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1. 发明授权

US5262484A Azlactone graft copolymers 失效
标题翻译：吖内酯接枝共聚物
公开(公告)号：US5262484A
公开(公告)日：1993-11-16
申请号：US942352
申请日：1992-09-09
申请人： Patrick L. Coleman , Thomas A. Kotnour , Richard J. Rolando
发明人： Patrick L. Coleman , Thomas A. Kotnour , Richard J. Rolando
IPC分类号： C08F255/00 , C08L51/06 , C08F255/02 , A61K37/02 , C08F8/18 , C08F8/30 , C08F8/32 , C08F8/36 , C08F263/04 , C08F279/02 , C08L51/04 , G01N33/545
CPC分类号： C08L51/06 , C08F255/00 , Y10T428/31692 , Y10T428/31696
摘要： Graft copolymers and processes for the preparation thereof are provided. The copolymers comprise a base polymer having grafted thereto a monomeric 2-alkenyl azlactone. The surface properties of the graft copolymers can be modified by binding thereto nucleophilic reagents comprising further functional groups with desired properties. Further, the amount of azlactone available at the surface of a graft copolymer for binding to such nucleophilic reagents can be controlled by selecting a surface against which the graft copolymer is formed. The graft copolymers exhibit desirable thermoplastic, melt flow, and adhesion properties and are particularly useful for immobilizing proteins. Methods of immunoassay based on the immobilization of proteins are also disclosed. Another utility of the graft copolymers involves the compatibilizing of immiscible polymer blends.
摘要翻译：提供接枝共聚物及其制备方法。共聚物包含接枝到其上的单体2-链烯基吖内酯的基础聚合物。接枝共聚物的表面性质可以通过与包含具有所需性质的另外的官能团的亲核试剂结合来修饰。此外，可以通过选择形成接枝共聚物的表面来控制在接枝共聚物的表面可用于结合这种亲核试剂的吖内酯的量。接枝共聚物表现出所需的热塑性，熔体流动性和粘合性，并且特别可用于固定蛋白质。还公开了基于蛋白质固定的免疫测定方法。接枝共聚物的另一个用途是使不混溶的聚合物共混物相容化。

2. 发明授权

US5466749A Graft copolymers and graft copolymer/protein compositions 失效
标题翻译：接枝共聚物和接枝共聚物/蛋白质组合物
公开(公告)号：US5466749A
公开(公告)日：1995-11-14
申请号：US283500
申请日：1994-09-14
申请人： Richard J. Rolando , Patrick L. Coleman , Steven L. Kangas , Thomas A. Kotnour
发明人： Richard J. Rolando , Patrick L. Coleman , Steven L. Kangas , Thomas A. Kotnour
IPC分类号： B01J20/32 , C08F255/00 , C08F255/02 , C08F257/00 , C08F257/02 , C08L51/00 , C08L89/00 , G01N33/50 , G01N33/545 , C08G63/48 , C08F8/00 , C08G63/91 , C08L39/04
CPC分类号： G01N33/545 , B01J20/261 , B01J20/264 , B01J20/28014 , B01J20/3007 , B01J20/321 , B01J20/327 , B01J20/3276 , B01J20/3278 , C08F255/02 , C08F257/02 , Y10S530/811 , Y10S530/812 , Y10S530/815 , Y10S530/816
摘要： Graft copolymers comprising a poly-alpha-olefin base polymer selected from the group consisting of polyethylene, polypropylene, polystyrene, and compatible mixtures thereof, having grafted thereto an olefinic monomer. The grafted monomer is present in an amount effective to increase the amount of protein that will bind to the graft copolymer as compared with the base polymer.Also disclosed are polymer/protein compositions comprising a graft copolymer having a protein immobilized on the surface thereof, processes for the preparation of the above-described graft copolymers and compositions, methods of immobilizing proteins, and methods of immunoassay based on such immobilization.
摘要翻译：包含选自聚乙烯，聚丙烯，聚苯乙烯及其相容的混合物的聚-α-烯烃基聚合物的接枝共聚物，其接枝有烯属单体。与基础聚合物相比，接枝单体以有效增加与接枝共聚物结合的蛋白质的量的量存在。还公开了包含具有固定在其表面上的蛋白质的接枝共聚物的聚合物/蛋白质组合物，制备上述接枝共聚物和组合物的方法，固定蛋白质的方法，以及基于这种固定的免疫测定方法。

