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1. 发明授权

US07364796B2 Adhesive composition and flexible packaging composite film 有权
标题翻译：粘合剂组合物和柔性包装复合膜
公开(公告)号：US07364796B2
公开(公告)日：2008-04-29
申请号：US10522016
申请日：2003-07-22
申请人： Shigetoshi Sasano , Sachio Igarashi
发明人： Shigetoshi Sasano , Sachio Igarashi
IPC分类号： B32B27/40 , C09J175/06 , C09J177/06
CPC分类号： B32B7/12 , B32B7/14 , B32B15/088 , B32B15/20 , B32B27/08 , B32B27/34 , B32B27/36 , B32B38/0008 , B32B2439/70 , B32B2439/80 , C08G18/10 , C08G18/4211 , C08G18/4233 , C08G18/606 , C08G18/755 , C09J175/06 , C09J175/12 , Y10T428/31551 , C08G18/42
摘要： Adhesive composition and a flexible packaging composite film that can produce a reduced amount of low-molecular-weight compounds eluted into contents of a composite film to prevent spoilage of inherent properties or performances of the contents, can produce improved oil resistance to prevent significant reduction in strength even when used for oily contents, and can develop favorable flexibility of the composite film to prevent reduction in peel strength. Polyester polyamide polyol and/or polyurethane polyester polyamide polyol including an amide bond produced by reaction between a dimer acid and polyamine is prepared as a polyol component and also concentration of a cyclic compound formed by the amide bond and/or an ester bond in extracted water which is extracted from a composite film adhesively bonded by the adhesive composition by water of 0.5 mL/cm2 per unit area of the composite film is set to be 0.5 ppb or less in terms of dibutyl phthalate concentration measured with a gas chromatograph-flame ionization detector.
摘要翻译：粘合剂组合物和柔性包装复合膜可以产生减少量的低分子量化合物洗脱到复合膜的内容物中，以防止内含物的固有性质或性能的变质，可以产生改善的耐油性以防止显着降低即使用于油性物质，也能够发挥复合膜的柔软性，防止剥离强度降低。制备包含通过二聚酸和多胺反应生成的酰胺键的聚酯聚酰胺多元醇和/或聚氨酯聚酯聚酰胺多元醇作为多元醇成分，还可以将萃取水中通过酰胺键和/或酯键形成的环状化合物的浓度从复合膜的每单位面积的0.5mL / cm 2的水用粘合剂组合物粘合的复合膜中提取的复合膜的浓度以测量的邻苯二甲酸二丁酯浓度计为0.5ppb以下用气相色谱 - 火焰离子化检测器。

2. 发明授权

US06908981B2 Laminate adhesive 有权
标题翻译：层压胶
公开(公告)号：US06908981B2
公开(公告)日：2005-06-21
申请号：US10055928
申请日：2002-01-28
申请人： Shigetoshi Sasano , Sachio Igarashi
发明人： Shigetoshi Sasano , Sachio Igarashi
IPC分类号： C09J175/04 , B32B7/12 , C08G18/42 , C09J175/06 , C08L75/06
CPC分类号： C09J175/06 , B32B7/12 , C08G18/4227 , Y10S528/905
摘要： A laminate adhesive that can suppress elution of a low molecular weight compounds of a composite film into the content, so as to prevent the inherent properties or performances of the content from being spoiled by the low molecular weight compounds. In the laminate adhesive, the polyester polyol contains naphthalenedicarboxylic acid and/or alkyl ester thereof as an acid component, and concentration of cyclic ester compounds in extracted water, which are extracted from a composite film bonded by the laminate adhesive by water of 0.5 mL/cm2 per unit area of the composite film, is 0.5 ppb or less in terms of dibutyl phthalate concentration measured by a gas chromatograph-flame ionization detector.
摘要翻译：可以抑制复合膜的低分子量化合物溶解成含量的层压粘合剂，以防止内容物的固有性质或性能被低分子量化合物破坏。在层压粘合剂中，聚酯多元醇含有作为酸成分的萘二甲酸和/或其烷基酯，以及萃取水中的环状酯化合物的浓度，从由层压粘合剂通过0.5mL / 复合膜的每单位面积的2cm 2，以气相色谱 - 火焰离子化检测器测定的邻苯二甲酸二丁酯浓度为0.5ppb以下。

