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1. 发明授权

US4201593A Novel intumescent composition 失效
标题翻译：新型膨胀成分
公开(公告)号：US4201593A
公开(公告)日：1980-05-06
申请号：US966930
申请日：1978-12-06
申请人： Kenneth J. Sienkowski , Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Kenneth J. Sienkowski , Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C09D5/18 , C09K21/00 , C09K21/12
CPC分类号： C09K21/00 , C09D5/185 , C09K21/12
摘要： An intumescent composition comprising a hydroxyalkyl amino alkyl phosphonic acid, a cyclic nitrogen compound, and water, wherein said phosphonic acid is selected from the group consisting of ##STR1## wherein x, y, and n are integers independently selected from the group consisting of 1 and 2, q is an integer selected from the group consisting of 1, 2, and 3, z is an integer selected from the group consisting of 0 and 1, R.sup.1 and R.sup.2 are independently selected from the group consisting of hydrogen, alkyl radicals containing from about 1 to about 6 carbon atoms, and haloalkyl radicals containing from about 1 to about 6 carbon atoms, and R.sup.3 is selected from the group consisting of alkyl radicals containing from about 1 to about 6 carbon atoms and haloalkyl radicals containing from about 3 to about 6 carbon atoms, provided that the total number of carbon atoms in the R.sup.1, R.sup.2, and R.sup.3 groups does not exceed about 14; and wherein said cyclic nitrogen compound is ##STR2## wherein a, b, and c are integers selected from the group consisting of 1 and 2, a plus b plus c equal about 3 to 6, and X, X', and X" are independently selected from the group consisting of hydrogen and --CH.sub.3.
摘要翻译：包含羟烷基氨基烷基膦酸，环状氮化合物和水的膨胀组合物，其中所述膦酸选自由下列组成的组：其中x，y和n是独立地选自基团由1和2组成，q是选自1,2和3的整数，z是选自0和1的整数，R 1和R 2独立地选自氢，含有约1至约6个碳原子的烷基和含有约1至约6个碳原子的卤代烷基，R 3选自含有约1至约6个碳原子的烷基和含有约3至约6个碳原子，条件是R1，R2和R3基团中的碳原子总数不超过约14; 并且其中所述环状氮化合物是其中a，b和c是选自1和2，a加b加c等于约3至6的整数，X，X'和X“ 独立地选自氢和-CH 3。

2. 发明授权

US4345002A Novel intumescent composition and flame retardant articles treated therewith 失效
标题翻译：新型膨胀组合物和用其处理的阻燃制品
公开(公告)号：US4345002A
公开(公告)日：1982-08-17
申请号：US76041
申请日：1979-09-17
申请人： Ray E. Smith , Jayendra G. Shukla , Richard R. Nicholson
发明人： Ray E. Smith , Jayendra G. Shukla , Richard R. Nicholson
IPC分类号： C07D251/70 , C07F9/09 , C07F9/146 , C07F9/24 , C09D5/18 , C09K21/10 , C09K21/12 , D06M15/673 , D04H1/58
CPC分类号： D06M15/673 , C07D251/70 , C07F9/091 , C07F9/146 , C07F9/2408 , C07F9/2458 , C09D5/185 , C09K21/10 , C09K21/12 , Y10S428/913 , Y10S428/921 , Y10T428/2938 , Y10T428/3196 , Y10T428/31967
摘要： An intumescent composition containing a cyclic nitrogen compound, a hydroxy-containing organo-phosphorus compound, an organo-phosphorus acid, and water, wherein:(a) said cyclic nitrogen compound is: ##STR1## wherein a, b, and c, are integers selected from the group consisting of 1 and 2, a plus b plus c equal about 3 to 6, and wherein and X, X', and X" are hydrogen or --CH.sub.3 ;(b) said hydroxy-containing organo-phosphorus compound is selected from the group consisting of: ##STR2## and mixtures thereof wherein R.sup.1, R.sup.2 and R.sup.3 are lower alkyl or haloalkyl radicals and R.sup.4 and R.sup.5 are hydrogen, lower alkyl or haloalkyl radicals;(c) said acid is selected from the group consisting of: ##STR3## and mixtures thereof, wherein R.sup.6, R.sup.7, R.sup.8 and R.sup.9 are hydrogen, lower alkyl, haloalkyl or hydroxyalkyl, R.sup.10 and R.sup.11 are lower alkyl, haloalkyl, hydroxy-polyalkyleneoxy, alkoxy, hydroxyalkoxy or haloalkoxy, ##STR4## wherein R.sup.12 is lower alkylene, haloalkylene, polyalkyleneoxy, hydroxy-alkylene and R.sup.13 and R.sup.14 are hydrogen, hydroxyl, lower alkyl, hydroxy-polyalkyleneoxy, alkoxy, hydroxyalkoxy or haloalkoxy.
摘要翻译：包含环状氮化合物，含羟基的有机磷化合物，有机磷酸和水的膨胀性组合物，其中：（a）所述环状氮化合物是：其中a，b和c分别为选自1和2，a加b加c等于3至6的整数，并且其中X，X'和X“是氢或-CH 3; （b）所述含羟基的有机磷化合物选自：其中R1，R2和R3是低级烷基或卤代烷基，R4和R5是氢，低级烷基或卤代烷基; （c）所述酸选自：其中R 6，R 7，R 8和R 9是氢，低级烷基，卤代烷基或羟烷基，R 10和R 11是低级烷基，卤代烷基，羟基 - 聚亚烷基氧基，烷氧基，羟基烷氧基或卤代烷氧基，其中R12是低级亚烷基，卤代亚烷基，聚亚烷基氧基，羟基 - 亚烷基，R13和R14是氢，羟基，低级烷基，羟基 - 聚亚烷基氧基，烷氧基，羟基烷氧基或卤代烷氧基。

