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    • 5. 发明授权
    • Vertical, packed-bed, film evaporator for halide-free,
silicon-containing compounds
    • 立式,填充床,无卤化物,含硅化合物的薄膜蒸发器
    • US5558687A
    • 1996-09-24
    • US368319
    • 1994-12-30
    • Michael B. Cain
    • Michael B. Cain
    • G02B6/00B01D3/34C03B8/04C03B19/14C03B37/014C03B37/018C23C16/40C23C16/44C23C16/448B01F3/04
    • C23C16/4483B01D3/346C03B19/1415C03B37/01413C23C16/402C23C16/4481C03B2207/32C03B2207/85Y10S159/01Y10S159/32Y10S261/65
    • A vaporizer (film evaporator) (13) for halide-free, silicon-containing liquid reactants used in producing preforms is provided. The vaporizer includes a plurality of packed-bed columns (22) surrounding a central tube (24). A mixture of liquid reactant, e.g., octamethyl-cyclotetrasiloxane, and gas, e.g., oxygen, is sprayed onto the top surfaces (54) of the columns (22) by a set of spray nozzles (32). The liquid reactant and the gas flow downward together through the columns and are heated by hot oil (28) which flows around the columns' walls (50). The liquid reactant evaporates into the gas until the dew point temperature is reached, at which point all of the liquid reactant will have been converted into vapor. The vapor/gas mixture exits the bottom surfaces 56 of columns (22), where its direction of flow changes from downward to upward. This change in flow direction separates higher molecular weight species (46) from the vapor/gas mixture. The vapor/gas mixture leaves the vaporizer (13) through central tube (24) and is supplied to soot-producing burners (20) where it is used to produce preforms.
    • 提供了一种用于生产预制件的无卤素,含硅液体反应物的蒸发器(薄膜蒸发器)(13)。 蒸发器包括围绕中心管(24)的多个填充床柱(22)。 液体反应物,例如八甲基环四硅氧烷和气体(例如氧)的混合物通过一组喷嘴(32)喷射到塔(22)的顶表面(54)上。 液体反应物和气体一起通过柱体向下流动,并被围绕柱壁(50)流动的热油(28)加热。 液体反应物蒸发到气体中直至达到露点温度,此时所有液体反应物都将转化为蒸气。 蒸汽/气体混合物离开塔(22)的底表面56,其流动方向从下向上变化到上方。 流动方向的这种变化将较高分子量物质(46)与气/气混合物分离。 蒸汽/气体混合物通过中心管(24)离开蒸发器(13),并被供应到烟炱生产燃烧器(20),在那里用于生产预制件。
    • 8. 发明授权
    • Fiber optic coupler
    • 光纤耦合器
    • US5131735A
    • 1992-07-21
    • US670273
    • 1991-03-15
    • George E. BerkeyMichael B. CainKenneth T. Overman
    • George E. BerkeyMichael B. CainKenneth T. Overman
    • C03C25/00G02B6/28
    • G02B6/2835C03C25/00
    • A fiber optic coupler is formed by providing a glass tube having a longitudinal aperture extending therethrough. Glass optical fibers, each having a core, cladding and coating are disposed within the longitudinal aperture, the fibers extending beyond each end thereof. The coating is removed from that portion of the fibers in the midregion of the tube. The midregion of the tube is heated, collapsed about the fibers, and drawn to reduce the diameter thereof over a predetermined length. The fibers that are used in the process of making the coupler are initially provided with a coating that is too thin to provide good handleability and strength. However, the thin initial coating enables the use of a tube having a small aperture and thereby enhances the tube collapse step. After the coupler is formed, the fibers extending therefrom are overcoated. The process can be used to make other kinds of optical devices including integrated optical components.
    • 通过提供具有延伸穿过其中的纵向孔的玻璃管形成光纤耦合器。 每个具有芯,包层和涂层的玻璃光纤设置在纵向孔内,纤维延伸超出其每一端。 从管的中间部分的纤维部分去除涂层。 管的中间部分被加热,围绕纤维折叠,并被拉伸以将其直径减小预定长度。 在制造耦合器的过程中使用的纤维最初设置有太薄的涂层,以提供良好的可操作性和强度。 然而,薄的初始涂层使得能够使用具有小孔径的管,从而增强了管塌陷步骤。 在形成耦合器之后,从其延伸的纤维被覆盖。 该过程可用于制造其他类型的光学器件,包括集成的光学元件。