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1. 发明授权

US08603199B2 Method to upgrade bio-oils to fuel and bio-crude 有权
标题翻译：将生物油升级为燃料和生物原油的方法
公开(公告)号：US08603199B2
公开(公告)日：2013-12-10
申请号：US12896741
申请日：2010-10-01
申请人： Philip H. Steele , Charles U. Pittman, Jr. , Leonard L. Ingram, Jr. , Sanjeev Gajjela , Zhijun Zhang , Priyanka Bhattacharya
发明人： Philip H. Steele , Charles U. Pittman, Jr. , Leonard L. Ingram, Jr. , Sanjeev Gajjela , Zhijun Zhang , Priyanka Bhattacharya
IPC分类号： C10L1/18
CPC分类号： C10L1/02 , B01J21/12 , B01J23/755 , C10C5/00 , C10G2300/1011 , C10K1/04 , Y02E50/13 , Y02E50/14 , Y02E50/32 , Y02P30/20
摘要： This invention relates to a method and device to produce esterified, olefinated/esterified, or thermochemolytic reacted bio-oils as fuels. The olefinated/esterified product may be utilized as a biocrude for input to a refinery, either alone or in combination with petroleum crude oils. The bio-oil esterification reaction is catalyzed by addition of alcohol and acid catalyst. The olefination/esterification reaction is catalyzed by addition of resin acid or other heterogeneous catalyst to catalyze olefins added to previously etherified bio-oil; the olefins and alcohol may also be simultaneously combined and catalyzed by addition of resin acid or other heterogeneous catalyst to produce the olefinated/esterified product.
摘要翻译：本发明涉及一种生产酯化，烯化/酯化或热溶解反应的生物油作为燃料的方法和装置。烯化/酯化产物可以单独使用或与石油原油组合用作输入炼油厂的生物重油。通过加入醇和酸催化剂催化生物油酯化反应。烯化/酯化反应通过加入树脂酸或其他非均相催化剂催化加入到先前醚化生物油中的烯烃催化; 烯烃和醇也可以通过加入树脂酸或其它非均相催化剂同时组合和催化，以产生烯化/酯化产物。

2. 发明授权

US07820285B1 Rocket motor insulation 有权
标题翻译：火箭发动机绝缘
公开(公告)号：US07820285B1
公开(公告)日：2010-10-26
申请号：US11357465
申请日：2006-02-10
申请人： Charles U. Pittman, Jr. , Rusty L. Blanski , Joseph H. Koo , Patrick N. Ruth , Shawn H. Phillips
发明人： Charles U. Pittman, Jr. , Rusty L. Blanski , Joseph H. Koo , Patrick N. Ruth , Shawn H. Phillips
IPC分类号： B32B5/02
CPC分类号： F02K9/974 , F05D2300/224 , F05D2300/614 , Y10T428/251
摘要： Provided is a solid rocket motor (SRM) insulation, wherein carbon nano fibers (CNF) are blended into a polyurethane matrix so as to disperse the CNF in the polymer. The so blended material is then extruded, injection molded or sprayed on or into the desired shape. Such SRM insulation has reduced ablation over prior art insulations, resulting in reduction in weight of the insulation needed in such rockets, permitting increase of payload therein.
摘要翻译：提供了一种固体火箭发动机（SRM）绝缘体，其中将碳纳米纤维（CNF）共混到聚氨酯基质中，以将CNF分散在聚合物中。然后将如此混合的材料挤出，注塑或喷涂到所需形状上或其上。这种SRM绝缘材料已经消除了现有技术的绝缘体，从而减少了这种火箭所需的绝缘重量，从而增加了其中的有效载荷。

3. 发明授权

US07144849B2 Cleaning solutions including nucleophilic amine compound having reduction and oxidation potentials 失效
公开(公告)号：US07144849B2
公开(公告)日：2006-12-05
申请号：US11181747
申请日：2005-07-15
申请人： Wai Mun Lee , Charles U. Pittman, Jr. , Robert J. Small
发明人： Wai Mun Lee , Charles U. Pittman, Jr. , Robert J. Small
IPC分类号： C11D7/26 , C11D7/32 , C11D7/50
CPC分类号： G03F7/425 , C11D7/261 , C11D7/3218 , C11D7/3227 , C11D7/3245 , C11D7/3263 , C11D7/34 , C11D7/5009 , C11D7/5013 , C11D7/5022 , C11D11/0047 , C23G1/18
摘要： A composition for removing resists and etching residue from substrates containing at least one nucleophilic amine compound having oxidation and reduction potentials, at least one organic solvent, water and, optionally, a chelating agent is described. The chelating agent is preferred to be included since it provides added stability and activity to the cleaning composition so that the composition has long term effectiveness. If a chelating agent is not present, the composition, while providing for adequate stripping and cleaning upon initial use of the composition following mixing, has only short term stability. In this latter instance, the nucleophilic amine compound and organic solvent components of the composition preferably are maintained separate from each other until it is desired to use the composition. Thereafter, the components are combined. Following use of the composition, the non-used portion of the composition can be disposed of or be reactivated by the addition of a chelating agent.

