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1. 发明授权

US07622618B2 Method for hydrating olefins 失效
标题翻译：烯烃水合方法
公开(公告)号：US07622618B2
公开(公告)日：2009-11-24
申请号：US12085853
申请日：2006-11-30
申请人： Shinichiro Yanagawa , Michikazu Hara
发明人： Shinichiro Yanagawa , Michikazu Hara
IPC分类号： C07C29/04
CPC分类号： C07C29/04 , C07B61/00 , C07C31/10 , C07C31/12
摘要： A novel olefin hydration method is provided for efficiently producing alcohols by hydration of olefins containing 2 to 5 carbon atoms in the presence of a catalyst. Thus, alcohols are produced by hydrating olefins containing 2 to 5 carbon atoms at reaction temperature of 100 to 250° C. in the presence of a solid acid catalyst consisting of carbonaceous materials containing sulfonic acid groups obtained from an organic matter by carbonization and sulfonation. In carrying out this method, the organic matter is preferably an aromatic hydrocarbon or a saccharide, the olefin is preferably propylene or a butenes, and the hydration reaction temperature is not lower than 120° C., more preferably not lower than 150° C.
摘要翻译：提供了一种新型的烯烃水合方法，用于在催化剂存在下，通过水合含2-5个碳原子的烯烃来有效生产醇。因此，在含有2-5个碳原子的烯烃的反应温度为100-250℃的存在下，通过碳酸化和磺化从含有有机物质的磺酸基的含碳材料组成的固体酸催化剂存在下，制备醇。在实施该方法时，有机物优选为芳香族烃或糖类，烯烃优选为丙烯或丁烯，水合反应温度为120℃以上，更优选为150℃以上。

2. 发明申请

US20090137850A1 Method for Hydrating Olefins 失效
标题翻译：保温烯烃的方法
公开(公告)号：US20090137850A1
公开(公告)日：2009-05-28
申请号：US12085853
申请日：2006-11-30
申请人： Shinichiro Yanagawa , Michikazu Hara
发明人： Shinichiro Yanagawa , Michikazu Hara
IPC分类号： C07C29/04
CPC分类号： C07C29/04 , C07B61/00 , C07C31/10 , C07C31/12
摘要： A novel olefin hydration method is provided for efficiently producing alcohols by hydration of olefins containing 2 to 5 carbon atoms in the presence of a catalyst. Thus, alcohols are produced by hydrating olefins containing 2 to 5 carbon atoms at reaction temperature of 100 to 250° C. in the presence of a solid acid catalyst consisting of carbonaceous materials containing sulfonic acid groups obtained from an organic matter by carbonization and sulfonation. In carrying out this method, the organic matter is preferably an aromatic hydrocarbon or a saccharide, the olefin is preferably propylene or a butenes, and the hydration reaction temperature is not lower than 120° C., more preferably not lower than 150° C.
摘要翻译：提供了一种新型的烯烃水合方法，用于在催化剂存在下，通过水合含2-5个碳原子的烯烃来有效生产醇。因此，在含有2-5个碳原子的烯烃的反应温度为100-250℃的存在下，通过碳酸化和磺化从含有有机物质的磺酸基的含碳材料组成的固体酸催化剂存在下，制备醇。在实施该方法时，有机物优选为芳香族烃或糖类，烯烃优选为丙烯或丁烯，水合反应温度为120℃以上，更优选为150℃以上。

3. 发明授权

US08765938B2 Process for production of polysaccharide and/or monosaccharide by hydrolysis of different polysaccharide 失效
标题翻译：通过不同多糖的水解生产多糖和/或单糖的方法
公开(公告)号：US08765938B2
公开(公告)日：2014-07-01
申请号：US12304916
申请日：2007-06-22
申请人： Michikazu Hara , Shinichiro Yanagawa , Akira Matsuo , Hidesato Kondo
发明人： Michikazu Hara , Shinichiro Yanagawa , Akira Matsuo , Hidesato Kondo
IPC分类号： C07H1/08
CPC分类号： C07H3/02 , B01J21/18 , B01J27/02 , B01J31/10 , C10B53/02 , C13K1/02 , Y02E50/14
摘要： The object is to produce a polysaccharide and/or a monosaccharide efficiently by hydrolyzing a different polysaccharide efficiently. The hydrolysis of a polysaccharide is an important means for producing a monosaccharide that can be used as a starting material for the production of ethanol, the solubilization of a water-insoluble polysaccharide, and the production of a useful water-soluble low-polymeric saccharide or the like. For achieving the object, a polysaccharide to be hydrolyzed is reacted with water in the presence of a carbonaceous material having sulfonic acid group therein to cause the hydrolysis of the polysaccharide to be hydrolyzed, thereby producing a other polysaccharide and/or a monosaccharide.
摘要翻译：目的是通过有效地水解不同的多糖来有效地生成多糖和/或单糖。多糖的水解是生产可以用作生产乙醇的起始原料，水不溶性多糖的溶解和生产有用的水溶性低聚糖的单糖的重要手段，或者类似。为了达到上述目的，在其中含有磺酸基的碳质材料的存在下，将要水解的多糖与水反应，导致多糖的水解被水解，从而产生另一种多糖和/或单糖。

