分类号： C07C2/66 , C07C7/04 , C07C7/10 , C07C7/12 , C07C7/13 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C07C2529/82 , Y02P20/125 , C07C15/085 , C07C11/06 , C07C15/04
摘要： Improved integrated processes for the production of alkyl aromatic compounds are disclosed wherein aromatic compounds which may be treated for removal of deleterious substances are reacted with olefin compounds, which may also be treated for contaminant removal, in the presence of acidic zeolite catalyst(s) to produce the desired alkyl aromatic compound(s). The aromatic and preferably also the olefin feeds are treated substantially to remove contaminants, particularly the nitrogen compounds contained therein, before they are brought together for reaction in the presence of the zeolite catalyst(s). In accordance with the present invention, it has been found that feed pretreatment for removal of nitrogen compounds significantly improves the run length and life of the acidic zeolite catalyst(s). The feed pretreatment of this invention may include the steps of distillation, extraction, and/or adsorption by solid adsorbent, which may be regenerated in accordance with further embodiments of this invention.
摘要翻译：公开了用于生产烷基芳族化合物的改进的一体化方法，其中可以处理去除有害物质的芳族化合物与烯烃化合物反应，烯烃化合物也可以在酸性沸石催化剂存在下进行处理以除去污染物，产生所需的烷基芳族化合物。在沸石催化剂的存在下，芳族化合物和烯烃进料基本上被处理以除去污染物，特别是其中所含的氮化合物，然后将它们聚集在一起进行反应。根据本发明，已经发现用于除去氮化合物的进料预处理显着地改善了酸性沸石催化剂的运行长度和使用寿命。本发明的进料预处理可以包括根据本发明的其它实施方案可以再生的固体吸附剂的蒸馏，萃取和/或吸附的步骤。

4. 发明授权

US07777087B2 Liquid phase alkylation with multiple catalysts 有权
标题翻译：用多种催化剂进行液相烷基化
公开(公告)号：US07777087B2
公开(公告)日：2010-08-17
申请号：US12624118
申请日：2009-11-23
申请人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
发明人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
IPC分类号： C07C2/66
CPC分类号： C10G29/205 , C07C2/66 , C07C6/126 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C10G2300/1092 , C10G2300/1096 , C10G2400/30 , Y02P20/52 , C07C15/073 , C07C15/02 , C07C15/085
摘要： A process is disclosed for producing an alkylaromatic compound in a multistage reaction system comprising at least first and second series-connected alkylation reaction zones, each containing an alkylation catalyst. A first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into the first alkylation reaction zone. The first and second alkylation reaction zones are operated under conditions of temperature and pressure effective to cause alkylation of the aromatic compound with the alkene in the presence of the alkylation catalyst, the temperature and pressure being such that the aromatic compound is at least partly in the liquid phase. The alkylation catalyst in the first alkylation reaction zone, which may be a reactor guard bed, has more acid sites per unit volume of catalyst than the alkylation catalyst in the second reaction zone.
摘要翻译：公开了一种在多级反应体系中生产烷基芳族化合物的方法，其包含至少第一和第二串联连接的烷基化反应区，每个含有烷基化催化剂。将包含可烷基化芳族化合物和包含烯烃的第二进料的第一进料引入第一烷基化反应区。第一烷基化反应区和第二烷基化反应区在温度和压力有效的条件下运行，以在烷基化催化剂存在下使芳族化合物与烯烃进行烷基化，温度和压力使芳族化合物至少部分在液相。在第一烷基化反应区（其可以是反应器保护床）中的烷基化催化剂与第二反应区中的烷基化催化剂相比，每单位体积催化剂具有更多的酸性位点。

