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1. 发明授权

US09441054B2 Vinylidene fluoride copolymers 有权
标题翻译：偏二氟乙烯共聚物
公开(公告)号：US09441054B2
公开(公告)日：2016-09-13
申请号：US13995275
申请日：2011-12-13
申请人： Milena Stanga , Bradley Lane Kent , Alessio Marrani , Giulio Brinati
发明人： Milena Stanga , Bradley Lane Kent , Alessio Marrani , Giulio Brinati
IPC分类号： H01M4/00 , C08F14/22 , C08F214/22 , C08J5/22 , C08L27/16 , H01M4/02 , H01M4/86 , H01M8/02 , H01M8/10 , H01M10/0565 , C08K5/06 , C08L33/02
CPC分类号： C08F14/22 , C08F214/22 , C08F214/225 , C08J5/2237 , C08J2327/16 , C08K5/06 , C08L27/16 , C08L33/02 , C08L2205/02 , C08L2205/025 , H01M4/02 , H01M4/8605 , H01M8/0289 , H01M8/1023 , H01M10/0565 , Y02E60/521 , Y02P70/56 , C08F2/16 , C08F220/06 , C08F214/182 , C08F214/24
摘要： The present invention pertains to a fluoropolymer [polymer (F)] comprising: recurring units derived from vinylidene fluoride (VDF), and from 0.01% to 5% by moles of recurring units derived from at least one (meth)acrylic monomer [monomer (MA)] having formula (I) here below: wherein: R1, R2 and R3, equal to or different from each other, are independently selected from a hydrogen atom and a C1-C3 hydrocarbon group, and ROH represents a hydrogen atom or a C1-C5 hydrocarbon moiety comprising at least one hydroxyl group, said polymer (F) comprising end groups having formula —CF2H and/or —CF2CH3 in an amount of at least 30 mmoles per Kg of vinylidene fluoride (VDF) recurring units. The invention also pertains to a process for the manufacture of said polymer (F) and to use of said polymer (F) as binders for the manufacture of electrodes or for the manufacture of membranes.
摘要翻译：本发明还涉及制备所述聚合物（F）的方法和所述聚合物（F）用作制备电极或制造膜的粘合剂。

2. 发明申请

US20130264522A1 Vinylidene fluoride copolymers 有权
标题翻译：偏二氟乙烯共聚物
公开(公告)号：US20130264522A1
公开(公告)日：2013-10-10
申请号：US13995275
申请日：2011-12-13
申请人： Milena Stanga , Bradley Lane Kent , Alessio Marrani , Giulio Brinati
发明人： Milena Stanga , Bradley Lane Kent , Alessio Marrani , Giulio Brinati
IPC分类号： C08F14/22 , C08L33/02 , C08K5/06
CPC分类号： C08F14/22 , C08F214/22 , C08F214/225 , C08J5/2237 , C08J2327/16 , C08K5/06 , C08L27/16 , C08L33/02 , C08L2205/02 , C08L2205/025 , H01M4/02 , H01M4/8605 , H01M8/0289 , H01M8/1023 , H01M10/0565 , Y02E60/521 , Y02P70/56 , C08F2/16 , C08F220/06 , C08F214/182 , C08F214/24
摘要： The present invention pertains to a fluoropolymer [polymer (F)] comprising: recurring units derived from vinylidene fluoride (VDF), and from 0.01% to 5% by moles of recurring units derived from at least one (meth)acrylic monomer [monomer (MA)] having formula (I) here below: wherein: R1, R2 and R3, equal to or different from each other, are independently selected from a hydrogen atom and a C1-C3 hydrocarbon group, and ROH represents a hydrogen atom or a C1-C5 hydrocarbon moiety comprising at least one hydroxyl group, said polymer (F) comprising end groups having formula —CF2H and/or —CF2CH3 in an amount of at least 30 mmoles per Kg of vinylidene fluoride (VDF) recurring units. The invention also pertains to a process for the manufacture of said polymer (F) and to use of said polymer (F) as binders for the manufacture of electrodes or for the manufacture of membranes.
摘要翻译：本发明涉及含氟聚合物[聚合物（F）]，其包含：衍生自偏二氟乙烯（VDF）的重复单元和0.01％至5％（摩尔）来源于至少一种（甲基）丙烯酸单体的重复单元[单体（ MA）]，其中：R 1，R 2和R 3彼此相同或不同，独立地选自氢原子和C1-C3烃基，ROH表示氢原子或包含至少一个羟基的C 1 -C 5烃部分，所述聚合物（F）包含具有式-CF 2 H和/或-CF 2 CH 3的端基，其量为至少30mmol / Kg偏二氟乙烯（VDF）重复单元。本发明还涉及制备所述聚合物（F）的方法和所述聚合物（F）用作制备电极或制造膜的粘合剂。

