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1. 发明授权

US4097641A Flame retardant finishes for textile materials 失效
标题翻译：纺织材料用阻燃漆
公开(公告)号：US4097641A
公开(公告)日：1978-06-27
申请号：US748957
申请日：1976-12-09
申请人： Ray E. Smith , James A. Albright
发明人： Ray E. Smith , James A. Albright
IPC分类号： D06M13/285 , D06M13/295 , D06M13/298 , D06M15/673 , D06M23/06 , C09D1/00
CPC分类号： D06M13/285 , D06M13/295 , D06M13/298 , D06M15/673 , D06M23/06 , Y10S428/921 , Y10T442/2697
摘要： Improved flame retardant concentrates and finishes containing triesters of pentavalent phosphorus acid having the general formula ##STR1## WHEREIN X, X' and X" are hydrogen, chlorine and bromine; a is 0 or 1; n is an integer of from 1 to 7; m is an integer of from 1 to n; b is an integer of from 1 to 7; and z is an integer of from 1 to b.
摘要翻译：具有通式为“X”，“X”和“X”的五价磷酸三酯的改进的阻燃浓缩物和表面处理剂是氢，氯和溴; a是0或1; n为1〜7的整数， m为1〜n的整数; b为1〜7的整数; z为1〜b的整数。

2. 发明授权

US4046701A Durable flame retardant finishes for textile materials 失效
标题翻译：耐用的阻燃涂料用于纺织材料
公开(公告)号：US4046701A
公开(公告)日：1977-09-06
申请号：US660502
申请日：1976-02-23
申请人： Ray E. Smith
发明人： Ray E. Smith
IPC分类号： D06M13/44 , D06M13/02 , D06M13/144 , D06M13/21 , D06M13/224 , D06M13/236 , D06M13/244 , D06M13/282 , D06M13/285 , D06M13/322 , D06M13/325 , D06M13/328 , D06M13/33 , D06M13/332 , D06M13/338 , D06M13/345 , D06M13/35 , D06M13/355 , D06M13/358 , D06M13/364 , D06M13/402 , D06M13/432 , D06M15/673 , C09K3/28
CPC分类号： D06M13/236 , D06M13/21 , D06M13/285 , D06M15/673
摘要： Novel flame retardant finishes comprising a water soluble quaternary phosphonium salt, a water soluble organic nitrogen containing compound, a halophthalate diol, water, and either an organic solvent characterized by having a flash point of at least 80.degree. F. and a boiling point within the range of about 300.degree. to about 350.degree. F. and an emulsifier having a hydrophile lipophile balance value of from about 10 to about 14 or an emulsifying agent which is capable of passing the following three tests: (1) Solubility (Compatability) Test: said emulsifying agent (20 parts by weight) must be soluble in 80 parts by weight of said phosphate ester at less than or equal to 80.degree. C.; (2) Shelf Life Test: a blend of said emulsifying agent and said phosphate ester prepared as in the Solubility Test must remain in one clear homogeneous phase at 22.degree. C. for at least one hour; (3) Finish Formulation Test: a flame retardant finish within the scope of this invention is prepared and must remain in one homogeneous phase for a minimum of one hour at 20.degree. C. These flame retardant finishes are excellent for flame retarding textile materials including polyester/cotton blend fabrics.
摘要翻译：新型阻燃整理剂，其包含水溶性季鏻盐，水溶性有机氮化合物，卤代邻苯二甲酸酯二醇，水和有机溶剂，其特征在于闪点至少为80°F，沸点在范围为约300至约350°F，亲水亲油平衡值为约10至约14的乳化剂或能够通过以下三个试验的乳化剂：（1）溶解度（兼容性）试验：所述乳化剂（20重量份）在小于或等于80℃时必须溶于80重量份的所述磷酸酯中。（2）保质期测试：如在溶解度试验中制备的所述乳化剂和所述磷酸酯的共混物必须在22℃下保持在一个清澈的均匀相中至少1小时; （3）精制制剂试验：制备本发明范围内的阻燃整理剂，并且必须在20℃下保持一个均匀相至少1小时。这些阻燃整理剂对于阻燃纺织品（包括聚酯）是优异的 /棉混纺面料。

