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1. 发明申请

US20080192252A1 Optical Measuring Device and Method, and Nanoparticle Measuring Method and Device 有权
标题翻译：光学测量装置及方法及纳米粒子测量方法及装置
公开(公告)号：US20080192252A1
公开(公告)日：2008-08-14
申请号：US11661492
申请日：2005-07-15
申请人： Naoji Moriya , Shinichiro Totoki , Yuzo Nagumo , Yukihisa Wada , Naofumi Sakauchi , Fujio Inoue , Masahiro Takebe , Makiko Masutomi
发明人： Naoji Moriya , Shinichiro Totoki , Yuzo Nagumo , Yukihisa Wada , Naofumi Sakauchi , Fujio Inoue , Masahiro Takebe , Makiko Masutomi
IPC分类号： G01N21/00
CPC分类号： G01N21/4788 , G01N15/0211 , G01N15/0227 , G01N2013/003 , G01N2015/0038 , G01N2015/0294
摘要： The invention provides an optical measuring device capable of performing measuring using a transient diffraction grating by only adjusting probe light, and a nanoparticle measuring device using the same principle as the optical measuring device. An optical measuring device includes: a power supply 15; a container 11 that stores a sample; a pair of electrodes 13 and 14 that generate an electric force line distribution in which areas having high electric force line density and areas having low electric force line density are regularly arranged; a dielectrophoresis control unit 19 that controls the generation of a transient diffraction grating using dielectrophoresis of particles in the sample caused by applying the voltage to the pair of electrodes 13 and 14 and a variation in the transient diffraction grating due to the diffusion of the particles in the sample according to a variation in the applied voltage; a light source 16 emitting light to the transient diffraction grating; and a plurality of photodetectors 18 detecting diffracted light generated by the transient diffraction grating. In the optical measuring device, the particles are evaluated on the basis of a variation in the intensity of the diffracted light generated by the transient diffraction grating. Further, for example, the particle diameter of a nanoparticle is measured by the same principle as the optical measuring device uses. As a result, it is possible to increase the intensity of a signal and to improve the sensitivity and the S/N ratio, as compared to a dynamic scattering method.
摘要翻译：本发明提供一种光学测量装置，该光学测量装置能够仅通过调节探测光来进行使用瞬态衍射光栅的测量，以及使用与光学测量装置相同原理的纳米粒子测量装置。光学测量装置包括：电源15; 存储样品的容器11; 产生电力线分布的一对电极13,14，其中规定排列具有高电力线密度的区域和具有低电力线密度的区域; 介电电泳控制单元19，其使用通过向一对电极13和14施加电压引起的样品中的颗粒的介电电泳，以及由于颗粒的扩散引起的瞬态衍射光栅的变化来控制瞬态衍射光栅的产生样品根据施加电压的变化; 将光发射到瞬态衍射光栅的光源16; 以及检测由瞬变衍射光栅产生的衍射光的多个光检测器18。在光学测量装置中，基于由瞬变衍射光栅产生的衍射光的强度的变化来评估颗粒。此外，例如，通过与光学测量装置使用的原理相同的原理来测量纳米颗粒的粒径。结果，与动态散射方法相比，可以增加信号的强度并提高灵敏度和S / N比。

