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1. 发明申请

US20050245751A1 Integrated method for synthesis propylene oxide 有权
标题翻译：合成环氧丙烷的综合方法
公开(公告)号：US20050245751A1
公开(公告)日：2005-11-03
申请号：US10526045
申请日：2003-08-29
申请人： Michael Bender , Peter Zehner , Otto Machhammer , Ulrich Muller , Klaus Harth , Gotz-Peter Schindler , Henrik Junicke
发明人： Michael Bender , Peter Zehner , Otto Machhammer , Ulrich Muller , Klaus Harth , Gotz-Peter Schindler , Henrik Junicke
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/125 , Y02P20/582
摘要： The present invention relates to an integrated process for the synthesis of propylene oxide, which comprises at least the following steps: (i) dehydrogenation of propane to give a substream T (0) comprising at least propane, propene and hydrogen; (ii) fractionation of the substream T (0) to give at least one gaseous hydrogen-rich substream T (2) and a substream T (1) comprising at least propene and propane; (iii) synthesis of hydrogen peroxide using the substream T (2), giving a substream T (4) which is rich in hydrogen peroxide and a gaseous substream T (6); (iv) fractionation of the substream T (1) to give at least one propane-rich substream T (5) and at least one propene-rich substream T (3); (v) reaction of the at least one substream T (3) with substream T (4) to give propylene oxide.
摘要翻译：本发明涉及一种用于合成环氧丙烷的综合方法，其包括至少以下步骤：（i）丙烷脱氢得到至少包含丙烷，丙烯和氢的分支T（O）; （ii）分流T（0）以产生至少一个富含气体的气流T（2）和至少包含丙烯和丙烷的子流T（1）; （iii）使用子流T（2）合成过氧化氢，得到富含过氧化氢的气流T（4）和气态分支T（6）; （iv）分流T（1）以产生至少一个富含丙烷的子流T（5）和至少一个富含丙烯的子流T（3）; （v）至少一个子流T（3）与子流T（4）的反应，得到环氧丙烷。

2. 发明授权

US07173143B2 Integrated method for synthesis propylene oxide 有权
标题翻译：合成环氧丙烷的综合方法
公开(公告)号：US07173143B2
公开(公告)日：2007-02-06
申请号：US10526045
申请日：2003-08-29
申请人： Michael Bender , Peter Zehner , Otto Machhammer , Ulrich Mueller , Klaus Harth , Goetz-Peter Schindler , Henrik Junicke
发明人： Michael Bender , Peter Zehner , Otto Machhammer , Ulrich Mueller , Klaus Harth , Goetz-Peter Schindler , Henrik Junicke
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/125 , Y02P20/582
摘要： The present invention relates to an integrated process for the synthesis of propylene oxide, which comprises at least the following steps: (i) dehydrogenation of propane to give a substream T(0) comprising at least propane, propene and hydrogen; (ii) fractionation of the substream T(0) to give at least one gaseous hydrogen-rich substream T(2) and a substream T(1) comprising at least propene and propane; (iii) synthesis of hydrogen peroxide using the substream T(2), giving a substream T (4) which is rich in hydrogen peroxide and a gaseous substream T(6); (iv) fractionation of the substream T(1) to give at least one propane-rich substream T(5) and at least one propene-rich substream T(3); (v) reaction of the at least one substream T(3) with substream T(4) to give propylene oxide.
摘要翻译：本发明涉及一种用于合成环氧丙烷的综合方法，其包括至少以下步骤：（i）丙烷脱氢得到至少包含丙烷，丙烯和氢的分支T（O）; （ii）分流T（0）以产生至少一个富含气体的气流T（2）和至少包含丙烯和丙烷的子流T（1）; （iii）使用子流T（2）合成过氧化氢，得到富含过氧化氢的气流T（4）和气态分支T（6）; （iv）分流T（1）以产生至少一个富含丙烷的子流T（5）和至少一个富含丙烯的子流T（3）; （v）至少一个子流T（3）与子流T（4）的反应，得到环氧丙烷。