3. 发明授权

US4265791A Novel phosphoric acid 失效
标题翻译：新型磷酸
公开(公告)号：US4265791A
公开(公告)日：1981-05-05
申请号：US101323
申请日：1979-12-06
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C07F9/09 , C09D5/18 , C09K21/12 , C09K3/28
CPC分类号： C09K21/12 , C07F9/091 , C09D5/185
摘要： A compound of the formula ##STR1## wherein a, b, c, d, and n are integers; a is from 1 to 3; b and c are independently selected from the group consisting of 0 and 1; d and n are independently selected from the group consisting of 1 and 2; R.sup.1 and R.sup.4 are independently selected from the group consisting of hydrogen, alkyl of 1 to 4 carbon atoms and haloalkyl of 1 to 4 carbon atoms and 1 to 2 halogen atoms; and R.sup.2 and R.sup.3 are independently selected from the group consisting of haloalkyl containing 1 to about 4 carbon atoms and 1 to about 2 halogen atoms selected from the group consisting of chlorine, bromine, and mixtures thereof.The use of this compound with specified amounts of a certain methylated methylol melamine and water allows one to produce an intumescent composition which is substantially superior to prior art intumescent compositions.
摘要翻译：其中a，b，c，d和n是整数的式（Ⅰ）化合物：其中a，b，c，d和n是整数; a是1到3; b和c独立地选自0和1组成的组; d和n独立地选自1和2; R 1和R 4独立地选自氢，1至4个碳原子的烷基和1至4个碳原子的卤代烷基和1至2个卤素原子; 并且R 2和R 3独立地选自含有1至约4个碳原子的卤代烷基和1至约2个选自氯，溴及其混合物的卤素原子。使用具有特定量的某些甲基化羟甲基三聚氰胺和水的该化合物允许产生基本上优于现有技术的膨胀组合物的膨胀组合物。

4. 发明授权

US4339357A Intumescent composition 失效
标题翻译：膨胀成分
公开(公告)号：US4339357A
公开(公告)日：1982-07-13
申请号：US76049
申请日：1979-09-17
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C07F9/09 , C09D5/18
CPC分类号： C09D5/185 , C07F9/091
摘要： A compound of the formula ##STR1## wherein a, b, c, d, and n are integers; a is from 1 to 3; b and c are independently selected from the group consisting of 0 and 1; d and n are independently selected from the group consisting of 1 and 2; R.sup.1 and R.sup.4 are independently selected from the group consisting of hydrogen, alkyl of 1 to 4 carbon atoms and haloalkyl of 1 to 4 carbon atoms and 1 to 2 halogen atoms; and R.sup.2 and R.sup.3 are independently selected from the group consisting of haloalkyl containing 1 to about 4 carbon atoms and 1 to about 2 halogen atoms selected from the group consisting of chlorine, bromine, and mixtures thereof.The use of this compound with specified amounts of a certain methylated methylol melamine and water allows one to produce an intumescent composition which is substantially superior to prior art intumescent compositions.
摘要翻译：其中a，b，c，d和n是整数的式（Ⅰ）化合物：其中a，b，c，d和n是整数; a是1到3; b和c独立地选自0和1组成的组; d和n独立地选自1和2; R 1和R 4独立地选自氢，1至4个碳原子的烷基和1至4个碳原子的卤代烷基和1至2个卤素原子; 并且R 2和R 3独立地选自含有1至约4个碳原子的卤代烷基和1至约2个选自氯，溴及其混合物的卤素原子。使用具有特定量的某些甲基化羟甲基三聚氰胺和水的该化合物允许产生基本上优于现有技术的膨胀组合物的膨胀组合物。