3. 发明授权

US5466747A Graft copolymers and graft copolymer/protein compositions 失效
公开(公告)号：US5466747A
公开(公告)日：1995-11-14
申请号：US283976
申请日：1994-09-26
申请人： Richard J. Rolando , Patrick L. Coleman , Steven L. Kangas , Thomas A. Kotnour
发明人： Richard J. Rolando , Patrick L. Coleman , Steven L. Kangas , Thomas A. Kotnour
IPC分类号： B01J20/32 , C08F255/00 , C08F255/02 , C08F257/00 , C08F257/02 , C08L51/00 , C08L89/00 , G01N33/50 , G01N33/545 , G01N33/53 , C12Q1/00
CPC分类号： G01N33/545 , B01J20/261 , B01J20/264 , B01J20/28014 , B01J20/3007 , B01J20/321 , B01J20/327 , B01J20/3276 , B01J20/3278 , C08F255/02 , C08F257/02 , Y10S530/811 , Y10S530/812 , Y10S530/815 , Y10S530/816
摘要： Graft copolymers comprising a poly-alpha-olefin base polymer selected from the group consisting of polyethylene, polypropylene, polystyrene, and compatible mixtures thereof, having grafted thereto an olefinic monomer. The grafted monomer is present in an amount effective to increase the amount of protein that will bind to the graft copolymer as compared with the base polymer. Also disclosed are polymer/protein compositions comprising a graft copolymer having a protein immobilized on the surface thereof, processes for the preparation of the above-described graft copolymers and compositions, methods of immobilizing proteins, and methods of immunoassay based on such immobilization.

4. 发明授权

US5364907A Graft copolymers and graft copolymer/protein compositions 失效
标题翻译：接枝共聚物和接枝共聚物/蛋白质组合物
公开(公告)号：US5364907A
公开(公告)日：1994-11-15
申请号：US71327
申请日：1993-06-02
申请人： Richard J. Rolando , Patrick L. Coleman , Steven L. Kangas , Thomas A. Kotnour
发明人： Richard J. Rolando , Patrick L. Coleman , Steven L. Kangas , Thomas A. Kotnour
IPC分类号： B01J20/32 , C08F255/00 , C08F255/02 , C08F257/00 , C08F257/02 , C08L51/00 , C08L89/00 , G01N33/50 , G01N33/545 , C08G63/48 , C08G63/91 , G08L9/00 , G08L47/00
CPC分类号： G01N33/545 , B01J20/261 , B01J20/264 , B01J20/28014 , B01J20/3007 , B01J20/321 , B01J20/327 , B01J20/3276 , B01J20/3278 , C08F255/02 , C08F257/02 , Y10S530/811 , Y10S530/812 , Y10S530/815 , Y10S530/816
摘要： Graft copolymers comprising a poly-alpha-olefin base polymer selected from the group consisting of polyethylene, polypropylene, polystyrene, and compatible mixtures thereof, having grafted thereto an olefinic monomer. The grafted monomer is present in an amount effective to increase the amount of protein that will bind to the graft copolymer as compared with the base polymer.Also disclosed are polymer/protein compositions comprising a graft copolymer having a protein immobilized on the surface thereof, processes for the preparation of the above-described graft copolymers and compositions, methods of immobilizing proteins, and methods of immunoassay based on such immobilization.
摘要翻译：包含选自聚乙烯，聚丙烯，聚苯乙烯及其相容的混合物的聚-α-烯烃基聚合物的接枝共聚物，其接枝有烯属单体。与基础聚合物相比，接枝单体以有效增加与接枝共聚物结合的蛋白质的量的量存在。还公开了包含具有固定在其表面上的蛋白质的接枝共聚物的聚合物/蛋白质组合物，制备上述接枝共聚物和组合物的方法，固定蛋白质的方法，以及基于这种固定的免疫测定方法。

