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1. 发明授权

US11575150B2 Lithium ion conductive material, all-solid-state secondary battery, and method of manufacturing solid electrolyte 有权
公开(公告)号：US11575150B2
公开(公告)日：2023-02-07
申请号：US16816828
申请日：2020-03-12
申请人： NGK INSULATORS, LTD.
发明人： En Yagi , Yosuke Sato
IPC分类号： H01M10/0562 , H01M10/0525
摘要： A lithium ion conductive material has a composition formula of Lia(OH)bFcCldBr1-d, where 1.8≤a≤2.3, b=a −c−1, 0

2. 发明授权

US10964974B2 Solid electrolyte, all-solid-state lithium-ion secondary battery, production method for solid electrolyte 有权
公开(公告)号：US10964974B2
公开(公告)日：2021-03-30
申请号：US16126182
申请日：2018-09-10
申请人： NGK INSULATORS, LTD.
发明人： Miyuki Kojima , Yosuke Sato , Yuji Katsuda , Yoshiaki Nagasawa , Kazuyuki Kaigawa
IPC分类号： C01B21/097 , C23C14/06 , C23C14/34 , H01M10/0525 , H01M10/0585 , H01M4/38 , H01M10/0562 , H01M4/525 , H01B1/08 , C23C14/35
摘要： A solid electrolyte is constituted by lithium phosphorus oxynitride (LiPON). A multiplication value obtained by multiplying a ratio of a peak intensity of nitrogen atoms having a single bond with one P atom and having a double bond with another P atom to a peak intensity of an N2 state in a Raman spectroscopy spectrum by a ratio of a content amount of N atoms to a content amount of P atoms is greater than or equal to 0.40.

3. 发明授权

US09437463B2 Heating device 有权
标题翻译：加热装置
公开(公告)号：US09437463B2
公开(公告)日：2016-09-06
申请号：US13863729
申请日：2013-04-16
申请人： NGK INSULATORS, LTD.
发明人： Nobuyuki Kondo , Morimichi Watanabe , Asumi Jindo , Yuji Katsuda , Yosuke Sato , Yoshinori Isoda
IPC分类号： H05B3/68 , H01L21/67 , C04B35/581 , H05B1/00 , B32B18/00 , H05B3/28 , H01L21/683 , C04B35/58 , C04B35/626 , C04B35/645 , C04B37/00 , C23C14/34
CPC分类号： H01L21/67 , B32B18/00 , C04B35/58 , C04B35/581 , C04B35/6261 , C04B35/62655 , C04B35/645 , C04B37/001 , C04B37/003 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3865 , C04B2235/5445 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C04B2235/9607 , C04B2237/08 , C04B2237/34 , C04B2237/343 , C04B2237/36 , C04B2237/366 , C04B2237/58 , C04B2237/704 , C04B2237/708 , C04B2237/72 , C23C14/3414 , H01L21/6831 , H05B1/00 , H05B3/283 , Y10T428/24942
摘要： A heating apparatus includes a susceptor having a heating face of heating a semiconductor and a supporting part joined with a back face of the susceptor. The susceptor comprises a ceramic material comprising magnesium, aluminum, oxygen and nitrogen as main components. The material comprises a main phase comprising magnesium-aluminum oxynitride phase exhibiting an XRD peak at least in 2θ=47 to 50° by CuKα X-ray.
摘要翻译：加热装置包括具有加热半导体的加热面的基座和与基座的背面接合的支撑部。感受体包括以镁，铝，氧和氮为主要成分的陶瓷材料。该材料包括主相，其包含通过CuKαX射线表现出至少2θ= 47至50°的XRD峰的镁 - 铝氧氮化物相。