3. 发明授权

US4345002A Novel intumescent composition and flame retardant articles treated therewith 失效
标题翻译：新型膨胀组合物和用其处理的阻燃制品
公开(公告)号：US4345002A
公开(公告)日：1982-08-17
申请号：US76041
申请日：1979-09-17
申请人： Ray E. Smith , Jayendra G. Shukla , Richard R. Nicholson
发明人： Ray E. Smith , Jayendra G. Shukla , Richard R. Nicholson
IPC分类号： C07D251/70 , C07F9/09 , C07F9/146 , C07F9/24 , C09D5/18 , C09K21/10 , C09K21/12 , D06M15/673 , D04H1/58
CPC分类号： D06M15/673 , C07D251/70 , C07F9/091 , C07F9/146 , C07F9/2408 , C07F9/2458 , C09D5/185 , C09K21/10 , C09K21/12 , Y10S428/913 , Y10S428/921 , Y10T428/2938 , Y10T428/3196 , Y10T428/31967
摘要： An intumescent composition containing a cyclic nitrogen compound, a hydroxy-containing organo-phosphorus compound, an organo-phosphorus acid, and water, wherein:(a) said cyclic nitrogen compound is: ##STR1## wherein a, b, and c, are integers selected from the group consisting of 1 and 2, a plus b plus c equal about 3 to 6, and wherein and X, X', and X" are hydrogen or --CH.sub.3 ;(b) said hydroxy-containing organo-phosphorus compound is selected from the group consisting of: ##STR2## and mixtures thereof wherein R.sup.1, R.sup.2 and R.sup.3 are lower alkyl or haloalkyl radicals and R.sup.4 and R.sup.5 are hydrogen, lower alkyl or haloalkyl radicals;(c) said acid is selected from the group consisting of: ##STR3## and mixtures thereof, wherein R.sup.6, R.sup.7, R.sup.8 and R.sup.9 are hydrogen, lower alkyl, haloalkyl or hydroxyalkyl, R.sup.10 and R.sup.11 are lower alkyl, haloalkyl, hydroxy-polyalkyleneoxy, alkoxy, hydroxyalkoxy or haloalkoxy, ##STR4## wherein R.sup.12 is lower alkylene, haloalkylene, polyalkyleneoxy, hydroxy-alkylene and R.sup.13 and R.sup.14 are hydrogen, hydroxyl, lower alkyl, hydroxy-polyalkyleneoxy, alkoxy, hydroxyalkoxy or haloalkoxy.
摘要翻译：包含环状氮化合物，含羟基的有机磷化合物，有机磷酸和水的膨胀性组合物，其中：（a）所述环状氮化合物是：其中a，b和c分别为选自1和2，a加b加c等于3至6的整数，并且其中X，X'和X“是氢或-CH 3; （b）所述含羟基的有机磷化合物选自：其中R1，R2和R3是低级烷基或卤代烷基，R4和R5是氢，低级烷基或卤代烷基; （c）所述酸选自：其中R 6，R 7，R 8和R 9是氢，低级烷基，卤代烷基或羟烷基，R 10和R 11是低级烷基，卤代烷基，羟基 - 聚亚烷基氧基，烷氧基，羟基烷氧基或卤代烷氧基，其中R12是低级亚烷基，卤代亚烷基，聚亚烷基氧基，羟基 - 亚烷基，R13和R14是氢，羟基，低级烷基，羟基 - 聚亚烷基氧基，烷氧基，羟基烷氧基或卤代烷氧基。

4. 发明授权

US4265791A Novel phosphoric acid 失效
标题翻译：新型磷酸
公开(公告)号：US4265791A
公开(公告)日：1981-05-05
申请号：US101323
申请日：1979-12-06
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C07F9/09 , C09D5/18 , C09K21/12 , C09K3/28
CPC分类号： C09K21/12 , C07F9/091 , C09D5/185
摘要： A compound of the formula ##STR1## wherein a, b, c, d, and n are integers; a is from 1 to 3; b and c are independently selected from the group consisting of 0 and 1; d and n are independently selected from the group consisting of 1 and 2; R.sup.1 and R.sup.4 are independently selected from the group consisting of hydrogen, alkyl of 1 to 4 carbon atoms and haloalkyl of 1 to 4 carbon atoms and 1 to 2 halogen atoms; and R.sup.2 and R.sup.3 are independently selected from the group consisting of haloalkyl containing 1 to about 4 carbon atoms and 1 to about 2 halogen atoms selected from the group consisting of chlorine, bromine, and mixtures thereof.The use of this compound with specified amounts of a certain methylated methylol melamine and water allows one to produce an intumescent composition which is substantially superior to prior art intumescent compositions.
摘要翻译：其中a，b，c，d和n是整数的式（Ⅰ）化合物：其中a，b，c，d和n是整数; a是1到3; b和c独立地选自0和1组成的组; d和n独立地选自1和2; R 1和R 4独立地选自氢，1至4个碳原子的烷基和1至4个碳原子的卤代烷基和1至2个卤素原子; 并且R 2和R 3独立地选自含有1至约4个碳原子的卤代烷基和1至约2个选自氯，溴及其混合物的卤素原子。使用具有特定量的某些甲基化羟甲基三聚氰胺和水的该化合物允许产生基本上优于现有技术的膨胀组合物的膨胀组合物。