3. 发明申请

US20050272898A1 Adhesive composition and soft packaging material composite film 有权
标题翻译：胶粘剂组合物和软包装材料复合膜
公开(公告)号：US20050272898A1
公开(公告)日：2005-12-08
申请号：US10522016
申请日：2003-07-22
申请人： Shigetoshi Sasano , Sachio Igarashi
发明人： Shigetoshi Sasano , Sachio Igarashi
IPC分类号： B32B7/12 , B32B7/14 , C08G18/10 , C08G18/42 , C08G18/60 , C08G18/75 , C09J175/06 , C09J175/12 , B32B27/00 , C08G18/00
CPC分类号： B32B7/12 , B32B7/14 , B32B15/088 , B32B15/20 , B32B27/08 , B32B27/34 , B32B27/36 , B32B38/0008 , B32B2439/70 , B32B2439/80 , C08G18/10 , C08G18/4211 , C08G18/4233 , C08G18/606 , C08G18/755 , C09J175/06 , C09J175/12 , Y10T428/31551 , C08G18/42
摘要： Adhesive composition and a flexible packaging composite film that can produce a reduced amount of low-molecular-weight compounds eluted into contents of a composite film to prevent spoilage of inherent properties or performances of the contents, can produce improved oil resistance to prevent significant reduction in strength even when used for oily contents, and can develop favorable flexibility of the composite film to prevent reduction in peel strength. Polyester polyamide polyol and/or polyurethane polyester polyamide polyol including an amide bond produced by reaction between a dimer acid and polyamine is prepared as a polyol component and also concentration of a cyclic compound formed by the amide bond and/or an ester bond in extracted water which is extracted from a composite film adhesively bonded by the adhesive composition by water of 0.5 mL/cm2 per unit area of the composite film is set to be 0.5 ppb or less in terms of dibutyl phthalate concentration measured with a gas chromatograph-flame ionization detector.
摘要翻译：粘合剂组合物和柔性包装复合膜可以产生减少量的低分子量化合物洗脱到复合膜的内容物中，以防止内含物的固有性质或性能的变质，可以产生改善的耐油性以防止显着降低即使用于油性物质，也能够发挥复合膜的柔软性，防止剥离强度降低。制备包含通过二聚酸和多胺反应生成的酰胺键的聚酯聚酰胺多元醇和/或聚氨酯聚酯聚酰胺多元醇作为多元醇成分，还可以将萃取水中通过酰胺键和/或酯键形成的环状化合物的浓度从复合膜的每单位面积的0.5mL / cm 2的水用粘合剂组合物粘合的复合膜中提取的复合膜的浓度以测量的邻苯二甲酸二丁酯浓度计为0.5ppb以下用气相色谱 - 火焰离子化检测器。