4. 发明申请

US20090176979A1 PROCESS FOR PRODUCTION OF POLYSACCHARIDE AND/OR MONOSACCHARIDE BY HYDROLYSIS OF DIFFERENT POLYSACCHARIDE 失效
标题翻译：通过不同多糖的水解生产多糖和/或单糖的方法
公开(公告)号：US20090176979A1
公开(公告)日：2009-07-09
申请号：US12304916
申请日：2007-06-22
申请人： Michikazu Hara , Shinichiro Yanagawa , Akira Matsuo , Hidesato Kondo
发明人： Michikazu Hara , Shinichiro Yanagawa , Akira Matsuo , Hidesato Kondo
IPC分类号： C07H1/00 , C08B1/00
CPC分类号： C07H3/02 , B01J21/18 , B01J27/02 , B01J31/10 , C10B53/02 , C13K1/02 , Y02E50/14
摘要： The object is to produce a polysaccharide and/or a monosaccharide efficiently by hydrolyzing a different polysaccharide efficiently. The hydrolysis of a polysaccharide is an important means for producing a monosaccharide that can be used as a starting material for the production of ethanol, the solubilization of a water-insoluble polysaccharide, and the production of a useful water-soluble low-polymeric saccharide or the like. For achieving the object, a polysaccharide to be hydrolyzed is reacted with water in the presence of a carbonaceous material having sulfonic acid group therein to cause the hydrolysis of the polysaccharide to be hydrolyzed, thereby producing a other polysaccharide and/or a monosaccharide.
摘要翻译：目的是通过有效地水解不同的多糖来有效地生成多糖和/或单糖。多糖的水解是生产可以用作生产乙醇的起始原料，水不溶性多糖的溶解和生产有用的水溶性低聚糖的单糖的重要手段，或者类似。为了达到上述目的，在其中含有磺酸基的碳质材料的存在下，将要水解的多糖与水反应，导致多糖的水解被水解，从而产生另一种多糖和/或单糖。

5. 发明授权

US07670712B2 Metal oxynitride electrode catalyst 有权
标题翻译：金属氮氧化物电极催化剂
公开(公告)号：US07670712B2
公开(公告)日：2010-03-02
申请号：US10581210
申请日：2004-11-30
申请人： Kenichiro Ota , Nobuyuki Kamiya , Shigenori Mitsushima , Akimitsu Ishihara , Kazunari Doumen , Michikazu Hara
发明人： Kenichiro Ota , Nobuyuki Kamiya , Shigenori Mitsushima , Akimitsu Ishihara , Kazunari Doumen , Michikazu Hara
IPC分类号： H01M4/90
CPC分类号： H01M4/90 , B01J27/24 , H01M4/9016 , H01M8/086
摘要： An electrode catalyst that maintains catalytic activity under conditions of an electrode potential as high as 0.4 V or above and exhibits improved stability. The metal oxynitride electrode catalyst is composed of an oxynitride containing at least one transition metal element selected from the group consisting of La, Ta, Nb, Ti, and Zr, the metal oxynitride electrode catalyst being used at a potential of 0.4 V or higher relative to the reversible hydrogen electrode potential in an acidic electrolyte. The metal oxynitride electrode catalyst is useful as an electrode catalyst for electrochemical systems used in acidic electrolytes in the fields of water electrolysis, organic electrolysis, fuel cells, etc.
摘要翻译：一种电极催化剂，其在电极电位高达0.4V或更高的条件下保持催化活性并表现出改进的稳定性。金属氧氮化物电极催化剂由含有选自La，Ta，Nb，Ti和Zr中的至少一种过渡金属元素的氧氮化物组成，金属氧氮化物电极催化剂以0.4V或更高的电位使用到酸性电解质中的可逆氢电极电位。金属氮氧化物电极催化剂可用作在水电解，有机电解，燃料电池等领域中用于酸性电解质的电化学体系的电极催化剂。