5. 发明授权

US4104172A Durable flame retardant finishes for textile materials 失效
标题翻译：耐用的阻燃涂料用于纺织材料
公开(公告)号：US4104172A
公开(公告)日：1978-08-01
申请号：US660500
申请日：1976-02-23
申请人： Ray E. Smith , James A. Albright
发明人： Ray E. Smith , James A. Albright
IPC分类号： D06M13/285 , D06M13/295 , D06M13/298 , D06M13/322 , D06M15/673 , C09K3/28
CPC分类号： D06M15/673 , D06M13/285 , D06M13/295 , D06M13/298 , D06M13/322
摘要： Novel flame retardant finishes comprising a water soluble quaternary phosphonium salt, a water soluble organic nitrogen containing compound, a haloalkyl phosphate of the formula ##STR1## WHEREIN EACH X is independently selected from chlorine, bromine, and hydrogen, wherein a is an integer from 1 to 2, wherein n is an integer from 1 to 8, wherein m is an integer from 0 to n, provided that when n is 1, m is 0, and mixtures of said haloalkyl phosphates, an emulsifiying agent which is capable of passing the following three tests: (1) Solubility (Compatability) Test: said emulsifying agent (20 parts by weight) must be soluble in 80 parts by weight of said phosphate ester at less than or equal to 80.degree. C.; (2) Shelf Life Test: a blend of said emulsifying agent and said phosphate ester prepared as in the Solubility Test must remain in one clear homogeneous phase at 22.degree. C. for at least 1 hour; (3) Finish Formulation Test: a flame retardant finish within the scope of this invention is prepared and must remain in one homogeneous phase for a minimum of 1 hour at 20.degree. C. These flame retardant finishes are excellent for flame retarding textile materials including polyester/cotton blend fabrics.
摘要翻译：新型阻燃整理剂，其包含水溶性季鏻盐，水溶性有机氮化合物，每个X独立地选自式（ⅩⅩⅧ）的卤代烷基磷酸酯，其中a为1 至2，其中n为1至8的整数，其中m为0至n的整数，条件是当n为1时，m为0，所述卤代烷基磷酸酯的混合物为能够使以下三个试验：（1）溶解性（兼容性）试验：所述乳化剂（20重量份）在80℃以下必须溶于80重量份的所述磷酸酯中。（2）保质期测试：如在溶解性试验中制备的所述乳化剂和所述磷酸酯的共混物必须在22℃下保持在一个清澈的均匀相中至少1小时; （3）精加工试验：制备本发明范围内的阻燃整理剂，并且必须在20℃下保持在一个均相中至少1小时。这些阻燃整理剂对于阻燃纺织材料（包括聚酯）是优异的 /棉混纺面料。

