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1. 发明授权

US4522976A Graft polymer dispersion in a mixture of low molecular weight polyols and polyether polyols and polyurethane foams prepared therefrom 失效
标题翻译：在低分子量多元醇和聚醚多元醇和由其制备的聚氨酯泡沫的混合物中的接枝聚合物分散体
公开(公告)号：US4522976A
公开(公告)日：1985-06-11
申请号：US611134
申请日：1984-05-17
申请人： Oscar M. Grace , Steven E. Wujcik , Duane A. Heyman
发明人： Oscar M. Grace , Steven E. Wujcik , Duane A. Heyman
IPC分类号： C08F283/00 , C08F283/06 , C08F290/06 , C08G18/00 , C08G18/63 , C08G18/64 , C08J9/02 , C08L25/08
CPC分类号： C08G18/635 , C08F290/062
摘要： A low viscosity, stable graft polymer dispersion is prepared by polymerizing in the presence of a free radical initiator, from about 25 to about 70 weight percent based on the total weight of the dispersion, an ethylenically unsaturated monomer or mixture of monomers, in a polyol mixture comprising (1) from about 25 to about 99 weight percent of a polyol containing from 2 to 8 hydroxyl groups and having an equivalent weight from 30 to about 200, (2) from about 1 to about 75 weight percent of a macromer containing induced unsaturation, said macromer comprising the reaction product of a polyether polyol having an equivalent weight from 100 to 10,000 with a compound having both ethylenic unsaturation and a group selected from the group consisting of a hydroxyl, carboxyl, anhydride, isocyanate and epoxy or mixtures thereof. These graft polymer dispersions are useful for preparing polyurethane products.
摘要翻译：通过在自由基引发剂的存在下聚合制备低粘度，稳定的接枝聚合物分散体，其中所述分散体的总重量为约25至约70重量％，烯属不饱和单体或单体混合物在多元醇混合物，其包含（1）约25至约99重量％的含有2至8个羟基并且具有30至约200当量的多元醇，（2）约1至约75重量％的含有诱导的大分子单体所述大分子单体包括当量为100至10,000的聚醚多元醇与具有不同烯键式的化合物和选自羟基，羧基，酸酐，异氰酸酯和环氧基或其混合物的基团的反应产物。这些接枝聚合物分散体可用于制备聚氨酯产品。

2. 发明授权

US4568705A Graft polymer dispersion in a mixture of low molecular weight polyols and polyether polyols and polyurethane foams prepared therefrom 失效
标题翻译：在低分子量多元醇和聚醚多元醇和由其制备的聚氨酯泡沫的混合物中的接枝聚合物分散体
公开(公告)号：US4568705A
公开(公告)日：1986-02-04
申请号：US737504
申请日：1985-05-24
申请人： Oscar M. Grace , Steven E. Wujcik , Duane A. Heyman
发明人： Oscar M. Grace , Steven E. Wujcik , Duane A. Heyman
IPC分类号： C08F290/06 , C08G18/63 , C08G18/14
CPC分类号： C08G18/63 , C08F290/062
摘要： A low viscosity, stable graft polymer dispersion is prepared by polymerizing in the presence of a free radical initiator, from about 25 to about 75 weight percent based on the total weight of the dispersion, an ethylenically unsaturated monomer or mixture of monomers, in a polyol mixture comprising (1) from about 25 to about 99 weight percent of a polyol containing from 2 to 8 hydroxyl groups and having an equivalent weight from 30 to about 200, (2) from about 1 to about 75 weight percent of a macromer containing induced unsaturation, said macromer comprising the reaction product of a polyether polyol having an equivalent weight from 100 to 10,000 with a compound having both ethylenic unsaturation and a group selected from the group consisting of a hydroxyl, carboxyl, anhydride, isocyanate and epoxy or mixtures thereof. These graft polymer dispersions are useful for preparing polyurethane products.
摘要翻译：通过在自由基引发剂的存在下聚合制备低粘度，稳定的接枝聚合物分散体，其量为约25至约75重量％，基于分散体，烯属不饱和单体或单体混合物的总重量，在多元醇混合物，其包含（1）约25至约99重量％的含有2至8个羟基并且具有30至约200当量的多元醇，（2）约1至约75重量％的含有诱导的大分子单体所述大分子单体包括当量为100至10,000的聚醚多元醇与具有不同烯键式的化合物和选自羟基，羧基，酸酐，异氰酸酯和环氧基或其混合物的基团的反应产物。这些接枝聚合物分散体可用于制备聚氨酯产品。

