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1. 发明申请

US20060207939A1 Separation system, components of a separation system and methods of making and using them 有权
标题翻译：分离系统，分离系统的组成部分以及制造和使用它们的方法
公开(公告)号：US20060207939A1
公开(公告)日：2006-09-21
申请号：US11337071
申请日：2006-01-19
申请人： Robert Allington , Shaofeng Xie , Tao Jiang , Mingcheng Xu
发明人： Robert Allington , Shaofeng Xie , Tao Jiang , Mingcheng Xu
IPC分类号： B01D15/08
CPC分类号： B01J20/3064 , B01D15/206 , B01J8/0005 , B01J19/0013 , B01J19/18 , B01J20/283 , B01J20/285 , B01J2219/00162 , B01J2220/54 , B01J2220/82 , G01N30/56 , G01N2030/522 , G01N2030/528 , G01N2030/567 , G01N30/30
摘要： Permeable polymeric monolithic materials are prepared in a column casing. In one embodiment, the permeable polymeric monolithic materials are polymerized while pressure is applied through a piston having a smooth piston head in contact with the polymerization mixture. The pressure eliminates wall effect and changes the structure in the column. Similarly, some columns that have a tendency to swell in the presence of aqueous solutions and pressurized while the solution is applied to prevent swelling and wall effect. This procedure also changes the structure in the column. The size of the separation effective openings can be controlled by the amount of the pressure and pores eliminated. Uniformity in the direction flow is improved by controlling polymerization with radiation rather than with conducted heat.
摘要翻译：在柱套管中制备可渗透的聚合物整体材料。在一个实施方案中，可渗透的聚合物整体材料在通过具有与聚合混合物接触的平滑活塞头的活塞施加压力时聚合。压力消除了墙壁效应并改变了柱子的结构。类似地，一些在水溶液存在下具有溶胀倾向并在施加溶液时加压以防止膨胀和壁效应的柱。此过程也会更改列中的结构。分离有效开口的尺寸可以通过消除的压力和孔隙的量来控制。通过用辐射而不是传导热来控制聚合来提高方向流动的均匀性。

2. 发明申请

US20050061745A1 Separation system, components of a separation system and methods of making and using them 审中-公开
标题翻译：分离系统，分离系统的组成部分以及制造和使用它们的方法
公开(公告)号：US20050061745A1
公开(公告)日：2005-03-24
申请号：US10914005
申请日：2004-08-06
申请人： Shaofeng Xie , Mingcheng Xu , Robert Allington
发明人： Shaofeng Xie , Mingcheng Xu , Robert Allington
IPC分类号： B01J20/281 , B01D15/20 , B01J8/00 , B01J19/00 , B01J19/18 , B01J20/283 , B01J20/285 , C08F2/00 , G01N30/16 , G01N30/46 , G01N30/52 , G01N30/56 , G01N30/80 , G01N30/88 , B01D15/08
CPC分类号： B01J20/285 , B01D15/20 , B01D15/206 , B01J8/0005 , B01J19/0013 , B01J19/18 , B01J20/28042 , B01J20/28052 , B01J20/283 , B01J2219/00162 , B01J2220/54 , B01J2220/82 , G01N30/52 , G01N30/54 , G01N30/56 , G01N2030/525 , G01N2030/528 , G01N2030/567 , G01N2030/522 , G01N30/30
摘要： Permeable polymeric monolithic materials are prepared in a column casing. In one embodiment, the permeable polymeric monolithic materials polymerized by the application of heat from an external source starting at a low temperature such as 40 degrees centigrade, depending on the mixture and size of the column, and continuing at a higher temperature, such as 60 degrees centigrade. The temperature at the start of the polymerization is low enough so as not to cause exothermal run-away conditions and to avoid high heat of reaction that would prevent a substantially constant temperature across the cross-section of the column. The higher temperature is used after sufficient monomer depletion has occurred and steric interference has increased so the polymerization reaction is sufficiently slow to avoid heat of reaction generation high enough to cause significant reduction in the homogeneousness of the pore sizes.
摘要翻译：在柱套管中制备可渗透的聚合物整体材料。在一个实施方案中，根据柱的混合物和尺寸，通过从外部源施加热量，从低温如40摄氏度开始聚合的可渗透聚合物整体材料，并且在较高温度下继续进行，例如60 摄氏度。聚合开始时的温度足够低，从而不会引起放热的脱离条件，并避免高度的反应热，从而阻止整个塔的截面上的基本恒定的温度。在发生足够的单体消耗并且空间干扰增加之后使用较高的温度，因此聚合反应足够慢，以避免足够高的反应产生热，导致孔径的均匀性显着降低。