2. 发明申请

US20090251695A1 OPTICAL MEASURING DEVICE 有权
标题翻译：光学测量装置
公开(公告)号：US20090251695A1
公开(公告)日：2009-10-08
申请号：US11996057
申请日：2006-01-17
申请人： Naoji Moriya , Yuzo Nagumo , Yukihisa Wada , Naofumi Sakauchi , Fujio Inoue , Masahiro Takebe , Kenji Takubo , Shinichiro Totoki
发明人： Naoji Moriya , Yuzo Nagumo , Yukihisa Wada , Naofumi Sakauchi , Fujio Inoue , Masahiro Takebe , Kenji Takubo , Shinichiro Totoki
IPC分类号： G01N15/02 , G01N21/47
CPC分类号： G01N15/0211 , G01N21/4788 , G01N2021/1721
摘要： Within a container 1 which is storing a sample is generated a regularly arranged electric field distribution by an impression of a voltage upon an electrode pair 2 provided within the container 1, thereby generating diffraction grating formed by a density modulation of particles within the sample within the container 1, there is obtained information upon a diffusion of the particles based upon a temporal change in an extinction process of an intensity of a diffracted light beam obtained by irradiating a light beam upon the diffraction grating formed by the density modulation of the particles, the electrodes 21, 22 constituting the electrode pair 2 are configured to have multiple linear electrode teeth 21a, 22a parallel with each other, the electrodes 21, 22 are arranged such that the electrode teeth 21a of one electrode 21 are inserted between the electrode teeth 22a of the other electrode 22, thereby increasing the width of the diffraction grating formed by the density modulation of the particles, and a ratio of a component of the diffracted light beam thereof included in an entire diffracted light beam is increased to increase sensitivity of a measurement. As a result, there is provided an optical measuring device which can measure the information upon the diffusion of the particles movably dispersed within a medium at a high sensitivity and with an excellent S/N ratio.
摘要翻译：在存储样品的容器1内通过设置在容器1内的电极对2上的电压印制产生规则排列的电场分布，从而产生通过在样品内的颗粒的密度调制形成的衍射光栅容器1根据粒子的密度调制形成的衍射光栅照射光束而获得的衍射光束的强度的消光处理中的时间变化，获得了粒子扩散的信息，构成电极对2的电极21,22被配置为具有彼此平行的多个线状电极齿21a，22a，电极21,22被布置成使得一个电极21的电极齿21a插入到电极齿22a 另一个电极22，从而增加由t的密度调制形成的衍射光栅的宽度并且包括在整个衍射光束中的衍射光束的分量的比率增加，以增加测量的灵敏度。结果，提供了一种光学测量装置，其可以以高灵敏度和良好的S / N比来测量可移动地分散在介质中的颗粒的扩散的信息。

3. 发明授权

US07911610B2 Optical measuring device 有权
标题翻译：光学测量装置
公开(公告)号：US07911610B2
公开(公告)日：2011-03-22
申请号：US11996057
申请日：2006-01-17
申请人： Naoji Moriya , Yuzo Nagumo , Yukihisa Wada , Naofumi Sakauchi , Fujio Inoue , Masahiro Takebe , Kenji Takubo , Shinichiro Totoki
发明人： Naoji Moriya , Yuzo Nagumo , Yukihisa Wada , Naofumi Sakauchi , Fujio Inoue , Masahiro Takebe , Kenji Takubo , Shinichiro Totoki
IPC分类号： G01N21/00
CPC分类号： G01N15/0211 , G01N21/4788 , G01N2021/1721
摘要： The present invention relates to an optical measuring device which includes container for storing a sample, and an electrode pair for generating an electric field distribution upon impression of a voltage by an electrical power supply, thereby generating or extinguishing diffraction grating formed by a density modulation of particles within the sample. The particles within the sample are evaluated based upon a temporal change of an intensity of a diffracted light beam obtained by irradiating a light beam upon the diffraction grating formed by the density modulation of the particles. The electrodes constituting the electrode pair are configured to have a comb-like electrode teeth that are parallel with each other and are arranged such that the electrode teeth of one electrode are inserted between the electrode teeth of the other electrode. From such configuration, an optical measuring device of a high sensitivity and excellent S/N ratio can be obtained.
摘要翻译：本发明涉及一种光学测量装置，该光学测量装置包括用于存储样品的容器和用于通过电源印制电压而产生电场分布的电极对，由此产生或熄灭由密度调制形成的衍射光栅样品内的颗粒。基于通过对通过颗粒的密度调制形成的衍射光栅照射光束而获得的衍射光束的强度的时间变化来评估样品内的颗粒。构成电极对的电极被构造为具有彼此平行的梳状电极齿，并且被布置成使得一个电极的电极齿插入另一个电极的电极齿之间。由此，可以得到灵敏度高，S / N比优异的光学测量装置。

