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1. 发明授权

US5880167A Polyurethane compositions with a low content of monomeric diisocyanates 失效
标题翻译：具有低含量单体二异氰酸酯的聚氨酯组合物
公开(公告)号：US5880167A
公开(公告)日：1999-03-09
申请号：US793024
申请日：1997-03-27
申请人： Michael Krebs , Gerd Bolte , Christa Dernst-Mentges , Guenter Henke , Wolfgang Klauck , Hermann Kluth , Manfred Schumann
发明人： Michael Krebs , Gerd Bolte , Christa Dernst-Mentges , Guenter Henke , Wolfgang Klauck , Hermann Kluth , Manfred Schumann
IPC分类号： C08J9/14 , C08G18/10 , C08G18/28 , C08G18/72 , C08G18/76 , C08G18/78 , C08G18/79 , C08G18/80 , C08G101/00 , C09J175/04 , C08L75/04
CPC分类号： C08G18/8061 , C08G18/2805 , C08G18/282 , C08G18/2825 , C08G18/289 , C08G18/72 , C08G18/7664 , C09J175/04 , C08G2170/20
摘要： The invention relates to polyurethane compositions with a low content of monomeric diisocyanates. Trifunctional isocyanates optionally reduced in their functionality to 3.0.+-.0.7 with a monofunctional terminator are preferably used for this purpose. In this way, the compositions contain considerably smaller quantities of readily volatile isocyanates. The compositions are suitable for use as reactive hotmelt adhesives, lamination adhesives, adhesive/sealing compounds, primers and for the production of foam plastics from non-reusable pressurized containers (aerosol cans). The low content of volatile monomeric diisocyanates enables the need for safety measures in the workplace to be significantly reduced, in addition to which the disposal of residues remaining in the containers is made considerably easier.
摘要翻译： PCT No.PCT / EP95 / 03216 Sec。 371日期1997年3月27日 102（e）1997年3月27日PCT PCT 1995年8月14日PCT公布。出版物WO96 / 06124 日期1996年2月29日本发明涉及具有低含量的单体二异氰酸酯的聚氨酯组合物。为了这个目的，优选使用三官能异氰酸酯，其功能性任选地用单官能终止剂还原为3.0 +/- 0.7。以这种方式，组合物含有相当少量的易挥发的异氰酸酯。该组合物适合用作反应性热熔粘合剂，层压粘合剂，粘合/密封化合物，底漆和用于从不可重复使用的加压容器（气溶胶罐）生产泡沫塑料。挥发性单体二异氰酸酯的低含量使得能够显着降低在工作场所中的安全措施的需要，另外残留在容器中的残留物的处理变得相当容易。

2. 发明授权

US5464494A Dispersion-based heat-sealable coating 失效
标题翻译：基于分散体的可热封涂层
公开(公告)号：US5464494A
公开(公告)日：1995-11-07
申请号：US240751
申请日：1994-05-10
申请人： Gerd Bolte , Guenter Henke , Ulrike Brueninghaus
发明人： Gerd Bolte , Guenter Henke , Ulrike Brueninghaus
IPC分类号： C09D163/00 , C08L63/00 , C09D175/00 , C09D175/04 , C09J163/00 , C09J175/04 , H01B3/30 , H05K3/28 , C09J5/06 , C09J135/02 , C09J163/02
CPC分类号： C09D175/04 , C08L63/00 , C09J175/04 , C08G2270/00 , H05K3/285
摘要： Film-forming reactive systems for the surface-to-surface bonding and/or coating of substrates, more particularly for heat-sealable coatings are provided. The system is based on an aqueous dispersion of at least two epoxy-curable resins (I) and an epoxy compound as the curing component (II). The epoxy-curable resins are a polyurethane polymer containing epoxy-reactive functional groups present as the curable resin (Ia) and an aqueous dispersion of an acrylate and/or methacrylate homopolymer or copolymer containing carboxyl and/or methylol groups present as an additional curable resin (Ib). Also provided is a method for the production of laminates which employs the reactive system to bond substrates.
摘要翻译： PCT No.PCT / EP92 / 02553 Sec。 371日期1994年5月10日 102（e）日期1994年5月10日PCT提交1992年11月6日PCT公布。公开号WO93 / 10202 PCT 日期：1993年5月27日。提供了用于表面 - 表面粘结和/或涂覆基材的成膜反应体系，更具体地涉及可热封的涂层。该系统基于至少两种环氧固化树脂（I）和作为固化组分（II）的环氧化合物的水分散体。环氧固化树脂是含有作为可固化树脂（Ia）存在的环氧反应性官能团和含有羧基和/或羟甲基的丙烯酸酯和/或甲基丙烯酸酯均聚物或共聚物的水性分散体的聚氨酯聚合物，作为附加的固化性树脂（Ib）。还提供了一种用于生产层压板的方法，其采用反应体系来粘结基材。