5. 发明授权

US4221837A Flame retardant article 失效
标题翻译：阻燃制品
公开(公告)号：US4221837A
公开(公告)日：1980-09-09
申请号：US75863
申请日：1979-09-17
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C09D5/18 , D04H1/58
CPC分类号： C09D5/185 , Y10S428/921 , Y10T428/31989 , Y10T428/31993 , Y10T442/2648
摘要： Disclosed is a flame retardant article comprised of an article treated with a flame-retardingly effective amount of an intumescent composition comprising a cyclic nitrogen compound, a phosphorous polyol, a phosphorous acid and water.
摘要翻译：公开了一种阻燃制品，其由用阻燃有效量的包含环状氮化合物，磷多元醇，亚磷酸和水的膨胀组合物处理的制品组成。

6. 发明授权

US4210452A Novel intumescent composition 失效
标题翻译：新型膨胀成分
公开(公告)号：US4210452A
公开(公告)日：1980-07-01
申请号：US966931
申请日：1978-12-06
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C09D5/18
CPC分类号： C09D5/185 , Y10S260/24 , Y10S428/921
摘要： There is provided an intumescent composition comprising a cyclic nitrogen compound, a phosphorus polyol, a phosphorus acid, and water.
摘要翻译：提供了包含环状氮化合物，磷多元醇，磷酸和水的膨胀组合物。

7. 发明授权

US4205022A 2,2-Bis(haloalkyl)-3-hydroxy-1-propyl phosphoric acids 失效
标题翻译： 2,2-二（卤代烷基）-3-羟基-1-丙基磷酸
公开(公告)号：US4205022A
公开(公告)日：1980-05-27
申请号：US939629
申请日：1978-09-05
申请人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
发明人： Richard R. Nicholson , Ray E. Smith , Jayendra G. Shukla
IPC分类号： C07F9/09 , C09D5/18
CPC分类号： C09D5/185 , C07F9/091
摘要： A compound of the formula ##STR1## wherein a, b, c, d, and n are integers; a is from 1 to 3; b and c are independently selected from the group consisting of 0 and 1; d and n are independently selected from the group consisting of 1 and 2; R.sup.1 and R.sup.4 are independently selected from the group consisting of hydrogen, alkyl of 1 to 4 carbon atoms and haloalkyl of 1 to 4 carbon atoms and 1 to 2 halogen atoms; and R.sup.2 and R.sup.3 are independently selected from the group consisting of haloalkyl containing 1 to about 4 carbon atoms and 1 to about 2 halogen atoms selected from the group consisting of chlorine, bromine, and mixtures thereof.The use of this compound with specified amounts of a certain methylated methylol melamine and water allows one to produce an intumescent composition which is substantially superior to prior art intumescent compositions.
摘要翻译：其中a，b，c，d和n是整数的式IMAMA的化合物; a是1到3; b和c独立地选自0和1组成的组; d和n独立地选自1和2; R 1和R 4独立地选自氢，1至4个碳原子的烷基和1至4个碳原子的卤代烷基和1至2个卤素原子; 并且R 2和R 3独立地选自含有1至约4个碳原子的卤代烷基和1至约2个选自氯，溴及其混合物的卤素原子。使用具有特定量的某些甲基化羟甲基三聚氰胺和水的该化合物允许产生基本上优于现有技术的膨胀组合物的膨胀组合物。