6. 发明授权

US4088592A Durable flame retardant finishes for textile materials 失效
标题翻译：耐用的阻燃涂料用于纺织材料
公开(公告)号：US4088592A
公开(公告)日：1978-05-09
申请号：US660503
申请日：1976-02-23
申请人： Ray E. Smith
发明人： Ray E. Smith
IPC分类号： D06M13/285 , D06M13/295 , D06M13/298 , D06M13/322 , D06M15/673 , C09K3/28
CPC分类号： D06M15/673 , D06M13/285 , D06M13/295 , D06M13/298 , D06M13/322
摘要： Novel flame retardant finishes comprising a water soluble quaternary phosphonium salt, a water soluble organic nitrogen containing compound, a phosphate ester of haloalkanols, an emulsifying agent which is capable of passing the following three tests: (1) Solubility (Compatability) Test: said emulsifying agent (20 parts by weight) must be soluble in 80 parts by weight of said phosphate ester at less than or equal to 80.degree. C.; (2) Shelf Life Test: a blend of said emulsifying agent and said phosphate ester prepared as in the Solubility Test must remain in one clear homogeneous phase at 22.degree. C. for at least one hour; (3) Finish Formulation Test: a flame retardant finish within the scope of this invention is prepared and must remain in one homogeneous phase for a minimum of 1 hour at 20.degree. C., and water. These flame retardant finishes are excellent for flame retarding textile materials including polyester/cotton blend fabrics.
摘要翻译：新型阻燃整理剂，其包含水溶性季鏻盐，水溶性有机氮化合物，卤代烷醇的磷酸酯，能够通过以下三个试验的乳化剂：（1）溶解性（兼容性）试验：所述乳化试剂（20重量份）必须在小于或等于80℃下可溶于80重量份的所述磷酸酯。（2）保质期测试：如在溶解度试验中制备的所述乳化剂和所述磷酸酯的共混物必须在22℃下保持在一个清澈的均匀相中至少1小时; （3）精制配方试验：制备本发明范围内的阻燃剂整理剂，并且必须在20℃保持一个均相至少1小时和水。这些阻燃整理剂对于阻燃纺织材料（包括聚酯/棉混纺织物）是优异的。

7. 发明授权

US4015037A Durable flame retardant finishes for textile materials 失效
标题翻译：耐用的阻燃涂料用于纺织材料
公开(公告)号：US4015037A
公开(公告)日：1977-03-29
申请号：US660520
申请日：1976-03-22
申请人： Ray E. Smith , James A. Albright
发明人： Ray E. Smith , James A. Albright
IPC分类号： D06M13/285 , D06M13/295 , D06M13/298 , D06M15/673 , D06M23/06 , C09D1/00
CPC分类号： D06M13/285 , D06M13/295 , D06M13/298 , D06M15/673 , D06M23/06 , Y10S428/921 , Y10T442/2697
摘要： Novel flame retardant finishes comprising a water soluble quaternary phosphonium salt, a water soluble organic nitrogen containing compound, a haloalkyl phosphate of the formula ##STR1## WHEREIN EACH X is independently selected from chlorine, bromine, and hydrogen, wherein a is an integer from 1 to 2, wherein n is an integer from 1 to 8, and wherein m is an integer from 0 to n, provided that when n is 1, m is 0, an organic solvent characterized by having a flash point of at least 80.degree. F. and a boiling point within the range of about 300.degree. to about 350.degree. F., an emulsifier having a hydrophile lipophile balance value of from about 10 to about 14, and water. These flame retardant finishes are excellent for flame retarding textile materials including polyester/cotton blend fabrics.
摘要翻译：新型阻燃整理剂，其包含水溶性季鏻盐，水溶性有机氮化合物，每个X独立地选自式（ⅩⅩⅧ）的卤代烷基磷酸酯，其中a为1 至2，其中n为1至8的整数，并且其中m为0至n的整数，条件是当n为1时，m为0，特征在于闪点为至少80°F的有机溶剂沸点在约300至约350°F范围内，具有约10至约14的亲水亲油平衡值的乳化剂和水。这些阻燃整理剂对于阻燃纺织材料（包括聚酯/棉混纺织物）是优异的。

8. 发明授权

US4339357A Intumescent composition 失效
标题翻译：膨胀成分
公开(公告)号：US4339357A
公开(公告)日：1982-07-13
申请号：US76049
申请日：1979-09-17
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C07F9/09 , C09D5/18
CPC分类号： C09D5/185 , C07F9/091
摘要： A compound of the formula ##STR1## wherein a, b, c, d, and n are integers; a is from 1 to 3; b and c are independently selected from the group consisting of 0 and 1; d and n are independently selected from the group consisting of 1 and 2; R.sup.1 and R.sup.4 are independently selected from the group consisting of hydrogen, alkyl of 1 to 4 carbon atoms and haloalkyl of 1 to 4 carbon atoms and 1 to 2 halogen atoms; and R.sup.2 and R.sup.3 are independently selected from the group consisting of haloalkyl containing 1 to about 4 carbon atoms and 1 to about 2 halogen atoms selected from the group consisting of chlorine, bromine, and mixtures thereof.The use of this compound with specified amounts of a certain methylated methylol melamine and water allows one to produce an intumescent composition which is substantially superior to prior art intumescent compositions.
摘要翻译：其中a，b，c，d和n是整数的式（Ⅰ）化合物：其中a，b，c，d和n是整数; a是1到3; b和c独立地选自0和1组成的组; d和n独立地选自1和2; R 1和R 4独立地选自氢，1至4个碳原子的烷基和1至4个碳原子的卤代烷基和1至2个卤素原子; 并且R 2和R 3独立地选自含有1至约4个碳原子的卤代烷基和1至约2个选自氯，溴及其混合物的卤素原子。使用具有特定量的某些甲基化羟甲基三聚氰胺和水的该化合物允许产生基本上优于现有技术的膨胀组合物的膨胀组合物。