3. 发明授权

US4810729A Flexible flame resistant polyurethane foams 失效
标题翻译：柔性阻燃聚氨酯泡沫
公开(公告)号：US4810729A
公开(公告)日：1989-03-07
申请号：US111854
申请日：1987-10-23
申请人： Pauls Davis , Oscar M. Grace , Steven E. Wujcik
发明人： Pauls Davis , Oscar M. Grace , Steven E. Wujcik
IPC分类号： C08J9/02 , C08G18/38 , C08G18/63 , C08J9/04 , C08K5/16 , C08K5/20 , C08K5/21 , C08L71/02 , C08L75/00 , C08L75/04 , C08J9/00 , C08G18/48
CPC分类号： C08K5/20 , C08G18/3825 , C08G18/3838 , C08G18/632 , C08K5/21 , C08G2101/0008 , C08G2101/0058 , Y10S521/906
摘要： The invention pertains to flame retardant polyurethane foams prepared by the reaction of a polyoxyalkylene polyether polyol with toluene diisocyanate and a blowing agent wherein the flame retardant compound is selected from the group consisting of dicyandiamide, oxamide and biuret. The amount of flame retardant may range from about 25 weight percent of about 75 weight percent of the total composition.
摘要翻译：本发明涉及通过聚氧化烯聚醚多元醇与甲苯二异氰酸酯和发泡剂反应制备的阻燃聚氨酯泡沫，其中阻燃化合物选自双氰胺，草酰胺和缩二脲。阻燃剂的量可以在总组合物的约25重量％的约75重量％的范围内。

4. 发明授权

US4454255A Process for the preparation of white graft polymer dispersions and flame-retardant polyurethane foams 失效
标题翻译：制备白色接枝聚合物分散体和阻燃聚氨酯泡沫的方法
公开(公告)号：US4454255A
公开(公告)日：1984-06-12
申请号：US364336
申请日：1982-04-01
申请人： Gerhard G. Ramlow , Duane A. Heyman , Oscar M. Grace , Curtis J. Reichel , Robert J. Hartman
发明人： Gerhard G. Ramlow , Duane A. Heyman , Oscar M. Grace , Curtis J. Reichel , Robert J. Hartman
IPC分类号： C08F299/00 , C08F283/06 , C08F290/00 , C08F291/08 , C08F299/02 , C08G18/00 , C08G18/63 , C08G63/676 , C08L51/08 , C08K5/06 , C08K5/10 , C08L29/02
CPC分类号： C08F283/06 , C08F291/08 , C08F299/022 , C08G18/63 , C08G63/676
摘要： White graft polymer dispersions in polyoxyalkylene polyether polyols are employed together with flame retardant compounds to prepare flame retardant polyurethane foams. The polymer dispersions employ less than 0.1 mole of induced unsaturation per mole of polyol mixture. Improved processes for the reparation of these polymer dispersions employ either isomerized maleate containing polyetherester polyols or polyetherester polyols prepared by reacting a polyoxyalkylene polyether polyol, a polycarboxylic acid anhydride and an alkylene oxide in the presence of salts and oxides of divalent metals.
摘要翻译：聚氧亚烷基聚醚多元醇中的白色接枝聚合物分散体与阻燃化合物一起使用以制备阻燃聚氨酯泡沫。聚合物分散体每摩尔多元醇混合物使用少于0.1摩尔的诱导不饱和度。用于修复这些聚合物分散体的改进方法使用含有聚醚酯多元醇的异构化马来酸酯或通过在二价金属的盐和氧化物的存在下使聚氧化烯聚醚多元醇，多元羧酸酐和烯化氧反应制备的聚醚酯多元醇。