4. 发明授权

US08313628B2 Method and apparatus for evaluating dielectrophoretic intensity of microparticle 失效
标题翻译：评估微粒介质电泳强度的方法和装置
公开(公告)号：US08313628B2
公开(公告)日：2012-11-20
申请号：US12374048
申请日：2006-07-19
申请人： Yoshio Tsunazawa , Yukihisa Wada , Naoji Moriya , Kenji Takubo , Shinichiro Totoki , Haruo Shimaoka
发明人： Yoshio Tsunazawa , Yukihisa Wada , Naoji Moriya , Kenji Takubo , Shinichiro Totoki , Haruo Shimaoka
IPC分类号： B03C5/02
CPC分类号： G01N21/4788 , B03C5/005 , B03C5/026 , G01N2015/0003 , G01N2015/0038
摘要： A distribution of AC electric field regularly arranged in a cell is formed while storing a sample having particles dispersed in a medium in the cell, whereby the particles are dielectrically migrated in the medium to generate a diffraction grating by density distribution of the particles. Diffracted light generated by irradiating the diffraction grating by density distribution with measuring light is detected, and evaluation of dielectrophoretic intensities of the particles and/or the medium is performed from the detection result. According to this method, evaluation of dielectrophoretic characteristics can be performed without adhering a phosphor to particles, and since even a particle small in size can achieve a detection level by collecting a number of such particles to form a diffraction grating, dielectric characteristics of microparticles of several nanometers in diameter can be thus quantitatively measured with high sensitivity.
摘要翻译：形成规则排列在电池中的AC电场的分布，同时将具有分散在介质中的粒子的样品储存在电池中，由此在介质中介电迁移，从而通过颗粒的密度分布产生衍射光栅。检测通过用测量光通过密度分布照射衍射光栅而产生的衍射光，并根据检测结果评估颗粒和/或介质的介电电泳强度。根据该方法，可以在不将荧光体附着于粒子的情况下进行介电电泳特性的评价，并且，即使通过收集多个这样的粒子来形成衍射光栅，尺寸小的粒子也能够达到检测水平，所以微粒的介电特性因此可以高灵敏度定量测量直径几纳米。

5. 发明申请

US20100012496A1 METHOD AND APPARATUS FOR EVALUATING DIELECTROPHORETIC INTENSITY OF MICROPARTICLE 失效
标题翻译：评估微电极的电磁强度的方法和装置
公开(公告)号：US20100012496A1
公开(公告)日：2010-01-21
申请号：US12374048
申请日：2006-07-19
申请人： Yoshio Tsunazawa , Yukihisa Wada , Naoji Moriya , Kenji Takubo , Shinichiro Totoki , Haruo Shimaoka
发明人： Yoshio Tsunazawa , Yukihisa Wada , Naoji Moriya , Kenji Takubo , Shinichiro Totoki , Haruo Shimaoka
IPC分类号： G01N15/00 , B01D57/02 , G01N15/02 , G01N21/47
CPC分类号： G01N21/4788 , B03C5/005 , B03C5/026 , G01N2015/0003 , G01N2015/0038
摘要： A distribution of AC electric field regularly arranged in a cell is formed while storing a sample having particles dispersed in a medium in the cell, whereby the particles are dielectrically migrated in the medium to generate a diffraction grating by density distribution of the particles. Diffracted light generated by irradiating the diffraction grating by density distribution with measuring light is detected, and evaluation of dielectrophoretic intensities of the particles and/or the medium is performed from the detection result. According to this method, evaluation of dielectrophoretic characteristics can be performed without adhering a phosphor to particles, and since even a particle small in size can achieve a detection level by collecting a number of such particles to form a diffraction grating, dielectric characteristics of microparticles of several nanometers in diameter can be thus quantitatively measured with high sensitivity.
摘要翻译：形成规则排列在电池中的AC电场的分布，同时将具有分散在介质中的粒子的样品储存在电池中，由此在介质中介电迁移，从而通过颗粒的密度分布产生衍射光栅。检测通过用测量光通过密度分布照射衍射光栅而产生的衍射光，并根据检测结果评估颗粒和/或介质的介电电泳强度。根据该方法，可以在不将荧光体附着于粒子的情况下进行介电电泳特性的评价，并且，即使通过收集多个这样的粒子来形成衍射光栅，尺寸小的粒子也能够达到检测水平，所以微粒的介电特性因此可以高灵敏度定量测量直径几纳米。