3. 发明申请

US20060057057A1 Process for preparing hydrogen peroxide from the elements 有权
标题翻译：从元素制备过氧化氢的方法
公开(公告)号：US20060057057A1
公开(公告)日：2006-03-16
申请号：US11258265
申请日：2005-10-26
申请人： Ulrich Muller , Olga Metelkina , Henrik Junicke , Thomas Butz , Omar Yaghi
发明人： Ulrich Muller , Olga Metelkina , Henrik Junicke , Thomas Butz , Omar Yaghi
IPC分类号： C01B15/029 , C07F15/00
CPC分类号： C01B15/029 , B01J23/44 , B01J23/60 , B01J31/1691 , B01J31/2239 , B01J35/002 , B01J35/1057 , B01J35/1061 , B01J2531/20 , B01J2531/26 , B01J2531/30 , B01J2531/40 , B01J2531/50 , B01J2531/60 , B01J2531/70 , B01J2531/80
摘要： The present invention relates to a process for the preparation of hydrogen peroxide from oxygen or oxygen-delivering substances and hydrogen or hydrogen-delivering substances in the presence of at least one catalyst containing a metal-organic framework material, wherein said framework material comprises pores and a metal ion and an at least bidentate organic compound, said bidentate organic compound being coordinately bound to the metal ion. The invention further relates to a novel material consisting of said metal organic framework material wherein the material is brought in contact with at least one additional metal.
摘要翻译：本发明涉及一种在至少一种含有金属 - 有机骨架材料的催化剂存在下由氧气或氧气输送物质和氢气或氢气输送物质制备过氧化氢的方法，其中所述骨架材料包括孔和金属离子和至少二齿有机化合物，所述二齿有机化合物与金属离子配位结合。本发明还涉及由所述金属有机骨架材料组成的新材料，其中所述材料与至少一种另外的金属接触。

4. 发明申请

US20080207953A1 Catalyst and Method for Hyrogenating Carbonyl Compounds 审中-公开
标题翻译：羰基化合物的催化剂和方法
公开(公告)号：US20080207953A1
公开(公告)日：2008-08-28
申请号：US11994500
申请日：2006-07-06
申请人： Christophe Houssin , Henrik Junicke , Ulrich Muller
发明人： Christophe Houssin , Henrik Junicke , Ulrich Muller
IPC分类号： C07C47/00 , B01J21/18
CPC分类号： C07C29/149 , B01J23/72 , B01J23/83 , B01J23/835 , B01J23/885 , B01J23/888 , B01J23/8892 , B01J37/0009 , B01J37/03 , B01J37/10 , C07C31/20
摘要： Process for hydrogenating an organic compound having at least one carbonyl group, in which the organic compound is contacted, in the presence of hydrogen, with a shaped body which is producible in a process in which (i) an oxidic material comprising copper oxide and aluminum oxide and at least one of the oxides of iron, lanthanum, tungsten, molybdenum, titanium, zirconium, tin or manganese, and if appropriate additionally tin oxide and/or manganese oxide, is provided, (ii) pulverulent metallic copper, copper flakes, pulverulent cement, graphite or a mixture thereof are added to the oxidic material, (iii) the mixture resulting from (ii) is shaped to a shaped body and (iv) the shaped body is treated with water or steam.
摘要翻译：氢化具有至少一个有机化合物的有机化合物的有机化合物的方法，其中有机化合物在氢的存在下与成型体形成，所述成形体可以在以下工艺中生产：（i）包含氧化铜和铝的氧化物质氧化物和铁，镧，钨，钼，钛，锆，锡或锰的氧化物中的至少一种，以及如果合适的话另外提供氧化锡和/或氧化锰，（ii）粉状金属铜，铜片，将粉末状水泥，石墨或其混合物加入到氧化物中，（iii）由（ii）得到的混合物成形为成形体，（iv）成形体用水或蒸汽处理。

5. 发明申请

US20050241478A1 Adsorption mass and method for removing carbon monoxide from flows of material 有权
标题翻译：吸附质量和从物料流中除去一氧化碳的方法
公开(公告)号：US20050241478A1
公开(公告)日：2005-11-03
申请号：US10526677
申请日：2003-09-11
申请人： Henrik Junicke , Markus Holzle , Michael Bender
发明人： Henrik Junicke , Markus Holzle , Michael Bender
IPC分类号： B01D53/04 , B01J20/06 , B01J20/34 , B01J21/06 , B01J23/80 , C01B3/58 , C01B21/04 , C01B23/00 , B01D53/02
CPC分类号： B01J20/0244 , B01D53/02 , B01D2253/10 , B01D2257/502 , B01D2259/40086 , B01D2259/40088 , B01D2259/4009 , B01J20/0211 , B01J20/0237 , B01J20/06 , B01J20/3433 , B01J20/3458 , B01J20/3483 , B01J21/066 , B01J23/80 , B01J2220/42 , C01B3/58 , C01B21/0455 , C01B23/0057 , C01B2210/0034 , C01B2210/005
摘要： Carbon monoxide is removed from flows of material by means of adsorption to a adsorption mass containing copper, zinc, and zirconium.
摘要翻译：一氧化碳通过吸附到含有铜，锌和锆的吸附物质的材料流中被除去。