5. 发明授权

US4690956A Process for the preparation of graft polymer dispersions and flame-retardant polyurethane foams 失效
标题翻译：制备接枝聚合物分散体和阻燃聚氨酯泡沫的方法
公开(公告)号：US4690956A
公开(公告)日：1987-09-01
申请号：US791873
申请日：1985-10-28
申请人： Gerhard G. Ramlow , Duane A. Heyman , Oscar M. Grace
发明人： Gerhard G. Ramlow , Duane A. Heyman , Oscar M. Grace
IPC分类号： C08L75/04 , C08F2/38 , C08F283/06 , C08F283/12 , C08F290/00 , C08F291/08 , C08F299/02 , C08G18/63 , C08G63/676 , C08L75/00 , C08K5/06 , C08K5/10 , C08L29/02 , C08L51/08
CPC分类号： C08F291/08 , C08F283/06 , C08F299/022 , C08F299/026 , C08G18/635 , C08G63/676
摘要： Graft polymer dispersions in polyoxyalkylene polyether polyols are employed together with flame retardant compounds to prepare flame retardant polyurethane foams. The polymer dispersions employ less than 0.1 mole of induced unsaturation per mole of polyol mixture. Processes for the preparation of these polymer dispersions employ fumarate derived polyetherester polyols or polyetherester polyols prepared by reacting a polyoxyalkylene polyether polyol with a compound selected from the group consisting of maleic acid, maleic anhydride and fumaric acid and an alkylene oxide in the presence of salts and oxides of divalent metals. The polymer dispersions are prepared in the presence of a reaction moderator and employ 50 weight percent or more of acrylonitrile.
摘要翻译：在聚氧化烯聚醚多元醇中的接枝聚合物分散体与阻燃化合物一起使用以制备阻燃聚氨酯泡沫。聚合物分散体每摩尔多元醇混合物使用少于0.1摩尔的诱导不饱和度。用于制备这些聚合物分散体的方法使用富马酸酯衍生的聚醚酯多元醇或聚醚酯多元醇，其通过聚氧亚烷基聚醚多元醇与选自马来酸，马来酸酐和富马酸的化合物和烯化氧在盐和/ 二价金属的氧化物。聚合物分散体在反应缓和剂存在下制备，并使用50重量％或更多的丙烯腈。

6. 发明授权

US4689354A Process for the preparation of white graft polymer dispersions and flame-retardant polyurethane foams 失效
标题翻译：制备白色接枝聚合物分散体和阻燃聚氨酯泡沫的方法
公开(公告)号：US4689354A
公开(公告)日：1987-08-25
申请号：US790435
申请日：1985-10-23
申请人： Gerhard G. Ramlow , Duane A. Heyman , Oscar M. Grace , Curtis J. Reichel , Robert J. Hartman
发明人： Gerhard G. Ramlow , Duane A. Heyman , Oscar M. Grace , Curtis J. Reichel , Robert J. Hartman
IPC分类号： C08F283/06 , C08F291/08 , C08F299/02 , C08G18/63 , C08G63/676 , C08K5/06 , C08K5/10 , C08L29/02 , C08L51/08
CPC分类号： C08G63/676 , C08F283/06 , C08F291/08 , C08F299/022 , C08G18/635
摘要： White graft polymer dispersions in polyoxyalkylene polyether polyols are employed together with flame retardant compounds to prepare flame retardant polyurethane foams. The polymer dispersions employ less than 0.1 mole of induced unsaturation per mole of polyol mixture. Improved processes for the preparation of these polymer dispersions employ either maleate or fumarate derived polyetherester polyols or polyetherester polyols prepared by reacting a polyoxyalkylene polyether polyol in the presence of a chain transfer agent with a compound selected from the group consisting of maleic acid, maleic anhydride and fumaric acid and an alkyklene oxide in the presence of salts and oxides of divalent metals.
摘要翻译：聚氧亚烷基聚醚多元醇中的白色接枝聚合物分散体与阻燃化合物一起使用以制备阻燃聚氨酯泡沫。聚合物分散体每摩尔多元醇混合物使用少于0.1摩尔的诱导不饱和度。用于制备这些聚合物分散体的改进方法使用马来酸酯或富马酸酯衍生的聚醚酯多元醇或聚醚酯多元醇，其通过在链转移剂存在下使聚氧化烯聚醚多元醇与选自马来酸，马来酸酐和富马酸和烷基烯烃在二价金属的盐和氧化物存在下进行。

7. 发明授权

US5179131A Process for the preparation of polyurethane foams employing polyol dispersions containing polyisocyanate polyaddition solids 失效
标题翻译：使用含有多异氰酸酯加聚固体的多元醇分散体制备聚氨酯泡沫体的方法
公开(公告)号：US5179131A
公开(公告)日：1993-01-12
申请号：US815299
申请日：1991-12-27
申请人： Steven E. Wujcik , Donald L. Christman , Oscar M. Grace
发明人： Steven E. Wujcik , Donald L. Christman , Oscar M. Grace
IPC分类号： C08G18/28 , C08G18/40 , C08G18/65
CPC分类号： C08G18/6541 , C08G18/281 , C08G18/409 , C08G2101/00
摘要： Addition of minor quantities of mono- or dicarboxylic acids to polyurethane foam formulations which employ polyisocyanate polyaddition polymer polyol dispersions prevents shrinkage and tightness in polyurethane foams prepared therefrom. If acid addition is made directly after dispersion preparation, reduction of polyol viscosity and more rapid stabilization against viscosity change is observed.

