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1. 发明申请

US20100089204A1 Process for Producing Ti and Apparatus Therefor 审中-公开
标题翻译：生产钛的方法及其设备
公开(公告)号：US20100089204A1
公开(公告)日：2010-04-15
申请号：US11992162
申请日：2006-08-22
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Toru Uenishi , Masahiko Hori , Kazuo Takemura , Katsunori Dakeshita
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Toru Uenishi , Masahiko Hori , Kazuo Takemura , Katsunori Dakeshita
IPC分类号： C22B34/12
CPC分类号： C25C3/28 , C22B34/1272 , C22B34/129 , C22B34/1295 , C25C3/02 , C25C7/005 , C25C7/06
摘要： A process for producing Ti, comprising a reduction step of reacting TiCl4 with Ca in a CaCl2-containing molten salt having the Ca dissolved therein to thereby form Ti particles, a separation step of separating the Ti particles formed in said molten salt from said molten salt and an electrolysis step of electrolyzing the molten salt so as to increase the Ca concentration, wherein the molten salt increased in Ca concentration in the electrolysis step is introduced into a regulating cell to thereby render the Ca concentration of the molten salt constant and thereafter the molten salt is used for the reduction of TiCl4 in the reduction step. In the present invention, the Ca concentration of the molten salt to be fed to the corresponding reduction vessel can be inhibited from fluctuating and, at the same time, can maintain high concentration levels. Further, a large volume of the molten salt can be treated continuously. Therefore, the reduction reaction of TiCl4 can be efficiently performed, and the process can be effectively utilized in the production of Ti by Ca reduction as a production process for realizing Ti production on an industrial scale.
摘要翻译：一种制备Ti的方法，包括在溶解有Ca的含CaCl 2的熔融盐中使TiCl4与Ca反应从而形成Ti颗粒的还原步骤，将在所述熔融盐中形成的Ti颗粒与所述熔融盐分离的分离步骤以及电解电解步骤，电解所述熔融盐以增加所述Ca浓度，其中将所述电解步骤中的Ca浓度升高的所述熔融盐引入调节池中，从而使所述熔融盐的Ca浓度恒定，盐在还原步骤中用于还原TiCl4。在本发明中，可以抑制供给到相应的还原容器的熔融盐的Ca浓度的波动，同时可以保持高浓度水平。此外，可以连续地处理大量的熔融盐。因此，可以有效地进行TiCl 4的还原反应，并且通过Ca还原可以有效地利用Ti的制造，作为实现工业规模的Ti生产的制造方法。

2. 发明申请

US20090101517A1 Method for Producing Ti or Ti Alloy, and Pulling Electrolysis Method Applicable Thereto 审中-公开
标题翻译：生产Ti或Ti合金的方法，以及拉拔电解方法
公开(公告)号：US20090101517A1
公开(公告)日：2009-04-23
申请号：US11887511
申请日：2006-03-16
申请人： Kazuo Takemura , Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori
发明人： Kazuo Takemura , Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori
IPC分类号： C25C1/24 , C25C1/06
CPC分类号： C25C3/28 , C22B5/04 , C22B34/1268 , C22B34/129 , C25C3/02 , C25C3/26 , C25C5/04 , C25C7/00
摘要： In producing Ti or a Ti alloy through reduction by Ca, an electrolytic-bath salt taken out from a reduction process is electrolyzed to recover Ca and the electrolytic-bath salt as a solid substance, and the recovered Ca and electrolytic-bath salt are delivered to the reduction process. Therefore, heat generation is suppressed in the reduction process by utilizing latent heat of fusion possessed by the solid substance, thereby largely improving production efficiency and thermal efficiency. Additionally, a reaction temperature is easily controlled, and a raw-material loading rate can be enhanced to efficiently produce Ti or the Ti alloy. At this point, using a pulling electrolysis method of the invention, the solid-state Ca and electrolytic-bath salt can be obtained at a low voltage and high current efficiency, i.e., with the relatively small power consumption. When the solid-state Ca and electrolytic-bath salt is used as a Ca source in producing Ti or the Ti alloy through reduction by Ca, the Ti or Ti alloy can efficiently be produced.
摘要翻译：在通过Ca还原生产Ti或Ti合金时，从还原过程中取出的电解浴盐被电解以回收Ca和作为固体物质的电解浴盐，并且回收的Ca和电解浴盐被输送到减少过程。因此，通过利用固体物质所具有的熔解潜热，在还原过程中抑制发热，从而大大提高生产效率和热效率。另外，可以容易地控制反应温度，并且可以提高原料负载率，以有效地生产Ti或Ti合金。此时，使用本发明的拉电解法，可以以低电压和高电流效率即功耗相对较小获得固态Ca和电解浴盐。当使用固态Ca和电解浴盐作为通过Ca还原生产Ti或Ti合金的Ca源时，可以有效地制备Ti或Ti合金。