5. 发明申请

US20090036722A1 Alkylaromatics production 有权
标题翻译：烷基芳烃生产
公开(公告)号：US20090036722A1
公开(公告)日：2009-02-05
申请号：US11881921
申请日：2007-07-30
申请人： Michael C. Clark , Vijay Nanda , Maruti Bhandarkar , Joseph C. Peters , Chung-Ming Chi , Brian Maerz
发明人： Michael C. Clark , Vijay Nanda , Maruti Bhandarkar , Joseph C. Peters , Chung-Ming Chi , Brian Maerz
IPC分类号： C07C2/68
CPC分类号： C07C2/66 , C07C15/073 , C07C15/02
摘要： A process is described for producing an alkylaromatic compound, in which a first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into a first alkylation reaction zone comprising a first alkylation catalyst. The first alkylation reaction zone is operated under conditions effective to cause alkylation of the alkylatable aromatic compound by the alkene to produce said alkylaromatic compound, the conditions being such that the alkylatable aromatic compound is at least predominantly in the vapor phase. A first effluent comprising the alkylaromatic compound and unreacted alkylatable aromatic compound is withdrawn from the first alkylation reaction zone and at least part of the unreacted alkylatable aromatic compound is treated to remove catalyst poisons therefrom and produce a treated unreacted alkylatable aromatic stream. At least part of the unreacted alkylatable aromatic compound and a third feed comprising said alkene is introduced into a second alkylation reaction zone comprising a second alkylation catalyst. The second alkylation reaction zone is operated under conditions effective to cause alkylation of the unreacted alkylatable aromatic compound by the alkene to produce said alkylaromatic compound, the conditions being such that the alkylatable aromatic compound is at least predominantly in the liquid phase. A second effluent comprising said alkylaromatic compound is withdrawn from the second alkylation reaction zone.
摘要翻译：描述了用于生产烷基芳族化合物的方法，其中将包含可烷基化芳族化合物的第一种进料和包含烯烃的第二种进料引入到包含第一烷基化催化剂的第一烷基化反应区中。第一烷基化反应区在有效使烷基化芳族化合物被烯烃烷基化以产生所述烷基芳族化合物的条件下运行，条件是使可烷基化芳族化合物至少主要在气相中。包含烷基芳族化合物和未反应的可烷基化芳族化合物的第一流出物从第一烷基化反应区取出，并且处理至少部分未反应的可烷基化芳族化合物以除去其中的催化剂毒物并产生经处理的未反应的可烷基化芳族物流。将至少部分未反应的可烷基化芳族化合物和包含所述烯烃的第三进料引入到包含第二烷基化催化剂的第二烷基化反应区中。第二烷基化反应区在有效使得未反应的可烷基化芳族化合物被烯烃烷基化以产生所述烷基芳族化合物的条件下运行，条件是使可烷基化芳族化合物至少主要在液相中。从第二烷基化反应区取出包含所述烷基芳族化合物的第二流出物。

6. 发明授权

US08445738B2 Process for producing cumene 有权
标题翻译：异丙苯生产工艺
公开(公告)号：US08445738B2
公开(公告)日：2013-05-21
申请号：US13119781
申请日：2009-09-23
申请人： Shyh-Yuan Hwang , Dana E. Johnson , Joseph C. Peters , Chung-Ming Chi , Kevin J. Fallon , Francis A. Demers
发明人： Shyh-Yuan Hwang , Dana E. Johnson , Joseph C. Peters , Chung-Ming Chi , Kevin J. Fallon , Francis A. Demers
IPC分类号： C07C2/86 , C07C37/08
CPC分类号： C07C2/864 , C07C29/145 , C07C37/08 , C07C2529/70 , Y02P20/52 , C07C15/085 , C07C31/10 , C07C39/04
摘要： A process is described for producing cumene comprising contacting a feed stream comprising benzene and a further feed stream comprising isopropanol or a mixture of isopropanol and propylene in the presence of an alkylation catalyst comprising at least a molecular sieve of the MCM-22, family in an alkylation zone under alkylation conditions of at least partial liquid phase and with a water concentration in the liquid phase of at least 50 ppm to react at least part of said isopropanol and benzene to produce an effluent stream containing cumene.
摘要翻译：描述了一种用于生产异丙基苯的方法，包括在包含至少分子筛MCM-22族的烷基化催化剂的烷基化催化剂存在下，使包含苯的进料流和包含异丙醇或异丙醇和丙烯的混合物的另外的进料流接触在至少部分液相的烷基化条件下，在液相中的水浓度为至少50ppm以使至少部分所述异丙醇和苯反应以产生含有枯烯的流出物流。