3. 发明授权

US06903167B2 Polyurethane prepolymers comprising NCO groups and a low content of monomeric polyisocyanate 有权
标题翻译：包含NCO基团和低含量单体多异氰酸酯的聚氨酯预聚物
公开(公告)号：US06903167B2
公开(公告)日：2005-06-07
申请号：US10448849
申请日：2003-05-30
申请人： Gerd Bolte , Guenter Henke , Claudia Meckel-Jonas , Dagmar Jahns
发明人： Gerd Bolte , Guenter Henke , Claudia Meckel-Jonas , Dagmar Jahns
IPC分类号： C08G18/10 , C08G18/12 , C08G18/40 , C08G18/42 , C09J175/04
CPC分类号： C09J175/04 , C08G18/10 , C08G18/12 , C08G18/4018 , C08G18/4216 , Y10S528/905 , C08G18/7843 , C08G18/42
摘要： Polyurethane prepolymers containing NCO (isocyanate) groups and having a low content of monomeric polyisocyanate, processes for their production and uses employing these prepolymers. The polyurethane prepolymers of the invention are produced from by a reaction employing monomeric polyisocyanates and polyols.
摘要翻译：含有NCO（异氰酸酯）基团并且具有低含量的单体多异氰酸酯的聚氨酯预聚物，其制备方法和使用这些预聚物。通过使用单体多异氰酸酯和多元醇的反应制备本发明的聚氨酯预聚物。

4. 发明授权

US06515164B1 Low monomer polyurethane prepolymer and process therefore 有权
标题翻译：低单体聚氨酯预聚物和工艺因此
公开(公告)号：US06515164B1
公开(公告)日：2003-02-04
申请号：US09341080
申请日：1999-07-02
申请人： Gerd Bolte , Guenter Henke , Markus Kruedenscheidt , Astrid Omoruyi
发明人： Gerd Bolte , Guenter Henke , Markus Kruedenscheidt , Astrid Omoruyi
IPC分类号： C07C26902
CPC分类号： C09J175/04 , B32B7/12 , C08G18/10 , C08G18/721 , C08G18/7607 , C08G18/7621 , C08G18/7671
摘要： A low-monomer PU prepolymer containing free NCO groups which is obtained from polyhydric alcohols and diisocyanates differing in their reactivity and which is distinguished by the ratio of the NCO groups of the partly slower-reacting diisocyanate to the NCO groups of the faster-reacting diisocyanate. It is greater than 6:1. Nevertheless the prepolymer according to the invention cures more quickly than a known prepolymer predominantly containing fast-reacting NCO groups. In a preferred embodiment, TDI is used as the partly slower-reacting diisocyanate while MDI is used as the faster-reacting diisocyanate. The prepolymer is produced in two stages. The prepolymer according to the invention is suitable for bonding plastic articles, metals and paper, especially films. The accelerated absence of migration is particularly noticeable in this regard.
摘要翻译：含有游离NCO基团的低单体PU预聚物，其由多元醇和其反应性不同的二异氰酸酯获得，其特征在于部分较慢反应的二异氰酸酯的NCO基团与较快反应的二异氰酸酯的NCO基团的比例。大于6：1。然而，根据本发明的预聚物比主要含有快速反应的NCO基团的已知预聚物更快地固化。在优选的实施方案中，TDI用作部分较慢反应的二异氰酸酯，而MDI用作较快反应的二异氰酸酯。预聚物分两个阶段生产。根据本发明的预聚物适用于粘合塑料制品，金属和纸，特别是薄膜。在这方面，加速不存在移民尤其明显。

5. 发明申请

US20060247326A1 Adhesive composition with barrier characteristics 审中-公开
标题翻译：具有阻隔特性的粘合剂组合物
公开(公告)号：US20060247326A1
公开(公告)日：2006-11-02
申请号：US11377487
申请日：2006-03-16
申请人： Guenter Henke , Markus Kruedenscheidt , Claudia Meckel-Jonas
发明人： Guenter Henke , Markus Kruedenscheidt , Claudia Meckel-Jonas
IPC分类号： B29C71/04
CPC分类号： B82Y30/00 , C08G18/10 , C08G18/289 , C08G18/672 , C08G2190/00 , C08K2201/011 , C08L75/04 , C09J11/04 , C09J175/04
摘要： An adhesive composition having barrier characteristics contains a) a compound having at least one NCO group and at least one reactive functional group that can be cured by irradiation and b) a nanoscale filler. Such compositions are useful as radiation curable one-component or two-component adhesives, particularly in the production of composite films with barrier characteristics. Composite films prepared in this manner can be utilized to package foods and medicaments.
摘要翻译：具有阻隔特性的粘合剂组合物包含a）具有至少一个NCO基团的化合物和至少一个可通过照射固化的反应性官能团，以及b）纳米级填料。这种组合物可用作可辐射固化的单组分或双组分粘合剂，特别是在制备具有阻隔特性的复合膜时。以这种方式制备的复合薄膜可用于包装食品和药物。