9. 发明授权

US4201593A Novel intumescent composition 失效
标题翻译：新型膨胀成分
公开(公告)号：US4201593A
公开(公告)日：1980-05-06
申请号：US966930
申请日：1978-12-06
申请人： Kenneth J. Sienkowski , Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Kenneth J. Sienkowski , Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C09D5/18 , C09K21/00 , C09K21/12
CPC分类号： C09K21/00 , C09D5/185 , C09K21/12
摘要： An intumescent composition comprising a hydroxyalkyl amino alkyl phosphonic acid, a cyclic nitrogen compound, and water, wherein said phosphonic acid is selected from the group consisting of ##STR1## wherein x, y, and n are integers independently selected from the group consisting of 1 and 2, q is an integer selected from the group consisting of 1, 2, and 3, z is an integer selected from the group consisting of 0 and 1, R.sup.1 and R.sup.2 are independently selected from the group consisting of hydrogen, alkyl radicals containing from about 1 to about 6 carbon atoms, and haloalkyl radicals containing from about 1 to about 6 carbon atoms, and R.sup.3 is selected from the group consisting of alkyl radicals containing from about 1 to about 6 carbon atoms and haloalkyl radicals containing from about 3 to about 6 carbon atoms, provided that the total number of carbon atoms in the R.sup.1, R.sup.2, and R.sup.3 groups does not exceed about 14; and wherein said cyclic nitrogen compound is ##STR2## wherein a, b, and c are integers selected from the group consisting of 1 and 2, a plus b plus c equal about 3 to 6, and X, X', and X" are independently selected from the group consisting of hydrogen and --CH.sub.3.
摘要翻译：包含羟烷基氨基烷基膦酸，环状氮化合物和水的膨胀组合物，其中所述膦酸选自由下列组成的组：其中x，y和n是独立地选自基团由1和2组成，q是选自1,2和3的整数，z是选自0和1的整数，R 1和R 2独立地选自氢，含有约1至约6个碳原子的烷基和含有约1至约6个碳原子的卤代烷基，R 3选自含有约1至约6个碳原子的烷基和含有约3至约6个碳原子，条件是R1，R2和R3基团中的碳原子总数不超过约14; 并且其中所述环状氮化合物是其中a，b和c是选自1和2，a加b加c等于约3至6的整数，X，X'和X“ 独立地选自氢和-CH 3。

10. 发明授权

US4092251A Durable flame retardant finishes for textile materials 失效
标题翻译：耐用的阻燃涂料用于纺织材料
公开(公告)号：US4092251A
公开(公告)日：1978-05-30
申请号：US660501
申请日：1976-02-23
申请人： Ray E. Smith
发明人： Ray E. Smith
IPC分类号： D06M13/285 , D06M13/298 , D06M13/322 , C09K3/28
CPC分类号： D06M13/322 , D06M13/285 , D06M13/298
摘要： Novel flame retardant finishes comprising a water soluble quaternary phosphonium salt, a water soluble organic nitrogen containing compound, a phosphate ester of haloalkanols, an organic solvent characterized by having a flash point of at least 80.degree. F. and a boiling point within the range of about 300.degree. to about 350.degree. F., an emulsifier having a hydrophile lipophile balance value of from about 10 to about 14, and water. These flame retardant finishes are excellent for flame retarding textile materials including polyester/cotton blend fabrics.
摘要翻译：新型阻燃整理剂，其包含水溶性季鏻盐，水溶性有机氮化合物，卤代烷醇的磷酸酯，有机溶剂的特征在于闪点至少为80°F，沸点在约300至约350°F，亲水亲油平衡值为约10至约14的乳化剂和水。这些阻燃整理剂对于阻燃纺织材料（包括聚酯/棉混纺织物）是优异的。

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