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1. 发明授权

US4985596A Process for producing substituted phenoxyethylamines oxime 失效
标题翻译：制备取代苯氧基乙胺肟的方法
公开(公告)号：US4985596A
公开(公告)日：1991-01-15
申请号：US397179
申请日：1989-08-21
申请人： Kikuo Ataka , Koji Imaoka , Kiyotaka Yoshii , Kenji Hirotsu
发明人： Kikuo Ataka , Koji Imaoka , Kiyotaka Yoshii , Kenji Hirotsu
IPC分类号： C07C249/08 , C07C213/02 , C07C249/04 , C07C251/38 , C07C251/40
CPC分类号： C07C213/02 , C07C249/04 , C07C251/38
摘要： A process for producing a substituted phenoxyacetaldehyde oxime of the formula: ##STR1## (wherein R.sup.1, R.sup.2 and R.sup.3 are as defined in the specification), which comprises reacting a substituted phenoxyacetaldehyde dialkylacetal of the formula: ##STR2## (wherein R.sup.1, R.sup.2, R.sup.3, R.sup.4 and R.sup.5 are as defined in the specification) with a hydroxylamine at a pH of from 0.1 to 1.0.

2. 发明授权

US5030755A Process for producing substituted phenoxyethylamines and intermediates 失效
标题翻译：制备取代苯氧基乙胺和中间体的方法
公开(公告)号：US5030755A
公开(公告)日：1991-07-09
申请号：US604757
申请日：1990-10-26
申请人： Kikuo Ataka , Koji Imaoka , Kiyotaka Yoshii , Kenji Hirotsu
发明人： Kikuo Ataka , Koji Imaoka , Kiyotaka Yoshii , Kenji Hirotsu
IPC分类号： C07C249/08 , C07C213/02 , C07C249/04 , C07C251/38 , C07C251/40
CPC分类号： C07C213/02 , C07C249/04 , C07C251/38
摘要： Disclosed are a process for producing a substituted phenoxyacetaldehyde oxime of the formula: ##STR1## (wherein R.sup.1, R.sup.2 and R.sup.3 are as defined in the specification), which comprises allowing a substituted phenoxyacetaldehyde dialkylacetal of the formula: ##STR2## (wherein R.sup.1, R.sup.2, R.sup.3, R.sup.4 and R.sup.5 are as defined in the specification) to react with hydroxylamine; a process for producing a substituted phenoxyethylamine of the formula: ##STR3## (wherein R.sup.1, R.sup.2 and R.sup.3 are as defined in the specification), which comprises reducing a substituted phenoxyacetaldehyde oxime of the formula (II) with hydrogen in the presence of a Raney-nickel catalyst; and a substituted phenoxyacetaldehyde oxime of the formula: ##STR4## (wherein R.sup.1, R.sup.2 and R.sup.6 are as defned in the specification).

3. 发明申请

US20100174098A1 3-ETHYLOXETHANE COMPOUND HAVING HYDROXYL GROUP AND METHOD FOR PRODUCING THE SAME 失效
标题翻译：具有羟基的3-乙基醚化合物及其制备方法
公开(公告)号：US20100174098A1
公开(公告)日：2010-07-08
申请号：US12303603
申请日：2007-06-05
申请人： Kenji Hirotsu , Tadashi Murakami
发明人： Kenji Hirotsu , Tadashi Murakami
IPC分类号： C07D305/06
CPC分类号： C07D305/06
摘要： Disclosed is a 3-ethyloxethane compound having a hydroxyl group which is represented by the following general formula (1). (1) (In the formula, A represents an alkylene group having 3-5 carbon atoms which may have an ether bond or an alkylene group having 3-5 carbon atoms which may be substituted by a hydroxyl group.) The 3-ethyloxethane compound having a hydroxyl group can be produced by reacting a 3-ethyloxethane compound represented by the general formula (2) below, a diol compound represented by the general formula (3) below and a base. (2) (In the formula, X represents a leaving group.) (3) (In the formula, A is as defined above.)
摘要翻译：公开了具有由以下通式（1）表示的羟基的3-乙氧基乙烷化合物。（1）（式中，A表示可具有醚键的3-5个碳原子的亚烷基或可被羟基取代的具有3-5个碳原子的亚烷基。）3-乙氧基乙烷化合物具有羟基的化合物可以通过下述通式（2）表示的3-乙基氧化乙烷化合物，下述通式（3）表示的二醇化合物和碱反应来制造。（2）（式中，X表示离去基团）（3）（式中，A如上定义）

