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1. 发明申请

US20090137822A1 Process for preparing 3-substituted thiophene 审中-公开
标题翻译：制备3-取代噻吩的方法
公开(公告)号：US20090137822A1
公开(公告)日：2009-05-28
申请号：US11920568
申请日：2006-05-16
申请人： Akio Matsushita , Kiyotaka Yoshii , Mizuho Oda , Masayoshi Oue , Shuji Yamada
发明人： Akio Matsushita , Kiyotaka Yoshii , Mizuho Oda , Masayoshi Oue , Shuji Yamada
IPC分类号： C07D333/38 , C07D333/22 , C07D333/16
CPC分类号： C07D333/38 , C07D333/22
摘要： The present invention relates to a process for preparing a 3-substituted thiophene represented by the formula (2): wherein R represents a cyano group, a formyl group, a carboxyl group, a hydrocarbyloxycarbonyl group which may have a substituent(s) or an acyl group which may have a substituent(s), which comprises reacting a vinyl compound represented by the formula (1): RCH═CHY (1) wherein R has the same meaning as defined above, and Y represents a leaving group, and an α-mercaptoacetaldehyde or a multimer thereof.
摘要翻译：本发明涉及一种由式（2）表示的3-取代噻吩的制备方法：其中R表示氰基，甲酰基，羧基，可具有取代基的烃氧基羰基或可以具有取代基的酰基，其包括使由式（1）表示的乙烯基化合物：<？in-line-formula description =“In-line formula”end =“lead”→RCH-CHY （1）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中R具有与上述相同的含义，Y表示离去基团，而α-巯基乙醛或多聚体其中。

2. 发明申请

US20070203336A1 Process for preparing dibenzothiazepine compounds 失效
标题翻译：二苯并硫氮杂化合物的制备方法
公开(公告)号：US20070203336A1
公开(公告)日：2007-08-30
申请号：US11708704
申请日：2007-02-21
申请人： Paul Murray , Luis-Manuel Vaz , Debra Ainge , Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
发明人： Paul Murray , Luis-Manuel Vaz , Debra Ainge , Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
IPC分类号： C07D281/12
CPC分类号： C07D281/18 , C07C319/18 , C07D281/16 , C07C323/62
摘要： A dibenzothiazepine compound is suitably prepared by subjecting a 2-amino-2′-carboxy-diphenylsulfide compound to dehydration-condensation reaction in the presence of an acidic catalyst; the 2-amino-2′-carboxy-diphenylsulfide compound is suitably prepared by reducing a 2-nitro-2′-carboxy-diphenylsulfide compound in a lower aliphatic ester solvent; and the 2-nitro-2′-carboxy-diphenylsulfide compound is suitably prepared by reacting a nitrobenzene compound with a thiosalicylic acid compound in a mixture of a lower aliphatic alcohol and water.
摘要翻译：二苯并硫氮杂化合物适宜地通过在酸性催化剂的存在下使2-氨基-2'-羧基 - 二苯硫醚化合物进行脱水缩合反应来制备; 2-氨基-2'-羧基二苯硫醚化合物通过在低级脂族酯溶剂中还原2-硝基-2'-羧基 - 二苯硫醚化合物来适当地制备; 2-硝基-2'-羧基二苯硫醚化合物可通过硝基苯化合物与硫代水杨酸化合物在低级脂族醇和水的混合物中反应来制备。

3. 发明申请

US20060173178A1 Process for preparing dibenzothiazepine derivatives 失效
标题翻译：二苯并硫氮杂衍生物的制备方法
公开(公告)号：US20060173178A1
公开(公告)日：2006-08-03
申请号：US11392577
申请日：2006-03-30
申请人： Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
发明人： Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
IPC分类号： C07D291/08
CPC分类号： C07D281/14 , C07C319/14 , C07C323/62 , C07D281/16
摘要： A process for preparing a dibenzothiazepine derivative such as dibenzo[b,f][1,4]thiazepin-11-one employable as a starting material for the preparation of 11-[4-(2-(2-hydroxyethoxy)ethyl)]-1-piperadinyldibenzothiazepine derivative which is known to be effective as an antipsychotic pharmaceutical, has the steps of reacting a nitrobenzene derivative with a thiosalicylic acid derivative, reducing the obtained 2-nitro-2′-carboxy-diphenylsulfide derivative, and subjecting the obtained 2-amino-2′-carboxy-diphenylsulfide derivative to dehydration-condensation reaction.
摘要翻译：制备二苯并氮杂吖庚因衍生物如二苯并[b，f] [1,4]硫杂吖庚因-11-酮的方法，其可用作制备11- [4-（2-（2-羟基乙氧基）乙基）] 已知有效作为抗精神病药物的1-哌嗪基二苯并硫氮杂衍生物具有使硝基苯衍生物与硫代水杨酸衍生物反应的步骤，将所得的2-硝基-2'-羧基二苯基硫醚衍生物还原， - 氨基-2'-羧基 - 二苯硫醚衍生物进行脱水缩合反应。