4. 发明授权

US09409824B2 Ceramic material and sputtering target member 有权
标题翻译：陶瓷材料和溅射靶材
公开(公告)号：US09409824B2
公开(公告)日：2016-08-09
申请号：US14692955
申请日：2015-04-22
申请人： NGK Insulators, Ltd.
发明人： Yosuke Sato , Yoshinori Isoda , Yuji Katsuda
IPC分类号： C04B35/053 , C04B35/04 , H01L43/10 , H01L43/12 , G11B5/39 , C23C14/08 , C23C14/34 , G01R33/09 , C01G25/00 , G01R33/00
CPC分类号： C04B35/04 , C01G25/006 , C01P2002/72 , C01P2002/74 , C01P2006/14 , C04B35/053 , C04B2235/3203 , C04B2235/3244 , C04B2235/76 , C04B2235/77 , C23C14/08 , C23C14/3414 , G01R33/0052 , G01R33/098 , G11B5/3909 , H01L43/10 , H01L43/12
摘要： A ceramic material of the present invention contains magnesium, zirconium, lithium, and oxygen as main components. The crystal phase of a solid solution obtained by dissolving zirconium oxide and lithium oxide in magnesium oxide is a main phase. The XRD peak of a (200) plane of the solid solution with CuKα rays preferably appears at 2θ=42.89° or less which is smaller than an angle at which a peak of a cubic crystal of magnesium oxide appears. The XRD peak more preferably appears at 2θ=42.38° to 42.89° and further preferably at 2θ=42.82° to 42.89°. In the ceramic material, the molar ratio Li/Zr of Li to Zr is preferably in the range of 1.96 or more and 2.33 or less.
摘要翻译：本发明的陶瓷材料含有镁，锆，锂和氧作为主要成分。通过将氧化锆和氧化锂溶解在氧化镁中而获得的固溶体的结晶相是主相。具有CuKα射线的固溶体的（200）面的XRD峰最好出现在2θ= 42.89°以下，小于出现氧化镁的立方晶的峰的角度。更优选的XRD峰出现在2θ= 42.38°〜42.89°，进一步优选在2θ= 42.82°〜42.89°。在陶瓷材料中，Li与Zr的摩尔比Li / Zr优选为1.96以上且2.33以下。

5. 发明授权

US09475733B2 Ceramic material and sputtering target member 有权
标题翻译：陶瓷材料和溅射靶材
公开(公告)号：US09475733B2
公开(公告)日：2016-10-25
申请号：US14692922
申请日：2015-04-22
申请人： NGK Insulators, Ltd.
发明人： Yosuke Sato , Yoshinori Isoda , Yuji Katsuda
IPC分类号： C04B35/053 , C23C14/34 , C04B35/04 , H01L43/10 , C23C14/08 , H01L21/02 , H01L43/12 , G11B5/39
CPC分类号： C04B35/04 , C04B35/053 , C04B2235/3203 , C04B2235/3286 , C04B2235/76 , C04B2235/77 , C23C14/08 , C23C14/3414 , G11B5/3909 , H01L21/02175 , H01L21/02194 , H01L21/02266 , H01L43/10 , H01L43/12
摘要： The present invention provides a ceramic material comprising magnesium, gallium, lithium, and oxygen as main components, wherein a crystal phase of a solid solution attained by dissolving gallium oxide and lithium oxide in magnesium oxide is a main phase. An XRD peak of a (200) plane of the solid solution with CuKα rays preferably appears at 2θ=42.91° or more which is larger than an angle at which a peak of a Cubic crystal of magnesium oxide appears, more preferably appears at 2θ=42.91° to 43.28°, and further preferably appears at 2θ=42.91° to 43.02°. In the ceramic material, a molar ratio Li/Ga of Li to Ga is preferably 0.80 or more and 1.20 or less.
摘要翻译：本发明提供一种以镁，镓，锂和氧为主要成分的陶瓷材料，其中通过将氧化镓和氧化锂溶解在氧化镁中而获得的固溶体的结晶相是主相。具有CuKα射线的固溶体的（200）面的XRD峰优选出现在2θ= 42.91°以上，其比出现氧化镁立方晶体的峰的角度大，更优选出现在2θ= 42.91°〜43.28°，进一步优选为2θ= 42.91°〜43.02°。在陶瓷材料中，Li与Ga的Li / Ga摩尔比优选为0.80以上且1.20以下。