6. 发明授权

US07435285B2 Adsorption mass and method for removing carbon monoxide from flows of material 有权
标题翻译：吸附质量和从物料流中除去一氧化碳的方法
公开(公告)号：US07435285B2
公开(公告)日：2008-10-14
申请号：US10526677
申请日：2003-09-11
申请人： Henrik Junicke , Markus Holzle , Michael Bender
发明人： Henrik Junicke , Markus Holzle , Michael Bender
IPC分类号： B01D53/02
CPC分类号： B01J20/0244 , B01D53/02 , B01D2253/10 , B01D2257/502 , B01D2259/40086 , B01D2259/40088 , B01D2259/4009 , B01J20/0211 , B01J20/0237 , B01J20/06 , B01J20/3433 , B01J20/3458 , B01J20/3483 , B01J21/066 , B01J23/80 , B01J2220/42 , C01B3/58 , C01B21/0455 , C01B23/0057 , C01B2210/0034 , C01B2210/005
摘要： Carbon monoxide is removed from flows of material by means of adsorption to a adsorption mass containing copper, zinc, and zirconium.
摘要翻译：一氧化碳通过吸附到含有铜，锌和锆的吸附物质的材料流中被除去。

7. 发明授权

US07759530B2 Moulded catalyst bodies and method for hydrogenation of carbonyl compounds 有权
标题翻译：成型催化剂体和羰基化合物氢化方法
公开(公告)号：US07759530B2
公开(公告)日：2010-07-20
申请号：US11571766
申请日：2005-07-07
申请人： Christophe Houssin , Henrik Junicke , Andrea Haunert
发明人： Christophe Houssin , Henrik Junicke , Andrea Haunert
IPC分类号： B01J21/04 , B01J23/10 , B01J23/28 , B01J23/30 , B01J23/72
CPC分类号： B01J23/83 , B01J23/002 , B01J23/72 , B01J23/85 , B01J23/885 , B01J23/888 , B01J37/0009 , B01J37/03 , B01J2523/00 , C07C29/149 , Y10T428/2982 , C07C31/20 , B01J2523/17 , B01J2523/27 , B01J2523/31 , B01J2523/3706
摘要： The invention relates to a method for hydrogenation of an organic compound comprising at least one carbonyl group, whereby the organic compound is brought into contact with a moulded body in the presence of hydrogen. Said body may be produced by a method in which (i) an oxidic material is prepared, comprising copper oxide, aluminum oxide, and at least one oxide of lanthanum, tungsten, molybdenum, titanium, or zirconium, followed by (ii) addition of powdered metallic copper, copper platelets, powdered cement, graphite, mixtures or a mixture thereof with graphite to the oxidic material and (iii) moulding the mixture from (ii) to give a moulded body, characterised in that the moulded body is in the form of catalyst tablets or catalyst extrudates with a diameter d and/or height h
摘要翻译：本发明涉及一种包含至少一个羰基的有机化合物的氢化方法，其中有机化合物在氢气存在下与成型体接触。所述体可以通过以下方法制备，其中（i）制备氧化物材料，其包含氧化铜，氧化铝和至少一种镧，钨，钼，钛或锆的氧化物，然后加入（ⅱ）粉末状金属铜，铜片，粉末水泥，石墨，与石墨的混合物或其混合物与氧化物材料，（iii）从（ii）模塑混合物得到成型体，其特征在于成型体为具有直径d和/或高度h <2.5mm的催化剂片剂或催化剂挤出物，直径d <2.5mm的催化剂珠粒或具有泡孔直径rz <2.5mm的催化剂蜂窝体。

8. 发明申请

US20090030250A1 SELECTIVE HYDROGENATION CATALYST 有权
标题翻译：选择性氢化催化剂
公开(公告)号：US20090030250A1
公开(公告)日：2009-01-29
申请号：US11577140
申请日：2005-10-13
申请人： Thomas Hill , Hermann Petersen , Germain Kons , Henrik Junicke
发明人： Thomas Hill , Hermann Petersen , Germain Kons , Henrik Junicke
IPC分类号： C07C5/05 , B01J27/25
CPC分类号： B01J23/50 , B01J21/04 , B01J23/44 , B01J23/56 , B01J23/76 , B01J35/0006 , B01J35/006 , B01J35/0073 , B01J35/008 , B01J35/0093 , B01J35/1014 , B01J37/0201 , B01J37/08 , B01J37/16 , C07C7/163 , C07C7/167 , C10G45/34 , C10G45/40
摘要： A catalyst on an oxidic support and processes for selectively hydrogenating unsaturated compounds in hydrocarbon streams comprising them using these catalysts are described.
摘要翻译：描述了在氧化载体上的催化剂和使用这些催化剂选择性地氢化包含它们的烃流中的不饱和化合物的方法。