6. 发明授权

US06784242B2 Polyurethane binding agents having a low content of highly volatile monomers 有权
标题翻译：具有低挥发性单体含量的聚氨酯粘合剂
公开(公告)号：US06784242B2
公开(公告)日：2004-08-31
申请号：US10140784
申请日：2002-05-06
申请人： Achim Huebener , Guenter Henke , Andreas Bauer
发明人： Achim Huebener , Guenter Henke , Andreas Bauer
IPC分类号： C08J300
CPC分类号： C08G18/6674 , C08G18/12 , C08G18/8019 , C09J175/04 , Y10T428/31551
摘要： A polyurethane binder with a low content of readily volatile isocyanate-functional monomer is provided by a process of (a) reacting a first at least difunctional isocyanate and a first polyol component at an NCO:OH ratio less than 2 wherein the first at least difunctional isocyanate has an NCO group with a slower rate of reaction with the OH groups than a second NCO group to produce a reaction product containing free OH groups and reacting the reaction product with a second polyol and a second at least difunctional isocyanate wherein the second at least difunctional isocyanate has isocyanate groups with a more rapid rate of reaction with the OH groups than the predominent percentage of isocyanate groups present in the reaction product.
摘要翻译：通过以下方法提供具有低挥发性异氰酸酯官能单体含量低的聚氨酯粘合剂：（a）使第一至少二官能异氰酸酯与低于2的NCO:HOH比率的第一多元醇组分反应，其中第一至少双官能异氰酸酯具有与第二NCO基团相比，OH基反应速度较慢的NCO基团，以产生含有游离OH基团的反应产物并使反应产物与第二多元醇和第二至少二官能异氰酸酯反应，其中至少二双官能异氰酸酯具有与OH基反应速度更快的异氰酸酯基，优于反应产物中存在的异氰酸酯基的主要百分比。

7. 发明申请

US20060162860A1 Binding agents having barrier properties 失效
标题翻译：具有阻隔性的结合剂
公开(公告)号：US20060162860A1
公开(公告)日：2006-07-27
申请号：US11388000
申请日：2006-03-23
申请人： Guenter Henke , Kamil Kalus , Annabelle Guilleux
发明人： Guenter Henke , Kamil Kalus , Annabelle Guilleux
IPC分类号： B32B7/12
CPC分类号： C09J175/16 , C08G18/10 , C08G18/289 , C08G18/672 , C08G18/809 , C08G18/8175 , C09D175/16
摘要： Binding agents having barrier properties are provided which contain: a) a compound having at least one NCO group and at least one reactive functional group, which can be cured by radiation and which serves as component (A), and; b) a silicon-organic compound serving as component (B) with at least one NCO group and at least one functional group of formula (I): —Si(X)3-n, in which X represents —NH2; —NH—CO—R; —OOC—R; —O—N═C(R)2 or OR′; R represents a linear or branched, saturated or unsaturated C1-C18 alkyl radical; R′ represents R, an oxyalkylene radical having up to 4 carbon atoms, a C5-C8 cycloalkyl radical; a C6-C10 aryl radical or a C7-C12 aralkyl radical; and n equals 0, 1 or 2. The binding agent can be used as a radiation curable binding agent in coating agents, fillers, sealants or adhesives, for example in the preparation of laminated films having barrier properties.
摘要翻译：提供具有阻隔性的结合剂，其含有：a）具有至少一个NCO基团和至少一个反应性官能团的化合物，其可通过辐射固化并用作组分（A），和 b）具有至少一个NCO基团和至少一个式（I）官能团的组分（B）的硅 - 有机化合物：-Si（X）3-n，其中X 表示-NH 2。 -NH-CO-R; -OOC-R; -O-N-C（R）2或OR'; R表示直链或支链，饱和或不饱和的C1-C18烷基; R'表示R，具有至多4个碳原子的氧亚烷基，C5-C8环烷基; C 6 -C 10芳基或C 7 -C 12芳烷基; 并且n等于0,1或2.粘合剂可用作包衣剂，填料，密封剂或粘合剂中的可辐射固化粘合剂，例如用于制备具有阻隔性的层压膜。