3. 发明申请

US20070068230A1 Liquid chromatographic method and system 失效
公开(公告)号：US20070068230A1
公开(公告)日：2007-03-29
申请号：US11605666
申请日：2006-11-28
申请人： Robert Allington , Robert Allington Estate , Dale Davison , Scott Blakley
发明人： Robert Allington , Robert Allington Estate , Dale Davison , Scott Blakley
IPC分类号： G01N30/00
CPC分类号： G01N30/466 , B01D15/12 , B01D15/166 , B01D15/247 , G01N1/14 , G01N1/38 , G01N30/22 , G01N30/24 , G01N30/32 , G01N30/34 , G01N30/74 , G01N30/88 , G01N35/1095 , G01N35/1097 , G01N2001/383 , G01N2030/027 , G01N2030/324 , G01N2030/326 , G01N2030/347
摘要： A chromatographic monitor includes an array of flow cells with individual light sensors that are collectively an array of photodiodes. The output from the photodiodes are multiplexed. To prevent losing information, the photodiodes are each connected to a different one of a plurality of inputs to the multiplexer through a corresponding one of a plurality of circuits that stores energy during the time the one inlet is not connected through the multiplexer to the signal processing circuitry that forms a part of an absorbance monitor. Preferably, the energy storing circuit is a non-switching circuit with low bandwidth and a flat-topped response to an impulse. This improves the signal to noise ratio. A one pole low pass filter with a (1-1/e) Dirac pulse fall time and equal to the multiplex entire cycle repeat time can perform this function and a one pole low pass filter provides satisfactory results. Still better results can be obtained from a three pole, one or two percent overshoot filter with combined minimum frequency bandwidth and fast rise time. A rise time equal to ½ the multiplex entire cycle.

4. 发明申请

US20050224403A1 Liquid chromatographic method and system 审中-公开
标题翻译：液相色谱法和体系
公开(公告)号：US20050224403A1
公开(公告)日：2005-10-13
申请号：US11149900
申请日：2005-06-10
申请人： Robert Allington , Dale Davison , Scott Blakley
发明人： Robert Allington , Dale Davison , Scott Blakley
IPC分类号： B01D15/12 , B01D15/16 , B01D15/24 , G01N1/00 , G01N1/38 , G01N30/02 , G01N30/22 , G01N30/24 , G01N30/32 , G01N30/46 , G01N30/74 , G01N30/88 , B01D15/08
CPC分类号： G01N30/466 , B01D15/12 , B01D15/166 , B01D15/247 , G01N1/14 , G01N1/38 , G01N30/22 , G01N30/24 , G01N30/32 , G01N30/34 , G01N30/74 , G01N30/88 , G01N35/1095 , G01N35/1097 , G01N2001/383 , G01N2030/027 , G01N2030/324 , G01N2030/326 , G01N2030/347
摘要： A chromatographic monitor includes an array of flow cells with individual light sensors that are collectively an array of photodiodes. The output from the photodiodes are multiplexed. To prevent losing information, the photodiodes are each connected to a different one of a plurality of inputs to the multiplexer through a corresponding one of a plurality of circuits that stores energy during the time the one inlet is not connected through the multiplexer to the signal processing circuitry that forms a part of an absorbance monitor. Preferably, the energy storing circuit is a non-switching circuit with low bandwidth and a flat-topped response to an impulse. This improves the signal to noise ratio. A one pole low pass filter with a (1−1/e) Dirac pulse fall time and equal to the multiplex entire cycle repeat time can perform this function and a one pole low pass filter provides satisfactory results. Still better results can be obtained from a three pole, one or two percent overshoot filter with combined minimum frequency bandwidth and fast rise time. A rise time equal to ½ the multiplex entire cycle.
摘要翻译：色谱监测器包括具有单独的光传感器的流动池阵列，它们共同地是一组光电二极管。来自光电二极管的输出被复用。为了防止丢失信息，光电二极管各自通过多个电路中的相应一个电路将多个输入中的不同的一个输入连接到多个电路，多个电路在一个入口未通过多路复用器连接到信号处理期间存储能量形成吸光度监测器的一部分的电路。优选地，能量存储电路是具有低带宽和对脉冲的平顶响应的非开关电路。这提高了信噪比。具有（1-1 / e）狄拉克脉冲下降时间并且等于多路复用全周期重复时间的单极低通滤波器可以执行该功能，并且单极低通滤波器提供令人满意的结果。可以从具有组合的最小频率带宽和快速上升时间的三极，一或二％过冲滤波器获得更好的结果。上升时间等于多路复用整个周期的1/2。