5. 发明授权

US5336717A Graft copolymers containing fluoroaliphatic groups 失效
标题翻译：含氟脂族基团的接枝共聚物
公开(公告)号：US5336717A
公开(公告)日：1994-08-09
申请号：US188454
申请日：1994-01-26
申请人： Richard J. Rolando , Thomas A. Kotnour , James E. Sax
发明人： Richard J. Rolando , Thomas A. Kotnour , James E. Sax
IPC分类号： C08F255/02 , C08F291/00 , C08L51/04 , C08F255/08 , C08F263/04 , C08F265/04 , C08F279/02 , C08J5/00 , C08J7/04 , C08L51/06
CPC分类号： C08F291/00 , C08F255/02
摘要： A fluorochemical graft copolymer comprising: a base polymer comprising polymerized units derived from monomers having terminal olefinic double bonds, having a moiety comprising a fluoroaliphatic group grafted thereto. Also disclosed are processes for preparing such fluorochemical graft copolymers, forming and annealing methods for enhancing the surface activity of such a graft copolymer, polymer blends comprising such a fluorochemical graft copolymer and a matrix polymer that is miscible with the base polymer, and a method for reducing the surface energy of a polymer comprising polymerized units derived from monomers having terminal olefinic double bonds.
摘要翻译：一种含氟化合物接枝共聚物，其包含：包含衍生自具有末端烯属双键的单体的聚合单元的基础聚合物，其具有包含接枝到其上的氟代脂族基团的部分。还公开了制备这种含氟化合物接枝共聚物的方法，用于增强这种接枝共聚物的表面活性的形成和退火方法，包含这种含氟化合物接枝共聚物的聚合物共混物和可与基础聚合物混溶的基质聚合物，以及用于降低包含衍生自具有末端烯属双键的单体的聚合单元的聚合物的表面能。

6. 发明授权

US4948859A Extruder polymerization of polyurethanes 失效
标题翻译：聚氨酯的挤出机聚合
公开(公告)号：US4948859A
公开(公告)日：1990-08-14
申请号：US263713
申请日：1988-10-28
申请人： Jimmie L. Echols , Walton J. Hammar , Thomas A. Kotnour
发明人： Jimmie L. Echols , Walton J. Hammar , Thomas A. Kotnour
IPC分类号： C08G18/08 , C08G18/67
CPC分类号： C08G18/0895 , C08G18/675 , C08G18/677
摘要： Bulk polymerization process for making radiation curable polyurethanes which comprises:(A) providing the following raw materials:(1) diisocyanate;(2) oligomeric diol>400 molecular weight; and(3) >1 chain extending monomer;(B) reacting the raw materials in a twin screw extruder under the following conditions:(1) molar ratio of isocyanate to hydroxy moieties of about 1;(2) ratio of chain extending monomer to other monomers sufficient to yield a polymer having chain extender incorporated at 0.1 to 10 weight percent;(3) extruder temperature sufficient to initiate and maintain reaction; and(4) residence time sufficient to obtain substantially complete reaction of diisocyanate;(C) cooling product polymer. Polyurethane product has weight average molecular weight greater than 80,000 and acrylate or methacrylate functionality. Process permits continuous production of radiation curable polyurethanes having narrow molecular weight distribution and high tensile strength.

7. 发明授权

US4843134A Acrylate pressure-sensitive adhesives containing insolubles 失效
标题翻译：含有不溶物的丙烯酸酯压敏粘合剂
公开(公告)号：US4843134A
公开(公告)日：1989-06-27
申请号：US127611
申请日：1987-11-30
申请人： Thomas A. Kotnour , Ronald L. Barber , Walter L. Krueger
发明人： Thomas A. Kotnour , Ronald L. Barber , Walter L. Krueger
IPC分类号： C08F2/02 , C09J7/02
CPC分类号： C08F2/02 , C09J7/021
摘要： A bulk polymerization process for free radical polymerization of vinyl monomers in a wiped surface reactor is disclosed. Referring to FIG. 1; monomer streams 5 (after purification and silica gel column 2) and 7 are combined with free radical initiator 9 to form a premix 16. Pump 18 transfers the premix stream 22 through static mixer 24 into a wiped surface reactor 27. The reactor can be a counter rotating twin screw extruder which produces polymer stream 36 without the need of solvent and using residence times much shorter than prior art solution or emulsion processes.Some unique pressure sensitive adhesive acrylate polymers have been produced. They are believed to have a relatively high degree of branching. The bulk polymerization process permits the manufacture of pressure sensitive adhesive articles by extruding directly from the twin screw extruder onto a substrate.
摘要翻译：公开了一种在擦拭表面反应器中乙烯基单体的自由基聚合的本体聚合方法。参考图 1; 单体流5（纯化后和硅胶柱2）和7与自由基引发剂9组合以形成预混物16.泵18将预混物流22通过静态混合器24转移到擦拭表面反应器27中。反应器可以是反向旋转双螺杆挤出机，其不需要溶剂并且使用比现有技术的溶液或乳液方法短得多的停留时间产生聚合物流36。已经生产了一些独特的压敏粘合剂丙烯酸酯聚合物。据信它们具有较高的分枝度。本体聚合方法允许通过直接从双螺杆挤出机挤出到基底上来制造压敏粘合剂制品。