4. 发明授权

US07745649B2 Processes for preparing tetrahydropyran-4-one and pyran-4-one 有权
标题翻译：制备四氢吡喃-4-酮和吡喃-4-酮的方法
公开(公告)号：US07745649B2
公开(公告)日：2010-06-29
申请号：US10583562
申请日：2004-12-17
申请人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Shinobu Suzuki
发明人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Shinobu Suzuki
IPC分类号： C07D309/30
CPC分类号： C07D309/38 , C07C45/00 , C07C49/185 , C07D309/30
摘要： The present invention relates to a process for preparing tetrahydropyran-4-one represented by the formula (1): which comprises reacting at least one kind of dihydropyran-4-one and pyran-4-one represented by the formula (2): wherein represents a single bond or a double bond, and hydrogen (a) in the presence of a metal catalyst, in a mixed solvent of an aprotic solvent and an alcohol solvent, or (b) in the presence of an anhydrous metal catalyst in which a hydrated metal catalyst is subjected to dehydration treatment, in a hydrophobic organic solvent.
摘要翻译：本发明涉及一种由式（1）表示的四氢吡喃-4-酮的制备方法：其包括使由式（2）表示的至少一种二氢吡喃-4-酮和吡喃-4-酮：其中表示单键或双键，氢（a）在金属催化剂的存在下，在非质子溶剂和醇溶剂的混合溶剂中，或（b）在无水金属催化剂存在下，其中水合金属催化剂在疏水性有机溶剂中进行脱水处理。

5. 发明授权

US07741497B2 Processes for preparing alkyl 3-(4-tetrahydropyranyl)-3-oxopropanoate compound and 4-acyltetrahydropyrane 失效
标题翻译：制备3-（4-四氢吡喃基）-3-氧代丙酸烷基酯化合物和4-酰基四氢吡喃的方法
公开(公告)号：US07741497B2
公开(公告)日：2010-06-22
申请号：US10583473
申请日：2004-12-17
申请人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Keiji Iwamoto , Takashi Harada
发明人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Keiji Iwamoto , Takashi Harada
IPC分类号： C07D309/06
CPC分类号： C07D309/06
摘要： The present invention is to provide a process for preparing an alkyl 3-(4-tetrahydropyranyl)-3-oxopropanoate compound represented by the formula (1): wherein R1 and R2 may be the same or different from each other, and represent a group which does not participate in the reaction, and R1 and R2 may be bonded to form a ring, and the ring may contain a hetero atom(s), and R3 represents a hydrocarbon group, which comprises reacting 4-acyltetrahydropyran represented by the formula (2): wherein R1 and R2 have the same meanings as defined above, and a carbonic acid diester represented by the formula (3): wherein R3 has the same meanings as defined above, and two R3s may be bonded to each other to form a ring, in the presence of a base, and a process for preparing 4-acyltetrahydropyran.
摘要翻译：本发明提供一种制备式（1）表示的3-（4-四氢吡喃基）-3-氧代丙酸烷基酯化合物的方法：其中R 1和R 2可以相同或不同，并且表示基团其不参与反应，并且R 1和R 2可以键合形成环，并且该环可以含有杂原子，并且R 3表示烃基，其包括使由式（Ⅳ）表示的4-酰基四氢吡喃与 2）：其中R1和R2具有与上述相同的含义，和由式（3）表示的碳酸二酯：其中R 3具有与上述相同的含义，并且两个R 3可以彼此键合形成在碱的存在下，以及制备4-酰基四氢吡喃的方法。