4. 发明授权

US06288201B1 Laminate adhesive 有权
标题翻译：层压胶
公开(公告)号：US06288201B1
公开(公告)日：2001-09-11
申请号：US09626913
申请日：2000-07-27
申请人： Shigetoshi Sasano , Sachio Igarashi
发明人： Shigetoshi Sasano , Sachio Igarashi
IPC分类号： C08G1834
CPC分类号： C08G18/4233 , C08G18/4211 , C09J175/06
摘要： A laminate adhesive that can suppress elusion of a low molecular weight compounds of a composite film into the content, so as to prevent the inherent properties or performances of the content from being spoiled by the low molecular weight compounds. The laminate adhesive comprises a polyisocyanate component and a polyol component, wherein the polyol component includes polyester polyol and/or polyester polyurethane polyol which is produced by reaction of polyester polyol and polyisocyanate, and wherein concentration of cyclic compounds in extracted water which are extracted from a composite film bonded by the laminate adhesive by water of 0.5 mL/cm2 per unit area of the composite film is 0.5 ppb or less in terms of dibutyl phthalate concentration measured by a gas chromatograph-flame ionization detector.
摘要翻译：可以抑制复合膜的低分子量化合物的含量降低的层压粘合剂，以防止低分子量化合物的内在特性或性能受到破坏。层压粘合剂包括多异氰酸酯组分和多元醇组分，其中所述多元醇组分包括通过聚酯多元醇和多异氰酸酯的反应制备的聚酯多元醇和/或聚酯聚氨酯多元醇，并且其中从萃取水中提取的环状化合物浓度通过层压粘合剂将复合膜的每单位面积的0.5mL / cm 2的水粘合的复合膜以气相色谱 - 火焰离子化检测器测定的邻苯二甲酸二丁酯浓度计为0.5ppb以下。

5. 发明授权

US06846894B2 Laminate adhesive and usage thereof 有权
标题翻译：层压粘合剂及其用途
公开(公告)号：US06846894B2
公开(公告)日：2005-01-25
申请号：US10199030
申请日：2002-07-22
申请人： Hideki Terada , Shigetoshi Sasano , Sachio Igarashi
发明人： Hideki Terada , Shigetoshi Sasano , Sachio Igarashi
IPC分类号： C08G18/32 , C08G18/42 , C09J175/06 , C08G18/77
CPC分类号： C08G18/3206 , C08G18/4211 , C09J175/06 , Y10T428/2809 , Y10T428/2852
摘要： To provide a laminate adhesive that can keep on having adequate adhesiveness and also can prevent the odor and taste of the inherent properties of the content packed by the packing product from being spoiled even after high temperature sterilization treatment, such as the hot-water spray sterilization treatment, the hot-water rotary sterilization treatment or the steam sterilization treatment, to provide a usage of the laminate adhesive, the laminate adhesive comprises a curing component containing polyisocyanate and a base component containing polyol, wherein a silane coupling agent is contained in at least the curing component. Preferably, the silane coupling agent is mixed with both of the curing component and the base component. Further preferably, epoxysilane is mixed with the curing component and also aminosilane and oxyacid of phosphorus or derivative thereof are mixed with the base component.
摘要翻译：为了提供能够保持足够粘附性的层压粘合剂，并且即使在高温灭菌处理（例如热水喷雾灭菌）之后也可以防止包装产品包装的成分的内在特性的气味和味道被破坏处理，热水旋转灭菌处理或蒸汽消毒处理，以提供层压粘合剂的用途，层压粘合剂包含含有多异氰酸酯的固化组分和含有多元醇的基础成分，其中至少包含硅烷偶联剂固化组分。优选地，将硅烷偶联剂与固化组分和基础组分两者混合。进一步优选将环氧硅烷与固化组分混合，并将磷或其衍生物的氨基硅烷和含氧酸与基础组分混合。

