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1. 发明授权

US07473777B2 Method for production of halogen-containing phthalocyanine compound 失效
标题翻译：含卤素酞菁化合物的生产方法
公开(公告)号：US07473777B2
公开(公告)日：2009-01-06
申请号：US11078070
申请日：2005-03-11
申请人： Kouichi Hirota , Yukihide Hashimoto , Kiyoshi Masuda , Masunori Kitao
发明人： Kouichi Hirota , Yukihide Hashimoto , Kiyoshi Masuda , Masunori Kitao
IPC分类号： C07B47/00
CPC分类号： C09B47/0671 , C09B47/067
摘要： This invention relates to a method for the production of a halogen-containing phthalocyaline compound by the cyclization of phthalonitrile compounds either singly or in combination with a metal compound, characterized in effecting the cyclization in an organic compound having a hydroxyl group and/or a carboxylic acid in an amount in the range of 0.01-10 mass parts per one mass part of the phthalonitrile compounds while continuing the introduction of an inert gas. This method, by using a solvent capable of serving as a specific oxygen source destined to participate in the reaction of complexing a metal compound introduced into a phthalocyanine dye, permits the production of a phthalocyanine compound inexpensively in a high yield.
摘要翻译：本发明涉及一种通过邻苯二甲腈化合物单独或与金属化合物环化来制备含卤素的邻苯二甲酸化合物的方法，其特征在于在具有羟基和/或羧基的有机化合物中进行环化酸的量为0.01-10质量份，每质量份邻苯二甲腈化合物，同时继续引入惰性气体。该方法通过使用能够作为特定氧源的溶剂参与将引入到酞菁染料中的金属化合物络合的反应，能够以高收率廉价地制造酞菁化合物。

2. 发明授权

US07238801B2 Phthalocyanine compound, method for production thereof, and near infrared absorbing dye and near infrared absorbing filter using same 有权
标题翻译：酞菁化合物，其制造方法和使用其的近红外吸收染料和近红外吸收滤光片
公开(公告)号：US07238801B2
公开(公告)日：2007-07-03
申请号：US10458349
申请日：2003-06-10
申请人： Kiyoshi Masuda , Masunori Kitao
发明人： Kiyoshi Masuda , Masunori Kitao
IPC分类号： C09B47/10 , C07D487/22 , F21V9/04
CPC分类号： C09B47/10 , C08K5/0041 , C09B47/22
摘要： A phthalocyanine compound (1) of a specific structure excelling in ability to absorb near infrared, ability to effect selective absorption of near infrared radiation particularly in a wavelength range exceeding 920 nm and falling short of 1050 nm, solubility in a solvent as well, compatibility with resin, and in such characteristic properties as heat resistance, light resistance, and weatherability, and a near infrared absorbing filter characterized by using the phthalocyanine compound (1) and phthalocyanine compound (2) having a maximum absorption wavelength at least in the range of 800–920 nm are provided. It enjoys a long service life and permits extensive use without selecting a substrate.
摘要翻译：具有吸收近红外能力优异的特殊结构的酞菁化合物（1），特别是在超过920nm的波长范围内并且低于1050nm的吸收近红外辐射的能力，在溶剂中的溶解度，兼容性具有耐热性，耐光性，耐气候性等特性的近红外线吸收滤光器，其特征在于，使用具有最大吸收波长的酞菁化合物（1）和酞菁化合物（2），所述酞菁化合物（1）和提供800-920纳米。它使用寿命长，允许广泛使用而不选择基材。

3. 发明授权

US07132465B2 Near-infrared absorbing coat film and near-infrared absorbing resin composition 失效
标题翻译：近红外吸收涂膜和近红外吸收树脂组合物
公开(公告)号：US07132465B2
公开(公告)日：2006-11-07
申请号：US10638430
申请日：2003-08-12
申请人： Takahiro Aoyama , Toshifumi Nishida , Nobuhisa Noda , Kiyoshi Masuda , Masunori Kitao
发明人： Takahiro Aoyama , Toshifumi Nishida , Nobuhisa Noda , Kiyoshi Masuda , Masunori Kitao
IPC分类号： C08K5/34 , C08K5/48
CPC分类号： G02B1/10 , G02B5/223
摘要： The present invention is directed to a near-infrared absorbing coat film comprising a near-infrared absorbing dye having a maximum absorption wavelength of 780 nm to 1200 nm, which has a residual near-infrared absorbing capacity of not less than 50% after 48 hours of light irradiation in an accelerated weathering test using a UV Auto Fade Meter.
摘要翻译：本发明涉及一种近红外吸收涂膜，其包含最大吸收波长为780nm至1200nm的近红外吸收染料，其在48小时后具有不小于50％的残留近红外吸收能力在使用UV自动衰落计的加速风化试验中的光照射。