6. 发明授权

US09350047B2 Ceramic material and process for producing the same 有权
标题翻译：陶瓷材料及其制造方法
公开(公告)号：US09350047B2
公开(公告)日：2016-05-24
申请号：US14482389
申请日：2014-09-10
申请人： NGK Insulators, Ltd.
发明人： Toshihiro Yoshida , Akihiko Honda , Yosuke Sato
IPC分类号： H01M10/056 , H01M10/0562 , B01J23/10 , B01J23/83 , C04B35/495 , H01M10/052 , C04B35/00 , C04B35/50
CPC分类号： H01M10/0562 , C04B35/00 , C04B35/50 , H01M10/052 , H01M2300/0071 , Y02E60/122
摘要： A ceramic material that can exhibit sufficient compactness and lithium (Li) conductivity to enable the use thereof as a solid electrolyte material for a lithium secondary battery and the like is provided. The ceramic material contains aluminum (Al) and has a garnet-type crystal structure or a garnet-like crystal structure containing lithium (Li), lanthanum (La), zirconium (Zr) and oxygen (O).
摘要翻译：提供了能够表现出足够的致密性和锂（Li）电导率以使其能够用作锂二次电池等的固体电解质材料的陶瓷材料。陶瓷材料含有铝（Al），并且具有石榴石型晶体结构或含有锂（Li），镧（La），锆（Zr）和氧（O）的石榴石状晶体结构。

7. 发明授权

US09287144B2 Heating device 有权
标题翻译：加热装置
公开(公告)号：US09287144B2
公开(公告)日：2016-03-15
申请号：US13863803
申请日：2013-04-16
申请人： NGK INSULATORS, LTD.
发明人： Nobuyuki Kondo , Morimichi Watanabe , Asumi Jindo , Yuji Katsuda , Yosuke Sato , Yoshinori Isoda
IPC分类号： H05B3/02 , H01L21/67 , C04B35/581 , H05B1/00 , B32B18/00 , H05B3/28 , H01L21/683 , C04B35/58 , C04B35/626 , C04B35/645 , C04B37/00 , C23C14/34
CPC分类号： H01L21/67 , B32B18/00 , C04B35/58 , C04B35/581 , C04B35/6261 , C04B35/62655 , C04B35/645 , C04B37/001 , C04B37/003 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3865 , C04B2235/5445 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C04B2235/9607 , C04B2237/08 , C04B2237/34 , C04B2237/343 , C04B2237/36 , C04B2237/366 , C04B2237/58 , C04B2237/704 , C04B2237/708 , C04B2237/72 , C23C14/3414 , H01L21/6831 , H05B1/00 , H05B3/283 , Y10T428/24942
摘要： A heating apparatus 1A includes a susceptor part 9A having a heating face 9a of heating a semiconductor W, and a ring shaped part 6A provided in the outside of the heating face 9a. The ring shaped part 6A is composed of a ceramic material comprising magnesium, aluminum, oxygen and nitrogen as main components. The ceramic material comprises a main phase comprising magnesium-aluminum oxynitride phase exhibiting an XRD peak at least in 2θ=47 to 50° taken by using CuKα ray.
摘要翻译：加热装置1A包括具有加热半导体W的加热面9a的基座部9A和设置在加热面9a的外侧的环状部6A。环形部6A由以镁，铝，氧，氮为主要成分的陶瓷材料构成。陶瓷材料包括主相，其包含镁 - 铝氧氮化物相，其表现出至少2％的XRD峰; =通过使用CuKα射线摄取47至50°。

8. 发明授权

US09209484B2 All-solid-state cell 有权
标题翻译：全固态电池
公开(公告)号：US09209484B2
公开(公告)日：2015-12-08
申请号：US14223169
申请日：2014-03-24
申请人： Kyushu University , NGK Insulators, Ltd.
发明人： Shigeto Okada , Eiji Kobayashi , Kazuhiro Yamamoto , Toshihiro Yoshida , Yosuke Sato
IPC分类号： H01M10/052 , H01M4/58 , H01M10/0562
CPC分类号： H01M10/052 , H01M4/5825 , H01M10/0562
摘要： An all-solid-state cell has a fired solid electrolyte body, a first electrode layer integrally formed on one surface of the fired solid electrolyte body by mixing and firing an electrode active material and a solid electrolyte, and a second electrode layer integrally formed on the other surface of the fired solid electrolyte body by mixing and firing an electrode active material and a solid electrolyte. The first and the second electrode layers are formed by mixing and firing the electrode active material and the amorphous solid electrolyte, which satisfy the relation Ty>Tz (wherein Ty is a temperature at which the capacity of the electrode active material is lowered by reaction between the electrode active material and the solid electrolyte material, and Tz is a temperature at which the solid electrolyte material is shrunk by firing).
摘要翻译：全固体电池具有烧制的固体电解质体，通过混合和烧制电极活性材料和固体电解质而一体地形成在烧制的固体电解质体的一个表面上的第一电极层和与通过混合和烧制电极活性材料和固体电解质来烧制固体电解质体的另一表面。第一和第二电极层通过混合和烧制电极活性材料和无定形固体电解质而形成，其满足关系式Ty> Tz（其中，Ty是电极活性材料的容量通过电极活性物质和固体电解质材料，Tz是固体电解质材料烧成而收缩的温度）。