6. 发明申请

US20090099345A1 Carbon-Based Solid Acid, Catalyst Comprising the Solid Acid, and Reaction Using the Solid Acid as Catalyst 有权
标题翻译：碳固体酸，包含固体酸的催化剂和使用固体酸作为催化剂的反应
公开(公告)号：US20090099345A1
公开(公告)日：2009-04-16
申请号：US12282253
申请日：2007-03-08
申请人： Shinichirou Yanagawa , Hidesato Kondo , Michikazu Hara
发明人： Shinichirou Yanagawa , Hidesato Kondo , Michikazu Hara
IPC分类号： C07G1/00 , C08B1/00 , C07C41/01 , C07C5/02 , C07C67/00 , C08B33/00
CPC分类号： C07C29/04 , B01J21/18 , B01J27/02 , B01J31/10 , B01J37/084 , C01B32/05 , C07C41/06 , C07C67/08 , C07C69/54 , C07C69/14 , C07C31/10 , C07C43/046
摘要： A carbon-based solid acid which has high activity and high thermal stability and is useful as an acid catalyst for various reactions such as hydration of olefins.The carbon-based solid acid for use as a catalyst is obtained by carbonization and sulfonation of an organic substance, which has a reduction rate of 10 mol % or less of acid content as measured by immersing the solid acid in hot water at 120° C. for 2 hours, is used as the acid catalyst.The organic substance to be used as the raw material for preparing the solid acid is preferably a saccharide having β1-4 glycosidic bond (e.g. cellulose) or lignin. Amylose is also suitable as the raw material. Examples of the reaction for which the solid catalyst can be used include hydration of olefins, etherification of olefins, and acid/alcohol esterification.
摘要翻译：一种具有高活性和高热稳定性的碳基固体酸，可用作各种反应（如烯烃水合）的酸催化剂。用作催化剂的碳系固体酸通过将固体酸浸渍在120℃的热水中而测定的有机物质的还原率为10摩尔％以下的有机物质进行碳化和磺化，使用2小时作为酸催化剂。用作制备固体酸的原料的有机物质优选是具有β1-4糖苷键（例如纤维素）或木质素的糖。直链淀粉也适合作为原料。可以使用固体催化剂的反应的实例包括烯烃的水合，烯烃的醚化和酸/醇的酯化。

7. 发明授权

US07335790B2 Polycyclic aromatic carbon based solid strong acid 有权
标题翻译：多环芳烃基固体强酸
公开(公告)号：US07335790B2
公开(公告)日：2008-02-26
申请号：US10544402
申请日：2003-09-08
申请人： Kazunari Domen , Michikazu Hara
发明人： Kazunari Domen , Michikazu Hara
IPC分类号： C07C309/38
CPC分类号： B01J31/06 , B01J31/0225 , B01J37/20 , B01J2231/40 , C07C309/38 , C07C309/62
摘要： A composite solid strong acid comprising, a solid acid and a carbon material, wherein said solid acid is obtained by heat treating of polycyclic aromatic hydrocarbons or polycyclic aromatic hydrocarbons to which the carbon material is blended in concentrated sulfuric acid or fuming sulfuric acid, transforming said polycyclic aromatic hydrocarbons to a solid acid which is insoluble in a polar solvent by condensation and sulfonation further compositing with said carbon material.
摘要翻译：一种复合固体强酸，其包含固体酸和碳材料，其中所述固体酸是通过热处理多碳芳族烃或多碳芳烃而得到的，所述多环芳烃或多环芳烃是在浓硫酸或发烟硫酸中混合的碳材料，将所述多环芳香烃与固体酸反应，该固体酸通过与所述碳材料进行缩合和磺化进一步合成而不溶于极性溶剂。