7. 发明授权

US07745676B2 Alkylaromatics production 有权
标题翻译：烷基芳烃生产
公开(公告)号：US07745676B2
公开(公告)日：2010-06-29
申请号：US11881921
申请日：2007-07-30
申请人： Michael C. Clark , Vijay Nanda , Maruti Bhandarkar , Joseph C. Peters , Chung-Ming Chi , Brian Maerz
发明人： Michael C. Clark , Vijay Nanda , Maruti Bhandarkar , Joseph C. Peters , Chung-Ming Chi , Brian Maerz
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C15/073 , C07C15/02
摘要： A process is described for producing an alkylaromatic compound, in which a first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into a first alkylation reaction zone comprising a first alkylation catalyst. The first alkylation reaction zone is operated under conditions effective to cause alkylation of the alkylatable aromatic compound by the alkene to produce said alkylaromatic compound, the conditions being such that the alkylatable aromatic compound is at least predominantly in the vapor phase. A first effluent comprising the alkylaromatic compound and unreacted alkylatable aromatic compound is withdrawn from the first alkylation reaction zone and at least part of the unreacted alkylatable aromatic compound is treated to remove catalyst poisons therefrom and produce a treated unreacted alkylatable aromatic stream. At least part of the unreacted alkylatable aromatic compound and a third feed comprising said alkene is introduced into a second alkylation reaction zone comprising a second alkylation catalyst. The second alkylation reaction zone is operated under conditions effective to cause alkylation of the unreacted alkylatable aromatic compound by the alkene to produce said alkylaromatic compound, the conditions being such that the alkylatable aromatic compound is at least predominantly in the liquid phase. A second effluent comprising said alkylaromatic compound is withdrawn from the second alkylation reaction zone.
摘要翻译：描述了用于生产烷基芳族化合物的方法，其中将包含可烷基化芳族化合物的第一种进料和包含烯烃的第二种进料引入到包含第一烷基化催化剂的第一烷基化反应区中。第一烷基化反应区在有效使烷基化芳族化合物被烯烃烷基化以产生所述烷基芳族化合物的条件下运行，条件是使可烷基化芳族化合物至少主要在气相中。包含烷基芳族化合物和未反应的可烷基化芳族化合物的第一流出物从第一烷基化反应区取出，并且处理至少部分未反应的可烷基化芳族化合物以除去其中的催化剂毒物并产生经处理的未反应的可烷基化芳族物流。将至少部分未反应的可烷基化芳族化合物和包含所述烯烃的第三进料引入到包含第二烷基化催化剂的第二烷基化反应区中。第二烷基化反应区在有效使得未反应的可烷基化芳族化合物被烯烃烷基化以产生所述烷基芳族化合物的条件下运行，条件是使可烷基化芳族化合物至少主要在液相中。从第二烷基化反应区取出包含所述烷基芳族化合物的第二流出物。

8. 发明授权

US07645913B2 Liquid phase alkylation with multiple catalysts 有权
公开(公告)号：US07645913B2
公开(公告)日：2010-01-12
申请号：US11655452
申请日：2007-01-19
申请人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
发明人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
IPC分类号： C07C2/66
CPC分类号： C10G29/205 , C07C2/66 , C07C6/126 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C10G2300/1092 , C10G2300/1096 , C10G2400/30 , Y02P20/52 , C07C15/073 , C07C15/02 , C07C15/085
摘要： A process is disclosed for producing an alkylaromatic compound in a multistage reaction system comprising at least first and second series-connected alkylation reaction zones, each containing an alkylation catalyst. A first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into the first alkylation reaction zone. The first and second alkylation reaction zones are operated under conditions of temperature and pressure effective to cause alkylation of the aromatic compound with the alkene in the presence of the alkylation catalyst, the temperature and pressure being such that the aromatic compound is at least partly in the liquid phase. The alkylation catalyst in the first alkylation reaction zone, which may be a reactor guard bed, has more acid sites per unit volume of catalyst than the alkylation catalyst in the second reaction zone.