8. 发明授权

US4201677A Intumescent composition comprising cyclic nitrogen compound and phosphorus compounds 失效
标题翻译：包含环状氮化合物和磷化合物的膨胀组合物
公开(公告)号：US4201677A
公开(公告)日：1980-05-06
申请号：US939625
申请日：1978-09-05
申请人： Jayendra G. Shukla , Ray E. Smith , Richard R. Nicholson
发明人： Jayendra G. Shukla , Ray E. Smith , Richard R. Nicholson
IPC分类号： B27K3/50 , C07D251/70 , C09D5/18 , C09K21/10 , C09K21/12 , D06M15/673 , C09K3/28
CPC分类号： C07D251/70 , C09D5/185 , C09K21/10 , C09K21/12 , D06M15/673 , Y10S428/921 , Y10T428/662
摘要： An intumescent composition comprising a cyclic nitrogen compound, an acid selected from the group consisting of phosphorous acid, phosphoric acid, and mixtures thereof, water, and an hydroxy-containing organo-phosphorus compound, wherein:(a) said cyclic nitrogen compound is ##STR1## wherein a, b, and c are integers selected from the group consisting of 1 and 2, a plus b plus c equal about 3 to 6, and X, X', and X" are independently selected from the group consisting of hydrogen and --CH.sub.3 ;(b) said hydroxy-containing organo-phosphorus compound is selected from the group consisting of ##STR2## and mixtures thereof, wherein d is an integer of from 0 to 2, e is an integer of from 0 to 2, f is an integer of from 1 to 3, and d plus e plus f equal 3; z is an integer of 0 to 1; x is an integer of 1 to 2, y is an integer of 1 to 2, and x plus y plus z equal 3; R.sup.1, R.sup.2, and R.sup.3 are selected from the group consisting of alkyl radicals containing from about 1 to about 6 carbon atoms and haloalkyl radicals containing from about 2 to about 6 carbon atoms, provided that when R.sup.3 is haloalkyl it contains at least 3 carbon atoms; R.sup.4 and R.sup.5 are selected from the group consisting of hydrogen, alkyl radicals, and haloalkyl radicals, wherein said radicals contain from about 1 to about 6 carbon atoms; and the total number of carbon atoms in the R.sup.1, R.sup.2, R.sup.3, R.sup.4, and R.sup.5 groups does not exceed about 14.
摘要翻译：一种膨胀性组合物，其包含环状氮化合物，选自亚磷酸，磷酸及其混合物的水，水和含羟基的有机磷化合物，其中：（a）所述环状氮化合物是其中a，b和c是选自1和2，a + b加c等于3至6的整数，X，X'和X“独立地选自氢和-CH 3; （b）所述含羟基的有机磷化合物选自由下列组成的组：其中d为0-2的整数，e为0的整数至2，f为1至3的整数，d加e加f等于3; z为0〜1的整数; x为1〜2的整数，y为1〜2的整数，x + y + z为3的整数。 R1，R2和R3选自包含约1至约6个碳原子的烷基和含有约2至约6个碳原子的卤代烷基，条件是当R3为卤代烷基时，其含有至少3个碳原子 ; R 4和R 5选自氢，烷基和卤代烷基，其中所述基团含有约1至约6个碳原子; 并且R1，R2，R3，R4和R5基团中的碳原子总数不超过约14。

9. 发明授权

US4226907A Flame retardant article 失效
标题翻译：阻燃制品
公开(公告)号：US4226907A
公开(公告)日：1980-10-07
申请号：US76098
申请日：1979-09-17
申请人： Kenneth J. Sienkowski , Richard R. Nicholson , Ray E. Smith
发明人： Kenneth J. Sienkowski , Richard R. Nicholson , Ray E. Smith
IPC分类号： C09D5/18 , C09K21/12 , D04H1/58
CPC分类号： C09D5/185 , C09K21/12 , Y10S428/921 , Y10T428/31989 , Y10T442/268
摘要： Disclosed is a flame retardant article comprising an article treated with a flame-retardingly effective amount of an intumescent composition comprising a hydroxyalkyl amino alkyl phosphonic acid, a cyclic nitrogen compound and water.
摘要翻译：公开了一种阻燃制品，其包括用阻燃有效量的包含羟烷基氨基烷基膦酸，环状氮化合物和水的膨胀组合物处理的制品。

10. 发明授权

US4174328A Flame retarded non-woven textile material comprised of flame retardant and vinyl chloride latex 失效
标题翻译：由阻燃和氯乙烯胶乳组成的阻燃无纺布材料
公开(公告)号：US4174328A
公开(公告)日：1979-11-13
申请号：US934123
申请日：1978-08-16
申请人： Ray E. Smith , Jayendra G. Shukla
发明人： Ray E. Smith , Jayendra G. Shukla
IPC分类号： D06M13/10 , D04H1/64 , D06M13/02 , D06M15/244 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/08 , D06M101/16 , D06M101/18 , D06M101/30 , D06M101/32 , C08L1/02
CPC分类号： D06M15/244 , D04H1/587 , D04H1/64
摘要： There is provided a flame-retarded non-woven material which contains a mixture of flame retardant and vinyl chloride latex, wherein said flame retardant is selected from the group consisting of ##STR1## wherein a and b are integers independently selected from the group consisting of 1, 2, 3, 4 and 5, a plus b is from about 6 to about 10, c is an integer of from 1 to 4, and alkylene is a straight chain carbon group having from one to six carbon atoms; and wherein more than 50 percent (by weight) of said flame retardant consists of particles with a diameter of from about 2 to about 25 microns.
摘要翻译：提供了含有阻燃剂和氯乙烯胶乳的混合物的阻燃非织造材料，其中所述阻燃剂选自由下列组成的组：其中a和b是独立选择的整数由1,2,3,4和5组成的组合，a为约6至约10，c为1至4的整数，亚烷基为具有1至6个碳原子的直链碳基团原子并且其中大于50重量％的所述阻燃剂由直径为约2至约25微米的颗粒组成。

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