9. 发明授权

US07345172B2 Methods and compositions for detecting polynucleotide duplex damage and errors 有权
标题翻译：检测多核苷酸双链体损伤和错误的方法和组合物
公开(公告)号：US07345172B2
公开(公告)日：2008-03-18
申请号：US10974474
申请日：2004-10-26
申请人： Jacqueline K. Barton , Henrik Junicke
发明人： Jacqueline K. Barton , Henrik Junicke
IPC分类号： C07D242/36
CPC分类号： C07F15/008 , A61K41/0042 , A61K49/0017 , A61K49/0019 , C12Q1/6827 , C12Q1/6883 , C12Q2600/156 , C12Q2563/173
摘要： In accordance with the present invention there is provided a new class of sterically demanding metallo-intercalators. These compounds intercalate between bases in a duplex polynucleotide, but only where the bases are not fully complementary, for example, where there is a base-pair mismatch. The compounds are sufficiently sterically demanding that intercalation between bases in fully complementary duplexes does not occur to a significant degree. These mismatch intercalators are useful for detecting DNA and RNA defects, for diagnosing disorders characterized by the presence or increase in DNA and/or RNA defects, and for treating such disorders. Further, the compounds are capable of catalyzing photolytic cleavage of nucleic acids at relatively long wavelengths, and under normal sunlight.
摘要翻译：根据本发明，提供了一类新颖的空间要求的金属 - 嵌入剂。这些化合物插入双链多核苷酸的碱基之间，但是仅在碱不完全互补的情况下，例如，其中存在碱基对失配。化合物足够空间要求在完全互补双链体中的碱基之间的嵌入不会显着地发生。这些错配嵌入剂可用于检测DNA和RNA缺陷，用于诊断以DNA和/或RNA缺陷的存在或增加为特征的疾病，以及用于治疗这些疾病。此外，化合物能够在相对长的波长和正常的阳光下催化核酸的光解裂解。

10. 发明申请

US20070135650A1 Method for the production of defined mixtures of thf, bdo and gbl by gas phase hydrogenation 失效
公开(公告)号：US20070135650A1
公开(公告)日：2007-06-14
申请号：US10581074
申请日：2004-12-04
申请人： Markus Rosch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
发明人： Markus Rosch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
IPC分类号： C07D307/02
CPC分类号： C07D307/33 , C07D307/08
摘要： The present invention provides a process for variably preparing mixtures of optionally alkyl-substituted BDO, GBL and THF by two-stage hydrogenation in the gas phase of C4 dicarboxylic acids and/or derivatives thereof, which comprises a) in a first step in the gas phase, hydrogenating a gas stream of C4 dicarboxylic acids and/or derivatives thereof over a catalyst at a pressure of from 2 to 100 bar and a temperature of from 200° C. to 300° C. in a first reactor in the presence of a catalyst in the form of shaped catalyst bodies having a volume of less than 20 mm3, said catalyst from 5 to 95% by weight of oxide of copper and from 5 to 95% by weight of an oxide having acidic sites, to give a stream mainly containing of optionally alkyl-substituted GBL and THF, b) removing any succinic anhydride formed by partial condensation, c) converting the products remaining predominantly in the gas phase in the partial condensation, THF, water and GBL, under the same pressure or under a pressure reduced by the pressure drops in the hydrogenation circuit and at a temperature of from 150 to 240° C., in a second reactor over a catalyst which ≦95% by weight of CuO and from 5 to 95% by weight of one or more oxides selected from the group of ZnO, Al2O3, SiO2, TiO2, ZrO2, CeO2, MgO, CaO, SrO, BaO, La2O3 and Mn2O3 to give a stream comprising a mixture of BDO, GBL and THF, d) removing the hydrogen from the products and recycling it into the hydrogenation, e) distillatively separating the products, THF, BDO, GBL and water, if appropriate recycling a GBL-rich stream into the second reactor or if appropriate discharging it, and working up BDO, THF and GBL distillatively, and setting the ratio of the products, THF, GBL and BDO, relative to one another within the range from 10 to 100% by weight of THF, from 0 to 90% by weight of GBL and from 0 to 90% by weight of BDO only by varying the temperatures in the two hydrogenation zones and also if appropriate the GBL recycle stream.

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