3. 发明授权

US10079388B2 Aqueous vinylidene fluoride-(meth)acrylic co-polymer latex, electrode and lithium ion secondary battery using the same 有权
公开(公告)号：US10079388B2
公开(公告)日：2018-09-18
申请号：US14232894
申请日：2012-07-13
申请人： Milena Stanga , Riccardo Pieri , Anna Maria Bertasa , Bradley Lane Kent , Giulio Brinati
发明人： Milena Stanga , Riccardo Pieri , Anna Maria Bertasa , Bradley Lane Kent , Giulio Brinati
IPC分类号： H01M4/04 , H01M4/1393 , H01M4/62 , H01M10/0525 , C08L27/16 , C09D127/16 , H01M4/133
CPC分类号： H01M4/623 , C08L27/16 , C09D127/16 , H01M4/0402 , H01M4/0404 , H01M4/133 , H01M4/1393 , H01M4/622 , H01M10/0525
摘要： The present invention pertains to an aqueous composition comprising: (A) an aqueous latex comprising at least one vinylidene fluoride (VDF) polymer [polymer (F)] comprising recurring units derived from vinylidene fluoride (VDF) and at least one (meth)acrylic monomer (MA) having formula (I) here below: wherein: —R1, R2 and R3, equal to or different from each other, are independently selected from a hydrogen atom and a C1-C3 hydrocarbon group, and —ROH is a hydrogen atom or a C1-C5 hydrocarbon moiety comprising at least one hydroxyl group, (B) at least one powdery electrode material, and (C) optionally, less than 10% by weight, based on the total weight of the aqueous composition, of at least one organic solvent (S), wherein the polymer (F) in the aqueous latex is under the form of primary particles having an average primary particle size of less than 1 μm, as measured according to ISO 13321. The present invention also pertains to a process for manufacturing an electrode using said aqueous composition, to an electrode comprising a metal substrate coated on at least one surface with said aqueous composition and to use of said electrode for manufacturing a non-aqueous-type electrochemical device.