5. 发明申请

US20070089493A1 Liquid chromatographic method and system 失效
标题翻译：液相色谱法和体系
公开(公告)号：US20070089493A1
公开(公告)日：2007-04-26
申请号：US11605980
申请日：2006-11-29
申请人： Robert Allington , Dale Davison , Scott Blakley
发明人： Robert Allington , Dale Davison , Scott Blakley
IPC分类号： G01N30/00
CPC分类号： G01N30/466 , B01D15/12 , B01D15/166 , B01D15/247 , G01N1/14 , G01N1/38 , G01N30/22 , G01N30/24 , G01N30/32 , G01N30/34 , G01N30/74 , G01N30/88 , G01N35/1095 , G01N35/1097 , G01N2001/383 , G01N2030/027 , G01N2030/324 , G01N2030/326 , G01N2030/347
摘要： A chromatographic monitor includes an array of flow cells with individual light sensors that are collectively an array of photodiodes. The output from the photodiodes are multiplexed. To prevent losing information, the photodiodes are each connected to a different one of a plurality of inputs to the multiplexer through a corresponding one of a plurality of circuits that stores energy during the time the one inlet is not connected through the multiplexer to the signal processing circuitry that forms a part of an absorbance monitor. Preferably, the energy storing circuit is a non-switching circuit with low bandwidth and a flat-topped response to an impulse. This improves the signal to noise ratio. A one pole low pass filter with a (1-1/e) Dirac pulse fall time and equal to the multiplex entire cycle repeat time can perform this function and a one pole low pass filter provides satisfactory results. Still better results can be obtained from a three pole, one or two percent overshoot filter with combined minimum frequency bandwidth and fast rise time. A rise time equal to ½ the multiplex entire cycle.
摘要翻译：色谱监测器包括具有单独的光传感器的流动池阵列，它们共同地是一组光电二极管。来自光电二极管的输出被复用。为了防止丢失信息，光电二极管各自通过多个电路中的相应一个电路将多个输入中的不同的一个输入连接到多个电路，多个电路在一个入口未通过多路复用器连接到信号处理期间存储能量形成吸光度监测器的一部分的电路。优选地，能量存储电路是具有低带宽和对脉冲的平顶响应的非开关电路。这提高了信噪比。具有（1-1 / e）狄拉克脉冲下降时间并且等于多路复用全周期重复时间的单极低通滤波器可以执行该功能，并且单极低通滤波器提供令人满意的结果。可以从具有组合的最小频率带宽和快速上升时间的三极，一或二％过冲滤波器获得更好的结果。上升时间等于多路复用整个周期的1/2。

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