4. 发明授权

US4985596A Process for producing substituted phenoxyethylamines oxime 失效
标题翻译：制备取代苯氧基乙胺肟的方法
公开(公告)号：US4985596A
公开(公告)日：1991-01-15
申请号：US397179
申请日：1989-08-21
申请人： Kikuo Ataka , Koji Imaoka , Kiyotaka Yoshii , Kenji Hirotsu
发明人： Kikuo Ataka , Koji Imaoka , Kiyotaka Yoshii , Kenji Hirotsu
IPC分类号： C07C249/08 , C07C213/02 , C07C249/04 , C07C251/38 , C07C251/40
CPC分类号： C07C213/02 , C07C249/04 , C07C251/38
摘要： A process for producing a substituted phenoxyacetaldehyde oxime of the formula: ##STR1## (wherein R.sup.1, R.sup.2 and R.sup.3 are as defined in the specification), which comprises reacting a substituted phenoxyacetaldehyde dialkylacetal of the formula: ##STR2## (wherein R.sup.1, R.sup.2, R.sup.3, R.sup.4 and R.sup.5 are as defined in the specification) with a hydroxylamine at a pH of from 0.1 to 1.0.

5. 发明授权

US07671195B2 Process for preparing dibenzothiazepine compounds 失效
标题翻译：二苯并硫氮杂化合物的制备方法
公开(公告)号：US07671195B2
公开(公告)日：2010-03-02
申请号：US11708704
申请日：2007-02-21
申请人： Paul Michael Murray , Luis-Manuel Vaz , Debra Ainge , Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
发明人： Paul Michael Murray , Luis-Manuel Vaz , Debra Ainge , Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
IPC分类号： C07D281/18
CPC分类号： C07D281/18 , C07C319/18 , C07D281/16 , C07C323/62
摘要： A dibenzothiazepine compound is suitably prepared by subjecting a 2-amino-2′-carboxy-diphenylsulfide compound to dehydration-condensation reaction in the presence of an acidic catalyst; the 2-amino-2′-carboxy-diphenylsulfide compound is suitably prepared by reducing a 2-nitro-2′-carboxy-diphenylsulfide compound in a lower aliphatic ester solvent; and the 2-nitro-2′-carboxy-diphenylsulfide compound is suitably prepared by reacting a nitrobenzene compound with a thiosalicylic acid compound in a mixture of a lower aliphatic alcohol and water.
摘要翻译：二苯并硫氮杂化合物适宜地通过在酸性催化剂的存在下使2-氨基-2'-羧基 - 二苯硫醚化合物进行脱水缩合反应来制备; 2-氨基-2'-羧基二苯硫醚化合物通过在低级脂族酯溶剂中还原2-硝基-2'-羧基 - 二苯硫醚化合物来适当地制备; 2-硝基-2'-羧基二苯硫醚化合物可通过硝基苯化合物与硫代水杨酸化合物在低级脂族醇和水的混合物中反应来制备。