4. 发明申请

US20140154573A1 AQUEOUS VINYLIDENE FLUORIDE POLYMER LATEX 审中-公开
标题翻译：水性乙烯基氟化物聚合物
公开(公告)号：US20140154573A1
公开(公告)日：2014-06-05
申请号：US14232894
申请日：2012-07-13
申请人： Milena Stanga , Riccardo Pieri , Anna Maria Bertasa , Bradley Lane Kent , Giulio Brinati
发明人： Milena Stanga , Riccardo Pieri , Anna Maria Bertasa , Bradley Lane Kent , Giulio Brinati
IPC分类号： H01M4/62 , H01M4/04
CPC分类号： H01M4/623 , C08L27/16 , C09D127/16 , H01M4/0402 , H01M4/0404 , H01M4/133 , H01M4/1393 , H01M4/622 , H01M10/0525
摘要： The present invention pertains to an aqueous composition comprising: (A) an aqueous latex comprising at least one vinylidene fluoride (VDF) polymer [polymer (F)] comprising recurring units derived from vinylidene fluoride (VDF) and at least one (meth)acrylic monomer (MA) having formula (I) here below: wherein: —R1, R2 and R3, equal to or different from each other, are independently selected from a hydrogen atom and a C1-C3 hydrocarbon group, and —ROH is a hydrogen atom or a C1-C5 hydrocarbon moiety comprising at least one hydroxyl group, (B) at least one powdery electrode material, and (C) optionally, less than 10% by weight, based on the total weight of the aqueous composition, of at least one organic solvent (S), wherein the polymer (F) in the N aqueous latex is under the form of primary particles having an average primary particle size of less than 1 μm, as measured according to ISO 13321. The present invention also pertains to a process for manufacturing an electrode using said aqueous composition, to an electrode comprising a metal substrate coated on at least one surface with said aqueous composition and to use of said electrode for manufacturing a non-aqueous-type electrochemical device.
摘要翻译：本发明涉及一种水性组合物，其包含：（A）包含至少一种含偏二氯乙烯（VDF）的重复单元和至少一种（甲基）丙烯酸酯的偏二氟乙烯（VDF）聚合物[聚合物（F）具有式（I）的单体（MA）如下：其中：-R1，R2和R3彼此相同或不同，独立地选自氢原子和C1-C3烃基，-ROH是氢原子或包含至少一个羟基的C 1 -C 5烃部分，（B）至少一种粉末状电极材料，和（C）任选地，基于水性组合物的总重量，小于10重量％的至少一种有机溶剂（S），其中根据ISO 13321测量，N水性胶乳中的聚合物（F）的平均初级粒径小于1μm的初级粒子的形式。本发明还涉及涉及使用sai制造电极的方法 d含量的组合物涂覆到包含涂覆在至少一个表面上的金属基材与所述含水组合物并且使用所述电极制造非水型电化学装置的电极。

5. 发明申请

US20110294938A1 Perfluoroelastomer 有权
标题翻译：全氟弹性体
公开(公告)号：US20110294938A1
公开(公告)日：2011-12-01
申请号：US13148094
申请日：2010-02-08
申请人： Milena Stanga , Claudia Manzoni , Margherita Albano
发明人： Milena Stanga , Claudia Manzoni , Margherita Albano
IPC分类号： C08L27/22 , B29C71/02 , C08K3/22 , C08F8/00 , C08F214/26 , C08K5/098
CPC分类号： C08F214/26 , C08F214/262
摘要： A peroxide curable perfluoroelastomer comprising: recurring units derived from tetrafluoroethylene (TFE); and recurring units derived from perfluoromethylvinylether (MVE); such perfluoroelastomer possessing a Mooney Viscosity (ML2+9) at 121° C. of from 25 to 140 MU, when measured according to ASTM D1646 standard, and comprising such MVE recurring units in an amount of from 26 to 33% by moles with respect to total moles of TFE and MVE. A process for the manufacture of such perfluoroelastomer, and cured articles obtainable therefrom.
摘要翻译：一种过氧化物可固化的全氟弹性体，包括：衍生自四氟乙烯（TFE）的重复单元; 和衍生自全氟甲基乙烯基醚（MVE）的重复单元; 这种全氟弹性体在121℃下具有25至140MU的门尼粘度（ML2 + 9），当根据ASTM D1646标准测量时，并且包含这样的MVE重复单元的量为26至33摩尔％，相对于至TFE和MVE的总摩尔数。用于制造这种全氟弹性体的方法以及由其获得的固化制品。