6. 发明申请

US20070078272A1 Processes for preparing tetrahydropyran-4-one and pyran-4-one 有权
标题翻译：制备四氢吡喃-4-酮和吡喃-4-酮的方法
公开(公告)号：US20070078272A1
公开(公告)日：2007-04-05
申请号：US10583562
申请日：2004-12-17
申请人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Shinobu Suzuki
发明人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Shinobu Suzuki
IPC分类号： C07D315/00
CPC分类号： C07D309/38 , C07C45/00 , C07C49/185 , C07D309/30
摘要： The present invention relates to a process for preparing tetrahydropyran-4-one represented by the formula (1): which comprises reacting at least one kind of dihydropyran-4-one and pyran-4-one represented by the formula (2): wherein represents a single bond or a double bond, and hydrogen (a) in the presence of a metal catalyst, in a mixed solvent of an aprotic solvent and an alcohol solvent, or (b) in the presence of an anhydrous metal catalyst in which a hydrated metal catalyst is subjected to dehydration treatment, in a hydrophobic organic solvent.
摘要翻译：本发明涉及一种由式（1）表示的四氢吡喃-4-酮的制备方法：其包括使由式（2）表示的至少一种二氢吡喃-4-酮和吡喃-4-酮：其中 “img id =”custom-character-00001“he =”3.13mm“wi =”6.35mm“file =”US20070078272A1-20070405-P00900.TIF“alt =”custom character“img-content =”character“img-format =“tif”/>表示单键或双键，氢（a）在金属催化剂存在下，在非质子溶剂和醇溶剂的混合溶剂中，或（b）在在疏水性有机溶剂中，将水合金属催化剂进行脱水处理的无水金属催化剂。

7. 发明授权

US07049458B2 Process for producing β-ketonitrile compound 有权
标题翻译：生产β-酮腈化合物的方法
公开(公告)号：US07049458B2
公开(公告)日：2006-05-23
申请号：US10451280
申请日：2001-12-25
申请人： Katsumasa Harada , Shigeyoshi Nishino , Kenji Hirotsu , Akira Nakamura , Takashi Harada
发明人： Katsumasa Harada , Shigeyoshi Nishino , Kenji Hirotsu , Akira Nakamura , Takashi Harada
IPC分类号： C07C255/03
CPC分类号： C07C253/30 , C07C2601/02 , C07C255/17 , C07C255/31
摘要： A process comprising reacting an aliphatic carboxylic ester compound with acetonitrile in the presence of a metal alkoxide to yield a metal salt of a β-ketonitrile compound, subsequently transferring the salt to an aqueous medium, and neutralizing the solution to obtain the β-ketonitrile compound in a free state, wherein a water-immisible organic solvent and water are added to the reaction mixture containing the β-ketonitrile compound metal salt yielded to transfer the metal salt to the water, the resultant aqueous solution of the β-ketonitrile compound metal salt is separated from the organic solvent by phase separation or another technique and then neutralized, and the resultant free β-ketonitrile compound is taken out by extraction with an organic solvent.
摘要翻译：一种方法，其包括在金属醇盐存在下使脂族羧酸酯化合物与乙腈反应，得到β-酮腈化合物的金属盐，随后将盐转移到水性介质中，并中和溶液以获得β-酮腈化合物在游离状态下，其中将水不溶性有机溶剂和水加入到含有将金属盐转移到水中的β-酮腈复合金属盐的反应混合物中，得到β-酮腈复合金属盐水溶液通过相分离或其它技术与有机溶剂分离，然后中和，所得游离β-酮腈化合物通过用有机溶剂萃取而取出。

8. 发明授权

US08901254B2 Process for preparing polycarbonate diol diacrylate and high-purity polycarbonate diol diacrylate 有权
标题翻译：制备聚碳酸酯二醇二丙烯酸酯和高纯度聚碳酸酯二醇二丙烯酸酯的方法
公开(公告)号：US08901254B2
公开(公告)日：2014-12-02
申请号：US13638550
申请日：2011-03-28
申请人： Youichi Yoshida , Yasuhito Yamamoto , Kenji Hirotsu
发明人： Youichi Yoshida , Yasuhito Yamamoto , Kenji Hirotsu
IPC分类号： C08F283/00 , C08G64/04 , C12P7/62 , C08G64/02 , C08G64/42 , C08F283/02
CPC分类号： C08G64/42 , C08G64/0291 , C08G64/045 , C12P7/62
摘要： This is to provide a process for preparing a polycarbonate diol diacrylate from a polycarbonate diol and a vinyl acrylate compound without using a protonic acid or a metal component.This is a process for preparing a polycarbonate diol diacrylate which comprises reacting a polycarbonate diol represented by the formula (I) and a vinyl acrylate compound represented by the formula (II) in the presence of a hydrolase, and a polycarbonate diol diacrylate represented by the formula (III) having a terminal acrylated ratio of 97% or more.
摘要翻译：这是提供从聚碳酸酯二醇和丙烯酸乙酯化合物制备聚碳酸酯二醇二丙烯酸酯而不使用质子酸或金属成分的方法。这是制备聚碳酸酯二醇二丙烯酸酯的方法，该方法包括使式（I）表示的聚碳酸酯二醇和由式（II）表示的丙烯酸乙酯化合物在水解酶的存在下反应，和由末端丙烯酸酯化率为97％以上的式（III）。