6. 发明授权

US07314930B2 Process for preparing dibenzothiazepine derivatives 失效
标题翻译：二苯并硫氮杂衍生物的制备方法
公开(公告)号：US07314930B2
公开(公告)日：2008-01-01
申请号：US11392577
申请日：2006-03-30
申请人： Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
发明人： Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
IPC分类号： C07D291/08
CPC分类号： C07D281/14 , C07C319/14 , C07C323/62 , C07D281/16
摘要： A process for preparing a dibenzothiazepine derivative such as dibenzo[b,f][1,4]thiazepin-11-one employable as a starting material for the preparation of 11-[4-(2-(2-hydroxyethoxy)ethyl)]-1-piperadinyldibenzothiazepine derivative which is known to be effective as an antipsychotic pharmaceutical, has the steps of reacting a nitrobenzene derivative with a thiosalicylic acid derivative, reducing the obtained 2-nitro-2′-carboxy-diphenylsulfide derivative, and subjecting the obtained 2-amino-2′-carboxy-diphenylsulfide derivative to dehydration-condensation reaction.
摘要翻译：制备二苯并氮杂吖庚因衍生物如二苯并[b，f] [1,4]硫杂吖庚因-11-酮的方法，其可用作制备11- [4-（2-（2-羟基乙氧基）乙基）] 已知有效作为抗精神病药物的1-哌嗪基二苯并硫氮杂衍生物具有使硝基苯衍生物与硫代水杨酸衍生物反应的步骤，将所得的2-硝基-2'-羧基二苯基硫醚衍生物还原， - 氨基-2'-羧基 - 二苯硫醚衍生物进行脱水缩合反应。

7. 发明授权

US07045621B1 Process for producing dibenzothiazepine derivatives 失效
标题翻译：二苯并硫氮杂衍生物的制备方法
公开(公告)号：US07045621B1
公开(公告)日：2006-05-16
申请号：US10030251
申请日：1999-07-09
申请人： Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
发明人： Katsumasa Harada , Shigeyoshi Nishino , Kiyotaka Yoshii
IPC分类号： C07D281/16
CPC分类号： C07D281/14 , C07C319/14 , C07C323/62 , C07D281/16
摘要： A process for preparing a dibenzothiazepine derivative such as dibenzo[b,f] [1,4]thiazepin-11-one employable as a starting material for the preparation of 11-[4-(2-(2-hydroxyethoxy)ethyl)]-1-piperadinyldibenzothiazepine derivative which is known to be effective as an antipsychotic pharmaceutical, has the steps of reacting a nitrobenzene derivative with a thiosalicylic acid derivative, reducing the obtained 2-nitro-2′-carboxy-diphenylsulfide derivative, and subjecting the obtained 2-amino-2′-carboxy-diphenylsulfide derivative to dehydration-condensation reaction.
摘要翻译：制备二苯并氮杂吖庚因衍生物如二苯并[b，f] [1,4]硫杂吖庚因-11-酮的方法，其可用作制备11- [4-（2-（2-羟基乙氧基）乙基）] 已知有效作为抗精神病药物的1-哌嗪基二苯并硫氮杂衍生物具有使硝基苯衍生物与硫代水杨酸衍生物反应的步骤，将所得的2-硝基-2'-羧基二苯基硫醚衍生物还原， - 氨基-2'-羧基 - 二苯硫醚衍生物进行脱水缩合反应。

8. 发明授权

US09334211B2 Hydrocracking catalyst, method for producing same, and method for producing hydroxy compound using said catalyst 有权
标题翻译：加氢裂化催化剂及其制造方法以及使用该催化剂制造羟基化合物的方法
公开(公告)号：US09334211B2
公开(公告)日：2016-05-10
申请号：US14239863
申请日：2012-08-22
申请人： Kiyotaka Yoshii , Atsushi Yamada
发明人： Kiyotaka Yoshii , Atsushi Yamada
IPC分类号： C07C29/10 , C10G47/10 , C10G47/04 , C07C29/132 , B01J37/10 , B01J23/46 , B01J23/652 , B01J23/89 , B01J23/68 , B01J23/656
CPC分类号： C07C29/103 , B01J23/464 , B01J23/468 , B01J23/6525 , B01J23/6527 , B01J23/6567 , B01J23/688 , B01J23/8986 , B01J37/10 , C07C29/132 , C10G47/04 , C10G47/10 , C07C31/20
摘要： The present invention provides a hydrocracking catalyst obtainable by mixing a metal compound (A) including any one metal of Groups 3 to 11 of the Periodic Table, a compound (B) including at least one compound selected from the group consisting of a ruthenium oxide compound (B1) and a high-valence compound (B2) including any metal of Groups 8 to 11 of the Periodic Table, and a metal oxide (C) including a metal of Group 5, Group 6 or Group 7 of the Periodic Table, and conducting reduction treatment.
摘要翻译：本发明提供一种加氢裂化催化剂，其通过将包含元素周期表第3〜11族的金属化合物（A），包含至少一种选自氧化钌化合物（B1）和包含元素周期表第8〜11族金属的高价化合物（B2）和包含元素周期表第5族，第6族或第7族金属的金属氧化物（C），以及进行还原处理。