6. 发明授权

US07767764B2 Fluoroelastomers 有权
标题翻译：氟弹性体
公开(公告)号：US07767764B2
公开(公告)日：2010-08-03
申请号：US12162458
申请日：2007-01-15
申请人： Milena Stanga , Francesco Triulzi , Margherita Albano
发明人： Milena Stanga , Francesco Triulzi , Margherita Albano
IPC分类号： C08F14/18
CPC分类号： C08F214/22 , C08F214/222 , C08L27/16 , C08L27/18 , C08L2205/02 , C08L2666/04
摘要： VDF curable fluoroelastomers, ionically cured, having a compression set after a time of 24 h (ASTM D 39/B) at −10° C. lower than 60%, preferably lower than 50% and at −25° C. lower than 90%, preferably lower than 75%, comprising hexafluoropropene (HFP) in amounts higher than 10% by moles and one vinylether of formula: CF2═CFOCF2OCF3 (a), an amount of —COF and groups in the polymer lower than the sensitivity limit of the method using the FT-IR spectroscopy described in the present application.
摘要翻译： VDF固化的含氟弹性体，在-10℃下在24小时后（ASTM D 39 / B）具有压缩永久变形，低于60％，优选低于50％和-25℃，低于90° ％，优选低于75％，其含量高于10摩尔％的六氟丙烯（HFP），和一个式为CF 2 CFCFF 2 OCF 3（a）的乙烯基醚，其中-COF的含量低于聚合物的灵敏度极限该方法使用本申请中描述的FT-IR光谱。

7. 发明申请

US20110237751A1 Vulcanized (per)fluoroelastomer sealing articles 有权
标题翻译：硫化（per）含氟弹性体密封制品
公开(公告)号：US20110237751A1
公开(公告)日：2011-09-29
申请号：US13132333
申请日：2009-12-03
申请人： Milena Stanga , Claudia Manzoni , Giovanni Comino , Margherita Albano
发明人： Milena Stanga , Claudia Manzoni , Giovanni Comino , Margherita Albano
IPC分类号： C08L27/16 , C08L29/10 , C08J3/24
CPC分类号： C09K3/1009 , C08L27/16 , C08L2205/02 , C08L2666/04
摘要： This invention pertains to sealing articles of vulcanized (per)fluoroelastomer compositions incorporating particles of a vinylidene fluoride (VDF) polymers having a Shore A hardness of at least 85 when determined according to ASTM D 2240 Type A Durometer method, and a compression set of less than 30%, when determined according to ASTM D395 at 200° C. for 70 h on O-ring according to ASTM D1414, and to a process for their manufacture by vulcanizing-molding and thermal post-treating at a temperature above the melting point of the VDF polymer.
摘要翻译：本发明涉及根据ASTM D 2240 A型硬度计方法测定的硫化（每）含氟弹性体组合物的密封制品，该组合物结合了具有至少85的肖氏A硬度的偏二氟乙烯（VDF）聚合物的颗粒，并且压缩永久变形当根据ASTM D395在200℃下根据ASTM D1414在O型圈上测定70小时时，其含量超过30％，以及在高于熔点的温度下通过硫化模塑和热后处理制造的方法的VDF聚合物。

8. 发明申请

US20100311909A1 Vulcanisable fluoroelastomeric compositions 有权
标题翻译：可硫化含氟弹性体组合物
公开(公告)号：US20100311909A1
公开(公告)日：2010-12-09
申请号：US12743204
申请日：2008-11-20
申请人： Giovanni Comino , Claudia Manzoni , Milena Stanga , Margherita Albano
发明人： Giovanni Comino , Claudia Manzoni , Milena Stanga , Margherita Albano
IPC分类号： C08L27/16 , C08L27/18
CPC分类号： C08L27/16 , C08L27/12 , C08L27/18 , C08L27/20 , C08L51/003 , C08L2205/02 , C08L2666/24 , C08L2666/04
摘要： Vulcanizable fluoroelastomer compositions comprising: A) a fluoroelastomer matrix based on vinylidene fluoride (VDF) with a Mooney viscosity (1+10) at 121° C. of less than 35 MU (Mooney Units) measured according to ASTM standard D 1646; and B) a semi-crystalline fluoropolymer, in an amount of from 20% to 70% by weight relative to the total weight of A)+B), the semi-crystalline fluoropolymer being constituted of tetrafluoroethylene (TFE) homopolymers and copolymers of TFE with one or more monomers containing at least one unsaturation of ethylenic type, in an amount of from 0.01 to 10 mol %, said semi-crystalline fluoropolymer having a mean particle size between 10 and 400 nm.
摘要翻译：可硫化的含氟弹性体组合物，其包含：A）基于偏二氟乙烯（VDF）的氟弹性体基体，其在121℃下的门尼粘度（1 + 10）根据ASTM标准D1646测量小于35MU（门尼单位）; 和B）相对于A）+ B）的总重量为20重量％至70重量％的半结晶含氟聚合物），半结晶含氟聚合物由四氟乙烯（TFE）均聚物和TFE共聚物构成所述半结晶含氟聚合物的平均粒度为10-400nm，其中一种或多种含有烯属型不饱和键的单体的量为0.01至10mol％。