8. 发明授权

US5114988A Polyether polyols having reduced unsaturation and polyurethane foams prepared therefrom 失效
标题翻译：具有减少不均匀性的聚醚多元醇和制备的聚氨酯
公开(公告)号：US5114988A
公开(公告)日：1992-05-19
申请号：US425077
申请日：1989-10-23
申请人： Steven D. Gagnon , Oscar M. Grace , Theodore M. Smiecinski , Steven E. Wujcik
发明人： Steven D. Gagnon , Oscar M. Grace , Theodore M. Smiecinski , Steven E. Wujcik
IPC分类号： C08G18/50 , C08G65/26
CPC分类号： C08G65/2624 , C08G18/5033
摘要： Polyether polyols prepared by oxyalkylating a 1,2-diaminocycloalkane have reduced levels of unsaturation and may be used to prepare melamine containing flame retardant polyurethane foams capable of passing California 117 and 133, and other flame tests.
摘要翻译：通过1,2-二氨基环烷烃的烷氧基化而制备的聚醚多元醇具有降低的不饱和度，可用于制备能够通过加州117和133的三聚氰胺含阻燃聚氨酯泡沫以及其它火焰试验。

9. 发明授权

US4892893A Flame retardant polyurethane foams resistant to cigarette smoldering ignition 失效
标题翻译：阻燃聚氨酯泡沫抵抗香烟闷燃点火
公开(公告)号：US4892893A
公开(公告)日：1990-01-09
申请号：US312990
申请日：1989-02-17
申请人： Oscar M. Grace , Theodore M. Smiecinski , Steven E. Wujcik
发明人： Oscar M. Grace , Theodore M. Smiecinski , Steven E. Wujcik
IPC分类号： C08G18/38 , C08K5/3492
CPC分类号： C08G18/3851 , C08K5/34922 , C08G2101/0008 , Y10S521/906
摘要： The invention pertains to flame retardant flexible polyurethane foams resistant to cigarette smoldering after being subjected to flex fatigue, prepared by reacting a conventional polyether polyol, toluene diisocyanate, and a blowing agent, and incorporating substantially uncrushed melamine in an amount ranging from about 5 weight percent to about 25 weight percent.
摘要翻译：本发明涉及通过使常规的聚醚多元醇，甲苯二异氰酸酯和发泡剂反应制备的，经受挠曲疲劳之后耐香烟阴燃的阻燃软质聚氨酯泡沫，并掺入基本未裂化的三聚氰胺的量为约5重量％至约25重量％。

10. 发明授权

US4826884A Flame retardant polyurethane foams resistant to cigarette smoldering ignition 失效
标题翻译：阻燃聚氨酯泡沫抵抗香烟闷燃点火
公开(公告)号：US4826884A
公开(公告)日：1989-05-02
申请号：US75330
申请日：1987-07-20
申请人： Oscar M. Grace , Theodore M. Smiecinski , Steven E. Wujcik
发明人： Oscar M. Grace , Theodore M. Smiecinski , Steven E. Wujcik
IPC分类号： C08G18/66 , C08G18/30 , C08G18/38 , C08J9/00 , C08K5/3492 , C08G18/14
CPC分类号： C08J9/0028 , C08G18/3851 , C08K5/34922 , C08J2375/08 , Y10S521/906
摘要： The invention pertains to flame retardant flexible polyurethane foams resistant to cigarette smoldering after being subjected to flex fatigue prepared by reacting a polyether polyol, an organic isocyanate, and a blowing agent incorporating melamine in an amount ranging from about 5 weight percent to about 25 weight percent.
摘要翻译：本发明涉及耐受柔软聚苯乙烯泡沫的阻燃柔性聚氨酯泡沫，其经受挠曲疲劳之后，其通过使聚醚多元醇，有机异氰酸酯和含有约5重量％至约25重量％的量的三聚氰胺的发泡剂。

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