4. 发明授权

US06319885B1 Cleaning solutions including nucleophilic amine compound having reduction and oxidation potentials 失效
标题翻译：包括具有还原和氧化电位的亲核胺化合物的清洁溶液
公开(公告)号：US06319885B1
公开(公告)日：2001-11-20
申请号：US09603693
申请日：2000-06-26
申请人： Wai Mun Lee , Charles U. Pittman, Jr. , Robert J. Small
发明人： Wai Mun Lee , Charles U. Pittman, Jr. , Robert J. Small
IPC分类号： C11D162
CPC分类号： H01L21/02071 , B24B37/042 , C09D9/00 , C11D3/2058 , C11D3/2065 , C11D3/2086 , C11D3/30 , C11D3/3427 , C11D3/3472 , C11D3/43 , C11D7/261 , C11D7/262 , C11D7/263 , C11D7/265 , C11D7/267 , C11D7/32 , C11D7/3209 , C11D7/3218 , C11D7/3227 , C11D7/3245 , C11D7/3254 , C11D7/3263 , C11D7/3272 , C11D7/3281 , C11D7/34 , C11D7/5013 , C11D11/0047 , C11D11/0052 , C23G1/103 , C23G1/205 , G03F7/42 , G03F7/423 , G03F7/425 , H01L21/02052 , H01L21/02063 , H01L21/31133 , H01L21/76802 , H01L21/76885
摘要： A composition for removing resists and etching residue from substrates containing at least one nucleophilic amine compound having oxidation and reduction potentials, at least one organic solvent, water and, optionally, a chelating agent is described. The chelating agent is preferred to be included since it provides added stability and activity to the cleaning composition so that the composition has long term effectiveness. If a chelating agent is not present, the composition, while providing for adequate stripping and cleaning upon initial use of the composition following mixing, has only short term stability. In this latter instance, the nucleophilic amine compound and organic solvent components of the composition preferably are maintained separate from each other until it is desired to use the composition. Thereafter, the components are combined. Following use of the composition, the non-used portion of the composition can be disposed of or be reactivated by the addition of a chelating agent.
摘要翻译：描述了用于去除抗蚀剂并从含有至少一种具有氧化和还原电位的亲核胺化合物的底物蚀刻残余物的组合物，至少一种有机溶剂，水和任选的螯合剂。优选包含螯合剂，因为它为清洁组合物提供了增加的稳定性和活性，使得组合物具有长期有效性。如果不存在螯合剂，组合物在混合后初始使用组合物时提供足够的剥离和清洁，仅具有短期的稳定性。在后一种情况下，组合物的亲核胺化合物和有机溶剂组分优选彼此保持分开，直到期望使用该组合物。此后，组合组件。使用组合物后，组合物的未使用部分可以通过加入螯合剂来处理或再活化。

5. 发明授权

US5254665A Ammeline-melamine-formaldehyde resins (AMFR) and method of preparation 失效
标题翻译： Ammeline-三聚氰胺 - 甲醛树脂（AMFR）及其制备方法
公开(公告)号：US5254665A
公开(公告)日：1993-10-19
申请号：US933815
申请日：1992-08-24
申请人： George M. Crews , Shen Ji , Charles U. Pittman, Jr. , Ruicheng Ran
发明人： George M. Crews , Shen Ji , Charles U. Pittman, Jr. , Ruicheng Ran
IPC分类号： C08G12/26 , C08G12/32 , C08G12/30
CPC分类号： C08G12/32
摘要： Ammeline-melamine-formaldehyde resins (AMFR) containing from 5-100% ammeline were synthesized by the polymerization of the sodium salt of ammeline, which must be made in advance, melamine, and formaldehyde in basic medium (pH=9.2-10.0). In this copolymerization, it is possible to make uniform random AMFR resins with any mole ratio of ammeline salt to melamine. Preferably the AMFR resin will contain from 5-10% ammeline. As an "ionomer" or a "polyelectrolyte," both the solid and solution properties of these resins (such as melting temperature, solubility, solution stability, etc.) depended directly on the mole ratio of ammeline to melamine and formaldehyde, and/or on the pH value of the medium in which the AMFR resin was present. The pH value controlled the ammeline rings/ammeline's salt groups and also the ratio of unprotonated to protonated amino groups on both the melamine and ammeline rings.These polymers have different solubilities, cloud points and solution lifetimes (which depend on pH) than melamine-formaldehyde resins. AMFR systems containing from 5-10% ammeline are more flexible than MFR resins and exhibit different adhesion properties than MFR resins.