9. 发明授权

US09202718B2 Electrostatic chuck 有权
标题翻译：静电吸盘
公开(公告)号：US09202718B2
公开(公告)日：2015-12-01
申请号：US13864467
申请日：2013-04-17
申请人： NGK INSULATORS, LTD.
发明人： Kenichiro Aikawa , Morimichi Watanabe , Asumi Jindo , Yuji Katsuda , Yosuke Sato , Yoshinori Isoda
IPC分类号： H01L21/683 , H01L21/67 , C04B35/581 , H05B1/00 , B32B18/00 , H05B3/28 , C04B35/58 , C04B35/626 , C04B35/645 , C04B37/00 , C23C14/34
CPC分类号： H01L21/67 , B32B18/00 , C04B35/58 , C04B35/581 , C04B35/6261 , C04B35/62655 , C04B35/645 , C04B37/001 , C04B37/003 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3865 , C04B2235/5445 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C04B2235/9607 , C04B2237/08 , C04B2237/34 , C04B2237/343 , C04B2237/36 , C04B2237/366 , C04B2237/58 , C04B2237/704 , C04B2237/708 , C04B2237/72 , C23C14/3414 , H01L21/6831 , H05B1/00 , H05B3/283 , Y10T428/24942
摘要： An electrostatic chuck 1A includes a susceptor 11A having an adsorption face 11a of adsorbing a semiconductor, and an electrostatic chuck electrode 4 embedded in the susceptor. The susceptor 11A includes a plate shaped main body 3 and a surface corrosion resistant layer 2 including the adsorption face 2. The surface corrosion resistant layer 2 is made of a ceramic material comprising magnesium, aluminum, oxygen and nitrogen as main components. The ceramic material comprises a main phase comprising magnesium-aluminum oxynitride phase exhibiting an XRD peak at least in 2θ=47 to 50° by CuKα X-ray.
摘要翻译：静电吸盘1A包括具有吸附半导体的吸附面11a的基座11A和嵌入基座的静电卡盘电极4。基座11A包括板状主体3和包括吸附面2的表面耐腐蚀层2.表面耐腐蚀层2由以镁，铝，氧和氮为主要成分的陶瓷材料制成。陶瓷材料包括主相，其包含镁 - 铝氧氮化物相，其表现出至少2％的XRD峰;通过CuKαX射线显示47至50°。

10. 发明授权

US11862785B2 Lithium ion conductive material, all-solid-state secondary battery, and method of manufacturing solid electrolyte 有权
公开(公告)号：US11862785B2
公开(公告)日：2024-01-02
申请号：US17022532
申请日：2020-09-16
申请人： NGK INSULATORS, LTD.
发明人： Miyuki Kojima , Keita Miyanishi , Yosuke Sato , Yuji Katsuda
IPC分类号： H01M4/1315 , C01D15/04 , H01M4/136 , H01M10/0525 , H01M10/0562 , H01M4/02
CPC分类号： H01M4/1315 , C01D15/04 , H01M4/136 , H01M10/0525 , H01M10/0562 , C01P2002/72 , C01P2006/40 , H01M2004/027 , H01M2004/028 , H01M2300/008
摘要： A lithium ion conductive material has a composition formula of Lia(OH)bFcBr, where 1.8≤a≤2.3, b=a−c−1, 0.01≤c≤0.11, and includes an antiperovskite-type crystal phase. Preferably, the lithium ion conductive material further includes a layered antiperovskite-type crystal phase. More preferably, 0≤B/(A+B)≤0.2 is satisfied, where A is the peak intensity in the vicinity of 2θ=31.2° in the X-ray diffractometry using Cu-Kα ray and B is the peak intensity in the vicinity of 2θ=30.2°.

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