9. 发明授权

US07665290B2 Twister, method for producing twisted wire, ply, and pneumatic tire 失效
标题翻译：捻线机，捻线，帘布层和充气轮胎的生产方法
公开(公告)号：US07665290B2
公开(公告)日：2010-02-23
申请号：US10536446
申请日：2003-11-25
申请人： Shogo Ueda , Yoshiki Mizuta , Kojiro Torisu , Kiyotaka Yoshii
发明人： Shogo Ueda , Yoshiki Mizuta , Kojiro Torisu , Kiyotaka Yoshii
IPC分类号： D07B1/00
CPC分类号： D07B3/00 , B21F15/04 , D07B3/12 , D07B7/02
摘要： A compact twister and a method for producing a twisted wire that can efficiently produce a short twisted wire that satisfies performance requirements, as well as a ply and a pneumatic tire twisted using the twister or the method for producing a twisted wire, are provided. The twister includes a rotating body for twisting plural filament wires that are fed thereto to form a cord and for applying a feeding force to the cord. The rotating body includes a feeding mechanism within a housing, and the cord is discharged from the rotating body by the feeding mechanism. The twister carries out twisting operation with one of a cord side of a twisting point or a filament wire side of the twisting point being free. Thus, a compact twister, that can form a cord with excellent rotating property and straightness, is accomplished.
摘要翻译：提供了一种紧凑型扭绞机和一种能够有效地生产满足性能要求的短绞线的双绞线的制造方法，以及使用该捻线器或双绞线的制造方法的层叠和充气轮胎。捻线器包括用于扭转多个细丝线的旋转体，所述丝线被馈送到其中以形成绳索并且用于向绳索施加进给力。旋转体包括在壳体内的进给机构，并且绳索通过进给机构从旋转体排出。捻线机在扭转点的绳索侧或扭转点的丝线侧之一处进行扭转操作。因此，可以实现能够形成具有优异的旋转性能和直线度的帘线的紧凑型捻线机。

10. 发明申请

US20140288335A1 HYDROCRACKING CATALYST, METHOD FOR PRODUCING SAME, AND METHOD FOR PRODUCING HYDROXY COMPOUND USING SAID CATALYST 有权
标题翻译：水解反应催化剂，其生产方法和使用催化剂生产羟基化合物的方法
公开(公告)号：US20140288335A1
公开(公告)日：2014-09-25
申请号：US14239863
申请日：2012-08-22
申请人： Kiyotaka Yoshii , Atsushi Yamada
发明人： Kiyotaka Yoshii , Atsushi Yamada
IPC分类号： C07C29/10 , B01J23/46 , B01J23/656 , B01J23/652 , B01J23/89 , B01J23/68
CPC分类号： C07C29/103 , B01J23/464 , B01J23/468 , B01J23/6525 , B01J23/6527 , B01J23/6567 , B01J23/688 , B01J23/8986 , B01J37/10 , C07C29/132 , C10G47/04 , C10G47/10 , C07C31/20
摘要： The present invention provides a hydrocracking catalyst obtainable by mixing a metal compound (A) including any one metal of Groups 3 to 11 of the Periodic Table, a compound (B) including at least one compound selected from the group consisting of a ruthenium oxide compound (B1) and a high-valence compound (B2) including any metal of Groups 8 to 11 of the Periodic Table, and a metal oxide (C) including a metal of Group 5, Group 6 or Group 7 of the Periodic Table, and conducting reduction treatment.
摘要翻译：本发明提供一种加氢裂化催化剂，其通过将包含元素周期表第3〜11族的金属化合物（A），包含至少一种选自氧化钌化合物（B1）和包含元素周期表第8〜11族金属的高价化合物（B2）和包含元素周期表第5族，第6族或第7族金属的金属氧化物（C），以及进行还原处理。

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