6. 发明授权

US4377719A 1,7-Octadiene synthesis 失效
标题翻译： 1,7-辛二烯合成
公开(公告)号：US4377719A
公开(公告)日：1983-03-22
申请号：US969159
申请日：1978-12-13
申请人： Charles U. Pittman, Jr. , Ronald Hanes
发明人： Charles U. Pittman, Jr. , Ronald Hanes
IPC分类号： C07C2/74 , C07C6/00
CPC分类号： C07C2/74 , C07C2531/04 , C07C2531/24
摘要： A process for preparing 1,7-octadiene by dimerizing butadiene in the presence of a catalytic amount of palladium acetate and a tertiary phosphine, a solvent in an amount sufficient to dissolve the catalyst, a strong base and formic acid, wherein: (a) the molar ratio of the strong base to the formic acid is 1:1-2, (b) the mole ratio of tertiary phosphine to palladium is at least 1, (c) the amount of strong base present is such that the pH of the reaction medium is from 7.5 to 10.5 and (d) the solvent is at least one member selected from the group consisting of aromatic hydrocarbons, lower alkyl substituted aromatic hydrocarbon, halogenated aromatic hydrocarbons, halogenated lower aliphatic hydrocarbons, nitriles, amides, dilower alkyl ethers, lower alkyl phenyl ethers, lower alkyl esters of lower alkanoic acids, ketones and lower alkanols.
摘要翻译：在催化量的乙酸钯和叔膦，溶剂量足以溶解催化剂的溶剂，强碱和甲酸的存在下，使丁二烯二聚制备1,7-辛二烯的方法，其中：（a）强碱与甲酸的摩尔比为1：1-2，（b）叔膦与钯的摩尔比至少为1，（c）存在的强碱的量使得反应介质为7.5〜10.5，（d）溶剂为选自芳香烃，低级烷基取代芳香烃，卤代芳香烃，卤代低级脂族烃，腈，酰胺，二氟烷基醚中的至少一种，低级烷基苯基醚，低级链烷酸的低级烷基酯，酮和低级链烷醇。

7. 发明授权

US4304840A Method of delineating a desired integrated circuit pattern upon a circuit substrate 失效
标题翻译：在电路基板上划定期望的集成电路图案的方法
公开(公告)号：US4304840A
公开(公告)日：1981-12-08
申请号：US152261
申请日：1980-05-22
申请人： John N. Helbert , Charles U. Pittman, Jr.
发明人： John N. Helbert , Charles U. Pittman, Jr.
IPC分类号： G03F7/039 , G03F7/16 , G03C5/00
CPC分类号： G03F7/039 , G03F7/162 , Y10S430/143 , Y10S430/168
摘要： A method is disclosed of delineating a desired integrated circuit pattern upon a circuit substrate. According to the method, the copolymer poly(methyl alpha-chloroacrylate-co-methacrylonitrile) is formed by emulsion polymerization techniques. The copolymer is then dissolved in a spinning solvent that will dissolve the copolymer and form a viscous solution. The solution is applied to the surface of the substrate and the substrate spinned to form a smooth, uniform resist film of about 0.3 to 1.0 micron in thickness. The resist film is heated and the region of the resist film to be patterned then exposed to ionizing radiation until exposures greater than 1.5.times.10.sup.-5 C/cm.sup.2 are obtained. The exposed regions of the resist are then developed to the substrate.
摘要翻译：公开了一种在电路基板上划定期望的集成电路图案的方法。根据该方法，通过乳液聚合技术形成共聚物聚（α-氯丙烯酸甲酯 - 共 - 甲基丙烯腈）。然后将共聚物溶解在将溶解共聚物并形成粘性溶液的纺丝溶剂中。将溶液施加到基材的表面，并将基材旋转以形成厚度为约0.3至1.0微米的光滑均匀的抗蚀剂膜。加热抗蚀剂膜，然后将待图案化的抗蚀剂膜的区域暴露于电离辐射，直到获得大于1.5×10 -5 C / cm 2的曝光。然后将抗蚀剂的暴露区域显影到基底。