4. 发明申请

US20050041281A1 Near-infrared absorbing coat film and near-infrared absorbing resin composition 失效
标题翻译：近红外吸收涂膜和近红外吸收树脂组合物
公开(公告)号：US20050041281A1
公开(公告)日：2005-02-24
申请号：US10638430
申请日：2003-08-12
申请人： Takahiro Aoyama , Toshifumi Nishida , Nobuhisa Noda , Kiyoshi Masuda , Masunori Kitao
发明人： Takahiro Aoyama , Toshifumi Nishida , Nobuhisa Noda , Kiyoshi Masuda , Masunori Kitao
IPC分类号： G02B1/10 , G02B5/22 , G02B13/14
CPC分类号： G02B1/10 , G02B5/223
摘要： The present invention is directed to a near-infrared absorbing coat film comprising a near-infrared absorbing dye having a maximum absorption wavelength of 780 nm to 1200 nm, which has a residual near-infrared absorbing capacity of not less than 50% after 48 hours of light irradiation in an accelerated weathering test using a UV Auto Fade Meter.
摘要翻译：本发明涉及一种近红外吸收涂膜，其包含最大吸收波长为780nm至1200nm的近红外吸收染料，其在48小时后具有不小于50％的残留近红外吸收能力在使用UV自动衰落仪的加速风化试验中的光照射。

5. 发明申请

US20050203293A1 Method for production of halogen-containing phthalocyanine compound 失效
标题翻译：含卤素酞菁化合物的生产方法
公开(公告)号：US20050203293A1
公开(公告)日：2005-09-15
申请号：US11078070
申请日：2005-03-11
申请人： Kouichi Hirota , Yukihide Hashimoto , Kiyoshi Masuda , Masunori Kitao
发明人： Kouichi Hirota , Yukihide Hashimoto , Kiyoshi Masuda , Masunori Kitao
IPC分类号： C09B47/067 , C09B47/04
CPC分类号： C09B47/0671 , C09B47/067
摘要： This invention relates to a method for for the production of a halogen-containing phthalocyaline compound by the cyclization of phthalonitrile compounds either singly or in combination with a metal compound, characterized in effecting the cyclization in an organic compound having a hydroxyl group and/or a carboxylic acid in an amount in the range of 0.01-10 mass parts per one mass part of the phthalonitrile compounds while continuing the introduction of an inert gas. This method, by using a solvent capable of serving as a specific oxygen source destined to participate in the reaction of complexing a metal compound introduced into a phthalocyanine dye, permits the production of a phthalocyanine compound inexpensively in a high yield.
摘要翻译：本发明涉及一种通过邻苯二甲腈化合物单独或与金属化合物环化来制备含卤素的邻苯二甲酸化合物的方法，其特征在于，在具有羟基的有机化合物和/或羧酸的量为0.01〜10质量份，每质量份邻苯二甲腈化合物，同时继续引入惰性气体。该方法通过使用能够作为特定氧源的溶剂参与将引入到酞菁染料中的金属化合物络合的反应，能够以高收率廉价地制造酞菁化合物。

6. 发明授权

US06323340B1 Phthalocyanine compound, method for production thereof, and near infrared absorption dye using the compound 有权
标题翻译：酞菁化合物，其制备方法和使用该化合物的近红外吸收染料
公开(公告)号：US06323340B1
公开(公告)日：2001-11-27
申请号：US09624637
申请日：2000-07-24
申请人： Kiyoshi Masuda , Masunori Kitao , Chie Tateyama
发明人： Kiyoshi Masuda , Masunori Kitao , Chie Tateyama
IPC分类号： C09B4704
CPC分类号： G11B7/248 , C09B47/063 , C09B47/22
摘要： A phthalocyanine compound is provided which exhibits particularly high transmittance to a visible ray, offers a highly efficient cut of a near infrared ray, excels in the ability to effect selective absorption in a near infrared region, excels in the solubility in a solvent, excels in the compatibility with a resin, and excels in heat resistance, light resistance, and weatherability, a method for the production thereof, a near infrared absorbable dye using the same, and a heat ray shielding material, a plasma display grade filter and a near infrared absorbable material formed thereof. The phthalocyanine compound of this invention is represented by the following formula (1): wherein Z2, Z3, Z6, Z7, Z10, Z11, Z14, and Z15 independently stand for SR1, OR2, or a halogen atom, provided that at least one of them stands for SR1 or OR2; Z1, Z4, Z5, Z5, Z9, Z12, Z13, and Z16 independently stand for NHR3, SR1, OR2, or a halogen atom, provided that at least one of them stands for NHR3 and at least four of them stand for OR2; a plurality of R1, R2, and R3, independently to each other, stand for a substituted or non-substituted phenyl group, a substituted or non-substituted aralkyl group, or a substituted or non-substituted alkyl group of 1 to 20 carbon atoms; and M stands for a nonmetal, a metal, a metal oxide, or a metal halide.
摘要翻译：提供了对可见光线具有特别高的透射率的酞菁化合物，提供近红外线的高效切割，在近红外区域中实现选择性吸收的能力优异，在溶剂中的溶解性优异与树脂的相容性，耐热性，耐光性和耐候性优异，其制造方法，使用该树脂的近红外可吸收染料，以及热射线屏蔽材料，等离子体显示级过滤器和近红外由其形成的可吸收材料。本发明的酞菁化合物由下式（1）表示：其中Z2，Z3，Z6，Z7，Z10，Z11，Z14和Z15独立地代表SR1，OR2或卤原子，条件是至少一个代表SR1或OR2; Z 1，Z 4，Z 5，Z 5，Z 9，Z 12，Z 13和Z 16独立地代表NHR 3，SR 1，OR 2或卤原子，条件是它们中至少有一个代表NHR 3，并且至少有四个代表OR2; 多个R1，R2和R3彼此独立地表示取代或未取代的苯基，取代或未取代的芳烷基或取代或未取代的碳原子数1〜20的烷基 ; M代表非金属，金属，金属氧化物或金属卤化物。

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