8. 发明授权

US06548566B1 Laminating adhesives hardenable by radiation 失效
标题翻译：层压粘合剂可通过辐射固化
公开(公告)号：US06548566B1
公开(公告)日：2003-04-15
申请号：US09582301
申请日：2000-08-15
申请人： Achim Huebener , Guenter Henke , Michael Drobnik
发明人： Achim Huebener , Guenter Henke , Michael Drobnik
IPC分类号： C08G5962
CPC分类号： C09J163/00 , C08G59/62 , C08L2666/14 , C09J11/00 , Y10T428/31515
摘要： A method of forming a film laminate uses an adhesive containing at least three components A, B and C. The method includes providing a radiation curable adhesive that contains a) a compound bearing at least one epoxy group, b) a compound with at least three OH groups and a molecular weight below 400 and c) a photoinitiator which initiates a polymerization of components a) and b) after exposure to light with a wavelength of 100 to 600 nm.
摘要翻译：形成膜层叠体的方法使用含有至少三种组分A，B和C的粘合剂。该方法包括提供可辐射固化的粘合剂，其包含a）具有至少一个环氧基的化合物，b）具有至少三个 OH基团，分子量低于400，c）引发组分a）和b）的聚合的光引发剂，其在暴露于波长为100至600nm的光后。

9. 发明授权

US07419564B2 Binding agents having barrier properties 失效
标题翻译：具有阻隔性的结合剂
公开(公告)号：US07419564B2
公开(公告)日：2008-09-02
申请号：US11388000
申请日：2006-03-23
申请人： Guenter Henke , Kamil Kalus , Annabelle Guilleux
发明人： Guenter Henke , Kamil Kalus , Annabelle Guilleux
IPC分类号： B29C65/48 , C08G18/04 , C08G18/06 , C08F2/48
CPC分类号： C09J175/16 , C08G18/10 , C08G18/289 , C08G18/672 , C08G18/809 , C08G18/8175 , C09D175/16
摘要： Binding agents having barrier properties are provided which contain: a) a compound having at least one NCO group and at least one reactive functional group, which can be cured by radiation and which serves as component (A), and; b) a silicon-organic compound serving as component (B) with at least one NCO group and at least one functional group of formula (I): —Si(Z)n(X)3−n, in which Z represents C1-C18alkyl group, preferably C1-C4alkyl group; X represents —NH2; —NH—CO—R; —OOC—R; —O—N═C(R)2 or OR′; R represents a linear or branched, saturated or unsaturated C1-C18alkyl radical; R′ represents R, an oxyalkylene radical having up to 4 carbon atoms, a C5-C8 cycloalkyl radical; a C6-C10 aryl radical or a C7-C12 aralkyl radical; and n equals 0, 1 or 2. The binding agent can be used as a radiation curable binding agent in coating agents, fillers, sealants or adhesives, for example in the preparation of laminated films having barrier properties.
摘要翻译：提供具有阻隔性的结合剂，其含有：a）具有至少一个NCO基团和至少一个反应性官能团的化合物，其可通过辐射固化并用作组分（A），和 b）具有至少一个NCO基团和至少一个式（I）官能团的用作组分（B）的硅 - 有机化合物：-Si（Z）n（X） 3-n，其中Z表示C 1 -C 18烷基，优选C 1 -C 4烷基烷基; X表示-NH 2。 -NH-CO-R; -OOC-R; -O-N-C（R）2或OR'; R表示直链或支链的饱和或不饱和的C 1 -C 18烷基; R'表示R，具有至多4个碳原子的氧亚烷基，C 5 -C 8环烷基; C 6 -C 10芳基或C 7 -C 12芳烷基; C 6 -C 12芳基或C 7 -C 12芳烷基; 并且n等于0,1或2.粘合剂可用作包衣剂，填料，密封剂或粘合剂中的可辐射固化粘合剂，例如用于制备具有阻隔性的层压膜。

10. 发明授权

US06565696B1 Laminating adhesive hardenable by radiation and use of same 失效
标题翻译：层压粘合剂可通过辐射固化，并使用它
公开(公告)号：US06565696B1
公开(公告)日：2003-05-20
申请号：US09582244
申请日：2000-08-24
申请人： Achim Huebener , Guenter Henke , Michael Drobnik
发明人： Achim Huebener , Guenter Henke , Michael Drobnik
IPC分类号： B32B3100
CPC分类号： C09J11/00
摘要： An adhesive containing a) a compound containing at least one vinyl ether group which has a molecular weight of more than 400 and b) a photoinitiator which initiates a polymerization of component A after exposure to light with a wavelength of 100 to 600 nm is useful for the production of a film laminate.
摘要翻译：含有a）含有至少一种分子量大于400的乙烯基醚基的化合物和b）在暴露于波长为100至600nm的光后引发组分A的聚合的光引发剂可用于生产薄膜层压板。

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