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    • 1. 发明授权
    • Paraffin alkylation
    • 石蜡烷基化
    • US07250542B2
    • 2007-07-31
    • US10793028
    • 2004-03-04
    • Lawrence A. Smith, Jr.Mitchell E. LoescherJohn R. AdamsAbraham P. Gelbein
    • Lawrence A. Smith, Jr.Mitchell E. LoescherJohn R. AdamsAbraham P. Gelbein
    • C07C6/00C07C2/58C07C2/62
    • C07C2/62C07C11/02C07C2527/054C10G29/205C10G2300/1081C10G2300/1088
    • A process for the alkylation of alkane with olefin or olefin precursor such as an oligomer of tertiary olefin comprising contacting a liquid system comprising acid catalyst, isoparaffin and olefin in concurrent downflow into contact in a reaction zone with a disperser mesh under conditions of temperature and pressure to react said isoparaffin and said olefin to produce an alkylate product is disclosed. Preferably, the liquid system is maintained at about its boiling point in the reaction zone. Unexpectedly, the olefin oligomers have been found to function as olefin precursors and not as olefins in the reaction. Thus, for example, a cold acid alkylation using an oligomer of isobutene (principally dimer and trimer) with isobutane produces isooctane with the isobutane reacting with the constituent isobutene units of the oligomers on a molar basis. The product isooctane is essentially the same as that produced in the conventional cold acid process.
    • 一种烷烃与烯烃或烯烃前体烷基化的方法,例如叔烯烃的低聚物,包括使含有酸催化剂,异链烷烃和烯烃的液体体系同时向下流动,在温度和压力条件下在分散网中与反应区接触 使所述异链烷烃和所述烯烃反应生成烷基化物产物。 优选地,液体系统保持在反应区域的大约沸点。 出乎意料地,已经发现烯烃低聚物作为烯烃前体而不是反应中的烯烃。 因此,例如,使用异丁烯(主要是二聚体和三聚体)的低聚物与异丁烷的冷酸烷基化产生异辛烷,异丁烷与摩尔的低聚物的组分异丁烯单元反应。 产物异辛烷基本上与常规冷酸法中产生的相同。
    • 4. 发明授权
    • Paraffin alkylation
    • 石蜡烷基化
    • US07319180B2
    • 2008-01-15
    • US10973746
    • 2004-10-26
    • Lawrence A. Smith, Jr.Mitchell E. LoescherJohn R. AdamsAbraham P. Gelbein
    • Lawrence A. Smith, Jr.Mitchell E. LoescherJohn R. AdamsAbraham P. Gelbein
    • C07C2/54
    • C07C2/62C07C11/02C07C2527/054C10G29/205C10G2300/1081C10G2300/1088
    • A process for the alkylation of alkane with olefin or olefin precursor such as an oligomer of tertiary olefin comprising contacting a liquid system comprising acid catalyst, isoparaffin and olefin in concurrent downflow into contact in a reaction zone with a disperser mesh under conditions of temperature and pressure to react said isoparaffin and said olefin to produce an alkylate product is disclosed. Preferably, the liquid system is maintained at about its boiling point in the reaction zone. Unexpectedly, the olefin oligomers have been found to function as olefin precursors and not as olefins in the reaction. Thus, for example, a cold acid alkylation using an oligomer of isobutene (principally dimer and trimer) with isobutane produces isooctane with the isobutane reacting with the constituent isobutene units of the oligomers on a molar basis. The product isooctane is essentially the same as that produced in the conventional cold acid process.
    • 一种烷烃与烯烃或烯烃前体烷基化的方法,例如叔烯烃的低聚物,包括使含有酸催化剂,异链烷烃和烯烃的液体体系同时向下流动,在温度和压力条件下在分散网中与反应区接触 使所述异链烷烃和所述烯烃反应生成烷基化物产物。 优选地,液体系统保持在反应区域的大约沸点。 出乎意料地,已经发现烯烃低聚物作为烯烃前体而不是反应中的烯烃。 因此,例如,使用异丁烯(主要是二聚体和三聚体)的低聚物与异丁烷的冷酸烷基化产生异辛烷,异丁烷与摩尔的低聚物的组分异丁烯单元反应。 产物异辛烷基本上与常规冷酸法中产生的相同。