9. 发明申请

US20050230287A1 Hydroprocessing of hydrocarbon feedstock 有权
标题翻译：烃原料的加氢处理
公开(公告)号：US20050230287A1
公开(公告)日：2005-10-20
申请号：US10510463
申请日：2003-04-07
申请人： Marius Vaarkamp , Chung-Ming Chi , Hubertus Duijndam
发明人： Marius Vaarkamp , Chung-Ming Chi , Hubertus Duijndam
IPC分类号： B01J23/46 , B01J29/12 , B01J29/22 , C10G45/04 , C10G45/06 , C10G45/10 , C10G45/12 , C10G47/02 , C10G49/02 , C10G65/00 , C10G65/02 , C10G65/12
CPC分类号： C10G65/00 , C10G2300/1048 , C10G2300/202 , C10G2300/4093
摘要： The invention is directed to a process for hydroprocessing of hydrocarbon feedstock containing sulfur and/or nitrogen contaminants, said process comprising first contacting the hydrocarbon feedstock with hydrogen in the presence of at least one first group VIII metal on a first acidic support catalyst, and thereafter contacting the feedstock with hydrogen in the presence of at least one second group VIII metal catalyst on a less acidic support.
摘要翻译：本发明涉及用于加氢处理包含硫和/或氮污染物的烃原料的方法，所述方法包括首先在第一酸性载体催化剂上在至少一种第Ⅷ族金属存在下使烃原料与氢气接触，然后在至少一种第二组VIII金属催化剂存在下，在较不酸性的载体上使原料与氢气接触。

10. 发明授权

US09255053B2 Treatment of bisphenol-A residue streams 有权
标题翻译：双酚A残留物流的处理
公开(公告)号：US09255053B2
公开(公告)日：2016-02-09
申请号：US13487872
申请日：2012-06-04
申请人： David P. Palmer , Steven D. Evitt , Stephen W. Fetsko , Chung-Ming Chi
发明人： David P. Palmer , Steven D. Evitt , Stephen W. Fetsko , Chung-Ming Chi
IPC分类号： C07C37/72 , C07C37/52 , C07C37/20 , C07C45/51
CPC分类号： C07C37/52 , C07C37/20 , C07C37/72 , C07C45/51 , C07C39/04 , C07C39/16 , C07C49/08
摘要： In a method of treating a residue stream from the production of bisphenol-A, the residue stream is contacted with an aqueous solution of a base under conditions effective to hydrolyze at least part of said residue stream into acetone and phenol and produce an effluent stream. Acetone is recovered from the effluent stream to produce a phenol-containing mixed phase stream which is substantially free of acetone and which contains water and unhydrolyzed heavy organic compounds. The phenol-containing mixed phase stream is then treated with a water-immiscible organic solvent to extract phenol and unhydrolyzed heavy organic compounds into said solvent and produce an organic phase containing the solvent, phenol and unhydrolyzed heavy aromatic compounds and an aqueous phase with reduced concentrations of phenol and unhydrolyzed heavy organic compounds. At least part of the phenol and the organic solvent are subsequently recovered from the organic phase.
摘要翻译：在从生产双酚A处理残余物流的方法中，将残余物流与碱的水溶液接触，在有效地将至少部分所述残余物流水解成丙酮和苯酚并产生流出物流的条件下进行。从流出物流中回收丙酮以产生基本上不含丙酮并含有水和未水解的重质有机化合物的含苯酚混合物流。然后用与水不混溶的有机溶剂处理含苯酚的混合物流，将苯酚和未水解的重质有机化合物提取到所述溶剂中，并产生含有溶剂，苯酚和未水解的重芳族化合物的有机相和浓度降低的水相的酚和未水解的重质有机化合物。随后从有机相中回收至少部分的苯酚和有机溶剂。

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