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    • 5. 发明授权
    • Process for the continuous production of polycrystalline high-purity silicon granules
    • 连续生产多晶高纯度硅颗粒的工艺
    • US08722141B2
    • 2014-05-13
    • US12111291
    • 2008-04-29
    • Dieter WeidhausRainer HauswirthHarald Hertlein
    • Dieter WeidhausRainer HauswirthHarald Hertlein
    • B05D7/00B05C11/00
    • C01B33/027
    • High-purity polysilicon granules are prepared by depositing reaction gas on silicon granules in a fluidized bed reactor having: a reactor space comprising at least two zones lying one above the other, the lower zone weakly fluidized by introduction of a silicon-free gas into silicon granules in the lower zone by a plurality of individual dilution gas nozzles, and a second, reaction zone directly abutting the lower zone, the reaction zone heated via its outwardly bounding wall, introducing silicon-containing reaction gas as a vertical high speed gas jet into the reaction zone by reaction gas nozzle(s), forming local reaction gas jets surrounded by bubble-forming fluidized bed, gas decomposing leading to particle growth, wherein the reaction gas has fully or almost fully reacted to chemical equilibrium conversion before reaching the wall or bed surface.
    • 通过在流化床反应器中在硅颗粒上沉积反应气体来制备高纯度多晶硅颗粒,所述反应器具有:包含至少两个位于一个上方的区域的反应器空间,通过将无硅气体引入到硅中而使其弱化的下部区域 通过多个单独的稀释气体喷嘴在下部区域中的颗粒,以及直接邻接下部区域的第二反应区域,经由其向外界壁加热的反应区域,将含硅反应气体作为垂直高速气体射流引入 通过反应气体喷嘴形成反应区,形成由气泡形成流化床包围的局部反应气体射流,气体分解导致颗粒生长,其中反应气体在到达壁之前完全或几乎完全与化学平衡转化反应,或 床面。
    • 6. 发明授权
    • Process and apparatus for comminuting silicon
    • 粉碎硅的工艺和设备
    • US07490785B2
    • 2009-02-17
    • US11504156
    • 2006-08-15
    • Dieter Weidhaus
    • Dieter Weidhaus
    • B02C19/06
    • C01B33/02B02C19/068B02C23/14
    • An apparatus for producing silicon seed particles having a size of from 50 μm to 1000 μm from silicon granules having a size of from 300 μm to 5000 μm, comprising a vertically disposed jet chamber with a low cross sectional area and a jet nozzle at the base of the jet chamber through which a milling gas stream is introduced into the chamber; a larger cross section countercurrent gravity separator adjoining the jet chamber, and an inlet for silicon granules, wherein the jet chamber has a length sufficient to allow the milling gas stream to widen to the cross section of the jet chamber.
    • 一种从尺寸为300μm至5000μm的硅颗粒生产尺寸为50μm至1000μm的硅种子颗粒的装置,包括垂直设置的具有低截面面积的喷射室和在基座处的喷嘴 所述喷射室通过所述喷射室将研磨气流引入所述室中; 邻接喷射室的较大的横截面逆流重力分离器和用于硅颗粒的入口,其中喷射室具有足以允许研磨气流扩大到喷射室的横截面的长度。
    • 7. 发明申请
    • Process For The Continuous Production Of Polycrystalline High-Purity Silicon Granules
    • 多晶高纯度硅颗粒连续生产工艺
    • US20080299291A1
    • 2008-12-04
    • US12111291
    • 2008-04-29
    • Dieter WeidhausRainer HauswirthHarald Hertlein
    • Dieter WeidhausRainer HauswirthHarald Hertlein
    • B05D1/00B05D7/00
    • C01B33/027
    • High-purity polysilicon granules are prepared by depositing reaction gas on silicon granules in a fluidized bed reactor having: a reactor space comprising at least two zones lying one above the other, the lower zone weakly fluidized by introduction of a silicon-free gas into silicon granules in the lower zone by a plurality of individual dilution gas nozzles, and a second, reaction zone directly abutting the lower zone, the reaction zone heated via its outwardly bounding wall, introducing silicon-containing reaction gas as a vertical high speed gas jet into the reaction zone by reaction gas nozzle(s), forming local reaction gas jets surrounded by bubble-forming fluidized bed, gas decomposing leading to particle growth, wherein the reaction gas has fully or almost fully reacted to chemical equilibrium conversion before reaching the wall or bed surface.
    • 通过在流化床反应器中在硅颗粒上沉积反应气体来制备高纯度多晶硅颗粒,所述反应器具有:包含至少两个位于一个上方的区域的反应器空间,通过将无硅气体引入到硅中而使其弱化的下部区域 通过多个单独的稀释气体喷嘴在下部区域中的颗粒,以及直接邻接下部区域的第二反应区域,经由其向外界壁加热的反应区域,将含硅反应气体作为垂直高速气体射流引入 通过反应气体喷嘴形成反应区,形成由气泡形成流化床包围的局部反应气体射流,气体分解导致颗粒生长,其中反应气体在到达壁之前完全或几乎完全与化学平衡转化反应,或 床面。