6. 发明授权

US08377508B2 Solventless laminating adhesive and process for production of composite film 有权
标题翻译：无溶剂层压粘合剂和复合膜生产工艺
公开(公告)号：US08377508B2
公开(公告)日：2013-02-19
申请号：US12451903
申请日：2008-05-12
申请人： Takashi Uemura , Shigetoshi Sasano , Yasuhiko Kataoka
发明人： Takashi Uemura , Shigetoshi Sasano , Yasuhiko Kataoka
IPC分类号： B05D5/10 , C08F26/02
CPC分类号： C09J175/06 , B32B7/12 , B32B27/08 , B32B27/20 , B32B27/30 , B32B27/32 , B32B27/34 , B32B27/36 , B32B27/38 , B32B27/40 , B32B2255/20 , B32B2307/516 , B32B2307/518 , B32B2307/704 , B32B2307/718 , B32B2307/7242 , B32B2439/70 , B32B2439/80 , C08G18/10 , C08G18/12 , C08G18/3893 , C08G18/4213 , C08G18/4216 , C08G18/4219 , C08G18/4238 , C08G18/4812 , C08G18/4829 , C08G18/4854 , C08G18/725 , C08G18/7831 , C08G18/7837 , C08G18/792 , C08G2250/00 , Y10T428/2896 , C08G18/48 , C08G18/42
摘要： A solventless laminating adhesive comprising a polyisocyanate component and a polyol component, both of which are free from polyol components exhibiting crystalline properties at ordinary temperatures. The adhesive exhibits an initial viscosity of 500 to 1000 mPa s three minutes after mixing of the polyisocyanate component with the polyol component and a viscosity increase of 100 to 350% based on the initial viscosity 20 minutes after the mixing. In a coater which is provided with a pair of opposed rolls and in which the rolls rotates in the directions contrary to each other at the opposition site, the adhesive is applied to a film passing between the rolls.
摘要翻译：一种无溶剂层压粘合剂，其包含多异氰酸酯组分和多元醇组分，两者均不含在常温下显示结晶性质的多元醇组分。粘合剂在多异氰酸酯组分与多元醇组分混合后三分钟的初始粘度为500至1000mPa·s，混合后20分钟的粘度增加为100至350％。在设置有一对相对的辊的涂布机中，辊在相对的位置沿彼此相反的方向旋转，粘合剂被施加到通过辊之间的膜。

7. 发明申请

US20100242798A1 Laminating Adhesive 有权
标题翻译：层压胶
公开(公告)号：US20100242798A1
公开(公告)日：2010-09-30
申请号：US12223925
申请日：2007-02-14
申请人： Hideki Terada , Shigetoshi Sasano
发明人： Hideki Terada , Shigetoshi Sasano
IPC分类号： C09J4/00
CPC分类号： C08G18/4263 , C08G18/0823 , C08G18/10 , C08G18/606 , C08G18/8022 , C08K5/5435 , C08K5/544 , C09J175/06 , C08G18/289
摘要： A laminating adhesive includes a polyol; an acid-modified polyol obtained by reaction of a hydrophobic polyol containing a hydrocarbon moiety having 12 to 80 carbon atoms in its molecule in an amount of 30 to 95% by weight or a derivative thereof with an aromatic polycarboxylic acid anhydride and having a carboxyl group at a molecular terminal thereof; an organic polyisocyanate compound; and a silane coupling agent.A laminating adhesive film is excellent even after high-temperature sterilization treatment in adhesion performance between a metal foil or a barrier film and a plastic film serving as an inner layer, and also in adhesion performance between a metal foil or a barrier film and a plastic film serving as an outer layer.
摘要翻译：层压粘合剂包括多元醇; 通过使分子中含有碳原子数为12〜80的烃部分的疏水性多元醇的含量为30〜95重量％或其衍生物与芳香族多羧酸酐反应而具有羧基的酸改性多元醇在其分子末端; 有机多异氰酸酯化合物; 和硅烷偶联剂。即使在金属箔或阻挡膜与作为内层的塑料膜之间的粘合性能进行高温灭菌处理之后，也可以在金属箔或阻挡膜和塑料之间的粘合性能方面优异的层压粘合膜是优异的电影作为外层。

8. 发明授权

US5478897A Polyurethane adhesive compositions 失效
标题翻译：聚氨酯胶粘剂组合物
公开(公告)号：US5478897A
公开(公告)日：1995-12-26
申请号：US228856
申请日：1994-04-18
申请人： Shigetoshi Sasano , Teruo Hori , Kyuya Yamazaki
发明人： Shigetoshi Sasano , Teruo Hori , Kyuya Yamazaki
IPC分类号： C08G18/40 , C09J175/04 , C08L63/02 , C10B1/00
CPC分类号： C08G18/4213 , C08G18/10 , C08G18/246 , C08G18/3206 , C08G18/4045 , C08G18/4216 , C08G18/755 , C08G18/7621 , C08G18/7642 , C08G18/792 , C09J175/04
摘要： A polyurethane adhesive composition prepared by incorporating phosphorus oxy acid or a derivative thereof, an amine compound and an epoxy resin into an organic polyisocyanate and an organic polyol.The polyurethane adhesive composition is employed in the manufacture of composite films by lamination of various plastic films, metal foils and so forth. The composition is excellent in adhesive properties, acid resistance and hot water resistance.
摘要翻译：通过将磷酸或其衍生物，胺化合物和环氧树脂掺入有机多异氰酸酯和有机多元醇中制备的聚氨酯粘合剂组合物。聚氨酯粘合剂组合物用于通过各种塑料膜，金属箔等的层压制造复合膜。该组合物的粘合性，耐酸性和耐热水性优异。