9. 发明授权

US09234063B2 Perfluoroelastomer 有权
标题翻译：全氟弹性体
公开(公告)号：US09234063B2
公开(公告)日：2016-01-12
申请号：US13148094
申请日：2010-02-08
申请人： Milena Stanga , Claudia Manzoni , Margherita Albano
发明人： Milena Stanga , Claudia Manzoni , Margherita Albano
IPC分类号： C08L27/22 , C08F8/00 , C08F214/26
CPC分类号： C08F214/26 , C08F214/262
摘要： A peroxide curable perfluoroelastomer comprising: recurring units derived from tetrafluoroethylene (TFE); and recurring units derived from perfluoromethylvinylether (MVE); such perfluoroelastomer possessing a Mooney Viscosity (ML2+9) at 121° C. of from 25 to 140 MU, when measured according to ASTM D1646 standard, and comprising such MVE recurring units in an amount of from 26 to 33% by moles with respect to total moles of TFE and MVE. A process for the manufacture of such perfluoroelastomer, and cured articles obtainable therefrom.
摘要翻译：一种过氧化物可固化的全氟弹性体，包括：衍生自四氟乙烯（TFE）的重复单元; 和衍生自全氟甲基乙烯基醚（MVE）的重复单元; 这种全氟弹性体在121℃下具有25至140MU的门尼粘度（ML2 + 9），当根据ASTM D1646标准测量时，并且包含这样的MVE重复单元的量为26至33摩尔％，相对于至TFE和MVE的总摩尔数。用于制造这种全氟弹性体的方法以及由其获得的固化制品。

10. 发明授权

US08168714B2 (Per)fluoroelastomeric compositions 有权
标题翻译：（Per）含氟弹性体组合物
公开(公告)号：US08168714B2
公开(公告)日：2012-05-01
申请号：US12307061
申请日：2007-06-28
申请人： Milena Stanga , Giovanni Comino , Margherita Albano
发明人： Milena Stanga , Giovanni Comino , Margherita Albano
IPC分类号： C08L27/12
CPC分类号： C08K3/36 , C08F214/16 , C08F214/18 , C08F214/184 , C08F214/26 , C08K5/0025 , C08L27/12
摘要： A (per)fluoroelastomeric composition curable by peroxidic way comprising: 100 phr as (per)fluoroelastomer as filler, 0.5-50 phr of silica having a pH value, determined according to the DIN ISO 787-9 standard, higher than 7, preferably higher than 8, as crosslinking agent, from 0.5 to 10 phr of a bis-olefin having general formula: wherein: R1, R2, R3, R4, R5, R6, equal to or different from each other, are H or C1-C5 alkyls; Z is selected between a C1-C18 linear or branched alkylene or cycloalkylene radical, optionally containing oxygen atoms, preferably at least partially fluorinated, or a (per)fluoropolyoxyalkylene radical.
摘要翻译：通过过氧化物方法可固化的（全）含氟弹性体组合物，其包含：100phr作为（作为填料）的（含氟弹性体），0.5-50phr的具有pH值的二氧化硅，根据DIN ISO 787-9标准测定，高于7，优选较高作为交联剂，为0.5〜10phr的具有以下通式的双烯烃：其中：R 1，R 2，R 3，R 4，R 5，R 6，彼此相同或不同，为H或C 1 -C 5烷基 ; Z选自C1-C18直链或支链亚烷基或亚环烷基，任选地含有氧原子，优选至少部分氟化，或（全）氟聚氧亚烷基。

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