8. 发明授权

US07015171B2 Photocatalyst comprising titanium fluoride nitride for water decomposition with visible light irradiation 失效
标题翻译：光催化剂，包括氟化氮化钛，用可见光照射进行水分解
公开(公告)号：US07015171B2
公开(公告)日：2006-03-21
申请号：US10500283
申请日：2002-08-07
申请人： Kazunari Domen , Michikazu Hara , Tsuyoshi Takata , Kota Nukimizu
发明人： Kazunari Domen , Michikazu Hara , Tsuyoshi Takata , Kota Nukimizu
IPC分类号： B01J27/24 , B01J27/138 , B01J27/135 , B01J27/13 , B01J23/00
CPC分类号： B01J21/063 , B01J23/42 , B01J23/44 , B01J23/755 , B01J27/24 , B01J35/004 , B01J37/088 , C01B3/042 , C01B13/0207 , Y02E60/364
摘要： A photo-catalyst containing titanium fluoride nitride comprising, Ti(IV)OaNbFc or a compound represented by MeTi(IV)OaNbFc prepared by doping at least one metal Me selected from the group consisting of alkali or alkaline earth metals on Ti(IV)OaNbFc. (wherein, b is 0.1 to 1, c is 0.1 to 1 and a is a value to maintain Ti(IV) and is decided in relation to b and c.). The photo-catalyst containing titanium fluoride nitride is especially characterized by loading at least one promoter selected from the group consisting of Pt, Ni and Pd.
摘要翻译：包含Ti（IV）O N a N b C c C或由MeTi（IV）表示的化合物）的含氟化钛的光催化剂，通过在Ti（IV）上掺杂选自由碱金属或碱土金属组成的组中的至少一种金属Me而制备的N a C b 其中，C 1，C 2，C 3，C 3，（其中，b为0.1〜1，c为0.1〜1，a为保持Ti（IV）的值，并且相对于b和c决定）。含有氟化钛的光催化剂的特征在于加载至少一种选自Pt，Ni和Pd的助催化剂。

9. 发明申请

US20060058186A1 Novel solid acid catalyst 失效
标题翻译：新型固体酸催化剂
公开(公告)号：US20060058186A1
公开(公告)日：2006-03-16
申请号：US10533567
申请日：2003-06-16
申请人： Kazunari Domen , Michikazu Hara
发明人： Kazunari Domen , Michikazu Hara
IPC分类号： C01G23/04
CPC分类号： B01J37/30 , B01J23/002 , B01J23/20 , B01J35/002 , B01J35/1014 , B01J35/1019 , B01J2523/00 , C07C67/08 , C07C69/14 , B01J2523/47 , B01J2523/56 , B01J2523/13
摘要： A solid acid catalyst represented by HTixNbyO5 wherein x is 1.1 y>0.8, having a Ti/Nb atomic ratio z of 1
摘要翻译：由HT 1 x Nb 2 O 5表示的固体酸催化剂，其中x为1.1 y> 0.8，具有1

10. 发明授权

US08575281B2 Sulfonic acid group-containing carbonaceous material 失效
标题翻译：含磺酸基的含碳材料
公开(公告)号：US08575281B2
公开(公告)日：2013-11-05
申请号：US12528051
申请日：2008-02-20
申请人： Shinichirou Yanagawa , Hidesato Kondo , Michikazu Hara
发明人： Shinichirou Yanagawa , Hidesato Kondo , Michikazu Hara
IPC分类号： C08G8/32
CPC分类号： C07C29/04 , B01J27/02 , B01J31/10 , B01J37/084 , B01J2231/49 , C01B32/05 , C07C29/09 , C07C37/08 , C07C41/06 , C07C45/29 , C07C45/53 , C07C67/04 , C07C67/08 , Y02P20/52 , C07C49/10 , C07C49/08 , C07C69/14 , C07C39/04 , C07C43/04 , C07C31/10 , C07C31/12 , C07C31/08
摘要： A sulfonic acid group-containing carbonaceous material that is useful as a solid acid catalyst for various reactions such as hydration of olefins and acidolysis reaction of hydroperoxide and also useful as a proton conductor material having excellent proton conductivity is provided. In addition, an economical and environmentally friendly method for producing methyl ethyl ketone is provided. A sulfonic acid group-containing carbonaceous material having high catalytic activities for various acid catalyst reactions and also having high proton conductivity can be obtained by carbonization and sulfonation of a phenolic resin.
摘要翻译：提供了可用作各种反应的固体酸催化剂的含磺酸基的碳质材料，例如烯烃的水合和氢过氧化物的酸解反应，并且也可用作具有优异的质子传导性的质子导体材料。此外，提供了一种经济且环保的生产甲基乙基酮的方法。对于各种酸催化剂反应具有高催化活性并且具有高质子传导性的含磺酸基的碳质材料可以通过酚醛树脂的碳化和磺化获得。

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