6. 发明申请

US20050083524A1 Particle size analyzer 失效
标题翻译：粒度分析仪
公开(公告)号：US20050083524A1
公开(公告)日：2005-04-21
申请号：US10949190
申请日：2004-09-27
申请人： Shinichiro Totoki
发明人： Shinichiro Totoki
IPC分类号： G01N15/02 , G01N21/00
CPC分类号： G01N15/0205 , G01N15/0211 , G01N21/6428
摘要： A laser diffraction particle size analyzer irradiates a laser beam on particles in a scattered state, and measures a spatial intensity distribution of diffracted and scattered light from the particles. A particle size distribution of the particles is calculated from a result of the measurement. The laser diffraction particle size analyzer includes a laser device for generating an ultraviolet laser beam as a light source for generating a laser beam, and a fluorescent member closely attached to or disposed adjacent to a detecting surface of a photodiode array that measures the spatial intensity distribution of the diffracted and scattered light upon incidence thereof.
摘要翻译：激光衍射粒度分析仪将激光束照射在散射状态的粒子上，测定来自粒子的衍射光和散射光的空间强度分布。从测量结果计算颗粒的粒度分布。激光衍射粒度分析仪包括用于产生作为产生激光束的光源的紫外激光束的激光装置和紧密附着或邻近测量空间强度分布的光电二极管阵列的检测表面附近的荧光部件的衍射和散射光。

7. 发明授权

US06923848B2 Collecting apparatus of floating dusts in atmosphere 失效
标题翻译：大气中浮尘的收集装置
公开(公告)号：US06923848B2
公开(公告)日：2005-08-02
申请号：US10882621
申请日：2004-07-02
申请人： Shinichiro Totoki
发明人： Shinichiro Totoki
IPC分类号： B01D49/00 , G01N1/22 , G01N1/24 , G01N1/28 , G01N15/02 , G01N15/06 , B03C3/41 , B03C3/47
CPC分类号： B01D49/00 , B03C3/368 , B03C3/41 , B03C3/47 , B03C2201/04 , B03C2201/10 , B03C2201/24 , G01N1/2202 , G01N1/24 , G01N15/0211 , G01N15/0266 , G01N2001/2223 , G01N2001/2833 , G01N2015/0693
摘要： A collecting device for collecting particles floating in the atmosphere includes a collecting container; a pump for sucking the atmosphere into the collecting container; a discharge electrode disposed in the collecting container for generating single polarity ions to charge the particles in the collecting container; and a dust-collecting electrode for collecting the charged particles in the collecting container through a potential difference between the discharge electrode and the dust-collecting electrode. The dust on the dust-collecting electrode is measured and analyzed.
摘要翻译：用于收集浮在大气中的颗粒的收集装置包括收集容器; 用于将气氛吸入收集容器的泵; 放电电极，设置在收集容器中，用于产生单极性离子以对收集容器中的颗粒进行充电; 以及用于通过放电电极和集尘电极之间的电位差收集收集容器中的带电粒子的集尘电极。测量和分析集尘电极上的灰尘。

8. 发明申请

US20050126260A1 Method of measuring floating dusts 失效
标题翻译：测量浮尘的方法
公开(公告)号：US20050126260A1
公开(公告)日：2005-06-16
申请号：US11048895
申请日：2005-02-03
申请人： Shinichiro Totoki
发明人： Shinichiro Totoki
IPC分类号： B01D49/00 , G01N1/22 , G01N1/24 , G01N1/28 , G01N15/02 , G01N15/06 , G01N7/00
CPC分类号： B01D49/00 , B03C3/368 , B03C3/41 , B03C3/47 , B03C2201/04 , B03C2201/10 , B03C2201/24 , G01N1/2202 , G01N1/24 , G01N15/0211 , G01N15/0266 , G01N2001/2223 , G01N2001/2833 , G01N2015/0693
摘要： In a method of measuring particles floating in an atmosphere, the atmosphere containing the particles is sucked into a container, ions are generated from a discharge electrode disposed in the container to charge the particles with the ions. A dust-collecting electrode is arranged in the container to electrically conduct with a ground potential, wherein the dust collecting electrode is formed of a transparent plate having a transparent conductive film on a surface thereof facing the discharge electrode. The charged particles are collected on the dust-collecting electrode disposed in the container by using a potential difference relative to the discharge electrode, and the particles on the dust-collecting electrode are measured.
摘要翻译：在测量浮在大气中的颗粒的方法中，将含有颗粒的气氛吸入容器中，从设置在容器中的放电电极产生离子，以使离子粒子充电。集尘电极布置在容器中以与地电位导电，其中集尘电极由与其面对放电电极的表面上具有透明导电膜的透明板形成。通过使用相对于放电电极的电位差将带电粒子收集在设置在容器中的集尘电极上，并测量集尘电极上的颗粒。

