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    • 3. 发明授权
    • Microwave plasma monitoring system for the elemental composition
analysis of high temperature process streams
    • 微波等离子体监测系统,用于高温过程流的元素组成分析
    • US5671045A
    • 1997-09-23
    • US540575
    • 1995-10-06
    • Paul P. WoskovDaniel R. CohnCharles H. TitusJeffrey E. Surma
    • Paul P. WoskovDaniel R. CohnCharles H. TitusJeffrey E. Surma
    • G01N21/68G01N21/73G01J3/30G01N21/69H01P1/00
    • G01N21/73
    • Microwave-induced plasma for continuous, real time trace element monitoring under harsh and variable conditions. The sensor includes a source of high power microwave energy and a shorted waveguide made of a microwave conductive, high temperature capability refractory material communicating with the source of the microwave energy to generate a plasma. The high power waveguide is constructed to be robust in a hot, hostile environment. It includes an aperture for the passage of gases to be analyzed and a spectrometer is connected to receive light from the plasma. Provision is made for real time in situ calibration. The spectrometer disperses the light, which is then analyzed by a computer. The sensor is capable of making continuous, real time quantitative measurements of desired elements, such as the heavy metals lead and mercury. The invention may be incorporated into a high temperature process device and implemented in situ for example, such as with a DC graphite electrode plasma arc furnace. The invention further provides a system for the elemental analysis of process streams by removing particulate and/or droplet samples therefrom and entraining such samples in the gas flow which passes through the plasma flame. Introduction of and entraining samples in the gas flow may be facilitated by a suction pump, regulating gas flow, gravity or combinations thereof.
    • 微波诱导等离子体在恶劣条件下进行连续,实时的微量元素监测。 该传感器包括高功率微波能量源和由与微波能量源连通以产生等离子体的微波导电高温能耐火材料制成的短路波导。 高功率波导被构造为在热的,恶劣的环境中是坚固的。 它包括用于待分析气体通过的孔,并且连接光谱仪以接收来自等离子体的光。 经费用于实时在线校准。 光谱仪分散光,然后由计算机分析。 传感器能够对所需元素进行连续的实时定量测量,如重金属铅和汞。 本发明可以结合到高温工艺装置中并且例如用DC石墨电极等离子体电弧炉就地实现。 本发明还提供了一种用于通过从其中除去颗粒和/或液滴样品并将这些样品夹带在通过等离子体火焰的气流中进行元素分析工艺流的系统。 气流中的引入和夹带样品可以通过抽吸泵,调节气流,重力或其组合来促进。
    • 8. 发明授权
    • Self-calibrated active pyrometer for furnace temperature measurements
    • 自校准的有源高温计用于炉温测量
    • US5785426A
    • 1998-07-28
    • US539818
    • 1995-10-06
    • Paul P. WoskovDaniel R. CohnCharles H. TitusJeffrey E. Surma
    • Paul P. WoskovDaniel R. CohnCharles H. TitusJeffrey E. Surma
    • G01R29/08G01J5/46G01J5/52G01K11/00G01K11/12G01K17/00G01J5/08G01J5/62
    • G01K11/006G01J5/522G01K11/12G01K17/003
    • Pyrometer with a probe beam superimposed on its field-of-view for furnace temperature measurements. The pyrometer includes a heterodyne millimeter/sub-millimeter-wave or microwave receiver including a millimeter/sub-millimeter-wave or microwave source for probing. The receiver is adapted to receive radiation from a surface whose temperature is to be measured. The radiation includes a surface emission portion and a surface reflection portion which includes the probe beam energy reflected from the surface. The surface emission portion is related to the surface temperature and the surface reflection portion is related to the emissivity of the surface. The simultaneous measurement of surface emissivity serves as a real time calibration of the temperature measurement. In an alternative embodiment, a translatable base plate and a visible laser beam allow slow mapping out of interference patterns and obtaining peak values therefor. The invention also includes a waveguide having a replaceable end portion, an insulating refractory sleeve and/or a source of inert gas flow. The pyrometer may be used in conjunction with a waveguide to form a system for temperature measurements in a furnace. The system may employ a chopper or alternatively, be constructed without a chopper. The system may also include an auxiliary reflector for surface emissivity measurements.
    • 测高仪用探针光束叠加在其视场上进行炉温测量。 高温计包括外差毫米/亚毫米波或微波接收器,其包括用于探测的毫米/亚毫米波或微波源。 接收器适于接收来自待测温度的表面的辐射。 辐射包括表面发射部分和包括从表面反射的探测光束能量的表面反射部分。 表面发射部分与表面温度有关,表面反射部分与表面的发射率有关。 表面发射率的同时测量可作为温度测量的实时校准。 在替代实施例中,可平移底板和可见激光束允许从干涉图案中缓慢映射并获得其峰值。 本发明还包括具有可更换端部,绝缘耐火套和/或惰性气流源的波导。 高温计可以与波导结合使用以形成用于炉中的温度测量的系统。 该系统可以采用斩波器或替代地,在没有斩波器的情况下构建。 该系统还可以包括用于表面发射率测量的辅助反射器。
    • 9. 发明授权
    • Open tube resonator test setup for conductivity measurements
    • 用于电导率测量的开管谐振器测试设置
    • US4968945A
    • 1990-11-06
    • US278818
    • 1988-12-02
    • Paul P. WoskovDaniel R. Cohn
    • Paul P. WoskovDaniel R. Cohn
    • H01J23/20H01J25/00H01P1/16H01P3/08H01P3/12H01P7/06
    • H01P3/122H01J23/20H01J25/005H01P1/16H01P3/08H01P7/06
    • An apparatus and method for measurement of ohmic loss and surface resistivity is provided with a straight lumen waveguide with at least one opening at one end. Diffraction of radiation introduced to the lumen at one end of the tube provides feedback to establish resonances within the tube. Using the "whispering gallery" resonant modes maximizes the total ohmic loss and thereby enhances sensitivity of resistivity measurements. The angle at which resonant radiation exits the lumen is a function of the mode and size of the operative. Thus, preferred spatial detection allows enhancement of the device signal while discriminating against undesired modes. Selection of modes allows high frequency measurements, into the tetraherz range, to be made without disabling restrictions in the device dimensions, spatial input/output coupling or ohmic loss depending on alignment for analysis of, for example, high temperature superconductors. Furthermore, more than one longitudinal mode for a given transverse mode can be detected allowing for an unambiguous determination of ohmic losses from a measurement of the total Q.
    • 用于测量欧姆损耗和表面电阻率的装置和方法具有在一端具有至少一个开口的直管腔波导。 在管的一端引入管腔的辐射衍射提供反馈以在管内建立共振。 使用“耳语画廊”谐振模式最大化了总的欧姆损耗,从而提高电阻率测量的灵敏度。 谐振辐射离开管腔的角度是手术的模式和尺寸的函数。 因此,优选的空间检测允许在区分不期望的模式的同时增强设备信号。 模式的选择允许在四舍五尔范围内进行高频测量,而不会因为诸如高温超导体的分析的对准而在器件尺寸,空间输入/输出耦合或欧姆损耗方面不受限制。 此外,可以检测给定横向模式的多于一个纵向模式,允许从总Q的测量中明确确定欧姆损耗。