8. 发明授权

US5030759A Selective N-alkylation of aniline in the presence of zeolite catalysts 失效
标题翻译：在沸石催化剂存在下苯胺的选择性N-烷基化
公开(公告)号：US5030759A
公开(公告)日：1991-07-09
申请号：US343818
申请日：1989-04-27
申请人： Arthur C. Bayer , Charles U. Pittman, Jr. , Lichang Wang , Earl G. Alley , Anthony C. Maliyackel
发明人： Arthur C. Bayer , Charles U. Pittman, Jr. , Lichang Wang , Earl G. Alley , Anthony C. Maliyackel
IPC分类号： B01J29/70 , C07B61/00 , C07C209/18 , C07C209/60 , C07C211/48
CPC分类号： C07C209/18
摘要： The selective N-alkylation of anilines comprising providing a mixture of a lower alkanol and an aniline, exposing said mixture to a temperature of from 250.degree. C. to 350.degree. C. in the presence of an acidic zeolite having a pore size of from 6 to 8 angstroms with a three-dimensional tubular shape, such as S-115 zeolite, is described. These zeolites are predominantly selective to the formation of N-alkylanilines.
摘要翻译：包括提供低级烷醇和苯胺的混合物的苯胺的选择性N-烷基化，在孔径为6的酸性沸石存在下将所述混合物暴露于250℃至350℃的温度描述了具有三维管状形状的8埃，例如S-115沸石。这些沸石主要对N-烷基苯胺的形成具有选择性。

9. 发明授权

US4258206A Selective carbonylation of olefins by a polymer-supported Pd halide catalyst 失效
标题翻译：通过聚合物负载的Pd卤化物催化剂选择性羰基化烯烃
公开(公告)号：US4258206A
公开(公告)日：1981-03-24
申请号：US57819
申请日：1979-07-16
申请人： Charles U. Pittman, Jr. , Quock Y. Ng
发明人： Charles U. Pittman, Jr. , Quock Y. Ng
IPC分类号： B01J31/08 , B01J31/16 , B01J31/24 , C07C51/14 , C07C67/38
CPC分类号： C07C51/14 , B01J31/1658 , B01J31/2404 , C07C67/38 , B01J2231/321 , B01J2231/4205 , B01J2531/824
摘要： A solid supported catalyst useful in the carbonylation of olefins represented by the formula ##STR1## wherein Resin- represents a cross-linked solvent swellable high molecular weight resin; X represents a halide; m+n=4. A method for the carbonylation of .alpha.-olefins using the above-mentioned solid-supported catalyst.
摘要翻译：用于由式“IMAGE”表示的烯烃羰基化的固体负载催化剂，其中Resin-代表交联的溶剂可溶胀高分子量树脂; X表示卤化物; m + n = 4。使用上述固体负载型催化剂使α-烯烃羰基化的方法。

10. 发明授权

US07387130B2 Cleaning solutions including nucleophilic amine compound having reduction and oxidation potentials 失效
标题翻译：包括具有还原和氧化电位的亲核胺化合物的清洁溶液
公开(公告)号：US07387130B2
公开(公告)日：2008-06-17
申请号：US11633459
申请日：2006-12-05
申请人： Wai Mun Lee , Charles U. Pittman, Jr. , Robert J. Small
发明人： Wai Mun Lee , Charles U. Pittman, Jr. , Robert J. Small
IPC分类号： B08B3/04 , C11D3/26 , C11D3/30 , C11D3/43
CPC分类号： G03F7/425 , C11D7/261 , C11D7/3218 , C11D7/3227 , C11D7/3245 , C11D7/3263 , C11D7/34 , C11D7/5009 , C11D7/5013 , C11D7/5022 , C11D11/0047 , C23G1/18
摘要： A composition for removing resists and etching residue from substrates containing at least one nucleophilic amine compound having oxidation and reduction potentials, at least one organic solvent, water and, optionally, a chelating agent is described. The chelating agent is preferred to be included since it provides added stability and activity to the cleaning composition so that the composition has long term effectiveness. If a chelating agent is not present, the composition, while providing for adequate stripping and cleaning upon initial use of the composition following mixing, has only short term stability. In this latter instance, the nucleophilic amine compound and organic solvent components of the composition preferably are maintained separate from each other until it is desired to use the composition. Thereafter, the components are combined.
摘要翻译：描述了用于去除抗蚀剂并从含有至少一种具有氧化和还原电位的亲核胺化合物的底物蚀刻残余物的组合物，至少一种有机溶剂，水和任选的螯合剂。优选包含螯合剂，因为它为清洁组合物提供了增加的稳定性和活性，使得组合物具有长期有效性。如果不存在螯合剂，组合物在混合后初始使用组合物时提供足够的剥离和清洁，仅具有短期的稳定性。在后一种情况下，组合物的亲核胺化合物和有机溶剂组分优选彼此保持分开，直到期望使用该组合物。此后，组合组件。

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