9. 发明授权

US08735527B2 Laminating adhesive 有权
标题翻译：层压胶
公开(公告)号：US08735527B2
公开(公告)日：2014-05-27
申请号：US13430469
申请日：2012-03-26
申请人： Akihiro Imai , Takeshi Osaki , Shigetoshi Sasano
发明人： Akihiro Imai , Takeshi Osaki , Shigetoshi Sasano
IPC分类号： C08G18/32 , C09J175/04
CPC分类号： C08G18/4615 , C08G18/003 , C08G18/3212 , C08G18/4216 , C08G18/4238 , C08G18/44 , C08G18/4854 , C08G18/664 , C08G18/6674 , C08G18/755 , C08G18/757 , C08G18/79 , C08G18/792 , C09J175/06
摘要： [Solution to Problem] The laminating adhesive of the present invention includes a polyisocyanate component (A) and a polyol component (B), wherein the polyisocyanate component (A) contains a polyisocyanate (A1) that does not contain an aromatic ring, and the polyol component (B) contains a macropolyol (B1) that does not contain an aromatic ring but contains a cyclohexane ring.
摘要翻译： [问题的解决方案]本发明的层压粘合剂包括多异氰酸酯成分（A）和多元醇成分（B），其中，多异氰酸酯成分（A）含有不含芳环的多异氰酸酯（A1），多元醇成分（B）含有不含有芳香环但含有环己烷环的大分子多元醇（B1）。

10. 发明授权

US08097079B2 Laminating adhesive 有权
标题翻译：层压胶
公开(公告)号：US08097079B2
公开(公告)日：2012-01-17
申请号：US12223925
申请日：2007-02-14
申请人： Hideki Terada , Shigetoshi Sasano
发明人： Hideki Terada , Shigetoshi Sasano
IPC分类号： C09J4/00
CPC分类号： C08G18/4263 , C08G18/0823 , C08G18/10 , C08G18/606 , C08G18/8022 , C08K5/5435 , C08K5/544 , C09J175/06 , C08G18/289
摘要： A laminating adhesive includes a polyol; an acid-modified polyol obtained by reaction of a hydrophobic polyol containing a hydrocarbon moiety having 12 to 80 carbon atoms in its molecule in an amount of 30 to 95% by weight or a derivative thereof with an aromatic polycarboxylic acid anhydride and having a carboxyl group at a molecular terminal thereof; an organic polyisocyanate compound; and a silane coupling agent.A laminating adhesive film is excellent even after high-temperature sterilization treatment in adhesion performance between a metal foil or a barrier film and a plastic film serving as an inner layer, and also in adhesion performance between a metal foil or a barrier film and a plastic film serving as an outer layer.
摘要翻译：层压粘合剂包括多元醇; 通过使分子中含有碳原子数为12〜80的烃部分的疏水性多元醇的含量为30〜95重量％或其衍生物与芳香族多羧酸酐反应而具有羧基的酸改性多元醇在其分子末端; 有机多异氰酸酯化合物; 和硅烷偶联剂。即使在金属箔或阻挡膜与作为内层的塑料膜之间的粘合性能进行高温灭菌处理之后，也可以在金属箔或阻挡膜和塑料之间的粘合性能方面优异的层压粘合膜是优异的电影作为外层。

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