9. 发明授权

US08293448B2 Resin composition for stereolithography 有权
标题翻译：用于立体光刻的树脂组合物
公开(公告)号：US08293448B2
公开(公告)日：2012-10-23
申请号：US12304962
申请日：2007-06-15
申请人： Takashi Ito , Tsuneo Hagiwara , Kenji Hirotsu , Tadashi Murakami
发明人： Takashi Ito , Tsuneo Hagiwara , Kenji Hirotsu , Tadashi Murakami
IPC分类号： G03C9/00 , G03C5/00 , G03F7/00
CPC分类号： C08F2/50 , B33Y70/00 , C08G59/18 , C08L63/00 , G03F7/0037 , G03F7/038
摘要： Provided is a resin composition for stereolithography that absorbs little water and moisture over time in uncured state, maintains a low moisture absorption rate even under high humidity, and has high curing sensitivity, from which a stereolithography product excellent in the properties, such as dimensional accuracy, mechanical properties, and dimensional stability can be smoothly produced for reduced light irradiation time. The resin composition for stereolithography comprising an oxetane compound expressed by the general formula (I) below: wherein R1 denotes an alkyl group having 1 to 5 carbon atoms, and R2 denotes an alkylene group having 2 to 10 carbon atoms that may contain an ether bond, in the proportion of from 3 to 60 mass % based on the total mass of the resin composition for stereolithography.
摘要翻译：提供一种用于立体光刻的树脂组合物，其在未固化状态下随时间吸收几乎没有水分和水分，即使在高湿度下也保持低吸湿率，并且具有高固化灵敏度，由此可以获得诸如尺寸精度的性能优异的立体光刻产品，可以平滑地产生机械性能和尺寸稳定性，以减少光照射时间。用于立体光刻的树脂组合物，其包含由以下通式（I）表示的氧杂环丁烷化合物：其中R 1表示具有1至5个碳原子的烷基，R 2表示可含有醚键的具有2至10个碳原子的亚烷基，以用于立体光刻的树脂组合物的总质量为3〜60质量％的比例。

10. 发明授权

US07619084B2 Process for preparing 4-aminopyrimidine compound 失效
标题翻译： 4-氨基嘧啶化合物的制备方法
公开(公告)号：US07619084B2
公开(公告)日：2009-11-17
申请号：US11666510
申请日：2005-10-28
申请人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Takashi Harada
发明人： Shigeyoshi Nishino , Kenji Hirotsu , Hidetaka Shima , Takashi Harada
IPC分类号： C07D239/02
CPC分类号： C07D239/42
摘要： The present invention is to provide a process for preparing a 4-aminopyrimidine compound represented by the formula (3): wherein R1 and R2 each represent a hydrogen atom or group which does not participate in the reaction and which may have a substituent(s), and R1 and R2 may be bonded to each other to form a ring, and R4 represents a hydrogen atom or a hydrocarbon group, which comprises reacting ammonia, a 3-substituted or unsubstituted acrylonitrile compound represented by the formula (1): CR1(CN)═CR2Y (1) wherein R1 and R2 have the same meanings as defined above, and Y represents an amino group or OR, where R represents a hydrogen atom or a hydrocarbon group, and an organic acid compound represented by the formula (2): (R3O)3CR4 (2) wherein R3 represents a hydrocarbon group, and R4 has the same meaning as defined above.
摘要翻译：本发明提供一种制备式（3）表示的4-氨基嘧啶化合物的方法：其中R1和R2各自表示氢原子或不参与反应的基团，并且可以具有取代基， R 1和R 2可以彼此键合形成环，R 4表示氢原子或烃基，其包括使氨，3-取代或未取代的由式（1）表示的丙烯腈化合物：CR1（ CN）-CR2Y（1）其中R1和R2具有与上述相同的含义，Y表示氨基或OR，其中R表示氢原子或烃基，和由式（2）表示的有机酸化合物）：（R3O）3CR4（2）其中R3表示烃基，R4具有与上述相同的含义。

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