9. 发明授权

US06904787B2 Method for measuring suspended particulate matter in atmospheric air 失效
标题翻译：用于测量大气中悬浮颗粒物的方法
公开(公告)号：US06904787B2
公开(公告)日：2005-06-14
申请号：US10409506
申请日：2003-04-08
申请人： Shinichiro Totoki
发明人： Shinichiro Totoki
IPC分类号： G01N27/60 , G01N1/02 , G01N1/22 , G01N1/24 , G01N15/00 , G01N15/06 , G01N1/00
CPC分类号： G01N15/0618 , G01N1/2202 , G01N1/2273 , G01N1/24 , G01N15/0656 , G01N2001/2223 , G01N2001/2279
摘要： Particulate collector is carried onto airplane and collects suspended particulate matter in the atmospheric air in such a manner that suspended particulate matter is electrically charged by single-pole ions generated by a discharge electrode and the thus electrically charged particulates are attracted to a collecting electrode having an electric potential difference with respect to the discharge electrode so that the particulates are collected by the collecting electrode. The particulate collector is conveyed to an arbitrary altitude and driven so as to collect suspended particulate matter contained in the atmospheric air at the arbitrary altitude. Particulate collector is recovered onto the ground so as to make various measurements or the thus collected particulate collector is subjected to various measurements on airplane.
摘要翻译：颗粒收集器被携带在飞机上并以这样的方式收集大气中的悬浮颗粒物质，使得悬浮的颗粒物质被放电电极产生的单极离子带电，并且因此带电的微粒被吸引到具有相对于放电电极的电位差，使得微粒被收集电极收集。将颗粒收集器输送到任意高度并被驱动以便收集任意高度上包含在大气中的悬浮颗粒物质。将颗粒收集器回收到地面上以进行各种测量，或者如此收集的颗粒收集器在飞机上进行各种测量。

10. 发明授权

US06881246B2 Collecting device for suspended particles 有权
标题翻译：收集悬浮颗粒物
公开(公告)号：US06881246B2
公开(公告)日：2005-04-19
申请号：US10405355
申请日：2003-04-03
申请人： Shinichiro Totoki
发明人： Shinichiro Totoki
IPC分类号： G01N15/02 , B03C3/011 , B03C3/02 , B03C3/09 , B03C3/155 , B03C3/36 , G01N1/02 , B03C3/34
CPC分类号： B03C3/36 , B03C3/011 , B03C3/025 , B03C3/09 , B03C3/155
摘要： A collecting device for collecting suspended particles includes a mobility analysis device; a collecting container connected to an outlet of the mobility analysis device; a discharge electrode disposed inside the collecting container for charging the particles inside the collecting container by generating single polar ions; and a collecting electrode for collecting the charged particles inside the collecting container by an electric potential difference relative to the discharge electrode. In the mobility analysis device, the particles are charged and guided into a flow path. An electric field is created in the flow path, and the particles are guided into the path perpendicular to the electric field. Since a mobility of a particle in an electric field depends on a size of the particle, the particles guided in the path are separated according to the electric field, thereby obtaining particles with sizes in a specific range.
摘要翻译：用于收集悬浮颗粒的收集装置包括移动性分析装置; 连接到移动性分析装置的出口的收集容器; 放电电极，设置在收集容器内部，用于通过产生单极性离子来对收集容器内的颗粒进行充电; 以及收集电极，用于通过相对于放电电极的电位差来收集收集容器内的带电粒子。在移动性分析装置中，将颗粒充电并引导到流路中。在流路中产生电场，并且将粒子引导到垂直于电场的路径中。由于电场中的粒子的迁移率取决于粒子的尺寸，所以在路径中引导的粒子根据电场分离，从而获得尺寸在特定范围内的粒子。

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