8. 发明授权

US06656319B1 Fluid-activatable adhesive articles and methods 有权
标题翻译：流体可活化的粘合剂制品和方法
公开(公告)号：US06656319B1
公开(公告)日：2003-12-02
申请号：US09697007
申请日：2000-10-25
申请人： William C. Boyd , Joseph M. McGrath , Albert I. Everaerts , Laura J. Maursetter , Lang N. Nguyen , Deana A. Klein , Thomas A. Kotnour
发明人： William C. Boyd , Joseph M. McGrath , Albert I. Everaerts , Laura J. Maursetter , Lang N. Nguyen , Deana A. Klein , Thomas A. Kotnour
IPC分类号： B32B3106
CPC分类号： C09J5/02 , C09J7/22 , C09J7/38 , C09J2205/11 , E01F9/619 , E01F9/654 , E01F9/688 , G02B5/12 , G02B5/128 , Y10T156/1028
摘要： Adhesive articles and methods of applying and activating adhesive articles to bond to substrates using a fluid application aid. Preferably, the substrates are traffic devices such as traffic cones and the adhesive articles are retroreflective cone collars or sleeves.
摘要翻译：粘合剂制品和使用流体应用助剂施加和活化粘合剂制品以粘合到基材上的方法。优选地，基板是诸如交通锥的交通装置，并且粘合制品是回射式锥形套环或套筒。

9. 发明授权

US06294249B1 Packaged pre-adhesive composition 有权
标题翻译：包装预粘合剂组合物
公开(公告)号：US06294249B1
公开(公告)日：2001-09-25
申请号：US09245512
申请日：1999-02-05
申请人： Craig E. Hamer , John D. Moon , Thomas A. Kotnour
发明人： Craig E. Hamer , John D. Moon , Thomas A. Kotnour
IPC分类号： C09J13304
CPC分类号： C09J4/00 , B29B13/022 , B29C35/0888 , B29C37/0075 , B29C39/10 , B29C67/24 , B29K2105/0097 , B65D65/38 , C09J7/385 , Y10S206/813 , Y10T428/2809 , Y10T428/31504 , Y10T428/31855 , Y10T428/31909 , Y10T428/31913 , Y10T428/31917 , Y10T428/31935 , C08F220/18 , C08F220/00
摘要： Methods for preparing viscoelastic compositions (e.g., adhesives such as hot melt adhesives) in which a pre-viscoelastic composition (e.g., a pre-adhesive composition) is combined with a packaging material and then polymerized.
摘要翻译：制备粘弹性组合物（例如粘合剂如热熔粘合剂）的方法，其中预粘弹性组合物（例如预粘合剂组合物）与包装材料组合然后聚合。

10. 发明授权

US5804610A Methods of making packaged viscoelastic compositions 失效
标题翻译：包装粘弹性组合物的制备方法
公开(公告)号：US5804610A
公开(公告)日：1998-09-08
申请号：US919756
申请日：1997-08-28
申请人： Craig E. Hamer , John D. Moon , Thomas A. Kotnour
发明人： Craig E. Hamer , John D. Moon , Thomas A. Kotnour
IPC分类号： B29B13/02 , B29C35/08 , B29C37/00 , B29C39/10 , B29C67/24 , B65D65/38 , C08F2/46 , C09J4/00 , C09J7/02 , B65B5/00 , C09J4/02 , B32B27/16 , B32B27/30
CPC分类号： C09J7/0217 , B29B13/022 , B29C35/0888 , B29C37/0075 , B29C39/10 , B29C67/24 , B65D65/38 , C09J4/00 , B29K2105/0097 , Y10S206/813 , Y10T428/2809 , Y10T428/31504 , Y10T428/31855 , Y10T428/31909 , Y10T428/31913 , Y10T428/31917 , Y10T428/31935
摘要： Methods for preparing viscoelastic compositions (e.g., adhesives such as hot melt adhesives) in which a pre-viscoelastic composition (e.g., a pre-adhesive composition) is combined with a packaging material and then polymerized by transmissive energy.
摘要翻译：制备粘弹性组合物（例如，诸如热熔粘合剂的粘合剂）的方法，其中将预粘弹性组合物（例如预粘合剂组合物）与包装材料组合，然后通过透射能量聚合。

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