3. 发明申请

US20070131057A1 Method for producing ti or ti alloy through reduction by ca 审中-公开
标题翻译：通过还原制备钛或钛合金的方法
公开(公告)号：US20070131057A1
公开(公告)日：2007-06-14
申请号：US10575224
申请日：2004-10-06
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Yuko Urasaki , Kazuo Takemura
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Yuko Urasaki , Kazuo Takemura
IPC分类号： B22F9/24
CPC分类号： C25C3/28 , C22B34/1272 , C22B34/1295 , C25C3/02
摘要： A method for producing Ti or Ti alloys through reduction by Ca, including: a reduction step of holding a molten salt, containing CaCl2 and having Ca dissolved therein, in a reactor vessel 1, and reacting a metallic chloride containing TiCl4 with Ca in said salt to generate particles of Ti or Ti alloys in said salt; and a separation step of separating particles of Ti or Ti alloys, generated in said salt, from said salt. An electrolysis step 8, in which CaCl2 discharged outside the reactor vessel 1 is electrolyzed into Ca and Cl2, and the generated Ca is used for the generation reaction of Ti or Ti alloys in the reactor vessel 1, is preferably added. In the electrolysis step 8, an alloy electrode made of a molten Ca alloy, if applied for a cathode, is effective in enhancing the electricity efficiency, and also can be effectively utilized as a carrier medium of Ca for raising a Ca concentration of molten salt. By this method, high-purity Ti metals can be efficiently and economically produced.
摘要翻译：一种通过Ca还原制造Ti或Ti合金的方法，包括：将含有CaCl 2·Ca和Ca的溶解在其中的熔融盐保持在反应容器1中的还原步骤，并使金属在所述盐中含有TiCl 4 Si与Ca的氯化物，以在所述盐中产生Ti或Ti合金颗粒; 以及分离步骤，从所述盐分离在所述盐中产生的Ti或Ti合金的颗粒。电解步骤8，其中排放到反应容器1外部的CaCl 2电解为Ca和Cl 2，并且所产生的Ca用于Ti或优选添加反应器容器1中的Ti合金。在电解工序8中，如果用于阴极，则由熔融的Ca合金构成的合金电极，对于提高电效率是有效的，也可以有效地利用Ca作为提高熔融盐的Ca浓度的载体介质。通过这种方法，可以高效且经济地生产高纯度Ti金属。

4. 发明申请

US20070295167A1 Method for Producing Ti or Ti Alloy Through Reduction by Ca 审中-公开
标题翻译：通过Ca还原生产Ti或Ti合金的方法
公开(公告)号：US20070295167A1
公开(公告)日：2007-12-27
申请号：US10590863
申请日：2004-10-13
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Kazuo Takemura
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Kazuo Takemura
IPC分类号： C22B34/12 , C25C3/28
CPC分类号： C22B34/1272 , C22B5/04 , C22B34/129 , C22B34/1295 , Y02P10/212
摘要： A mixed molten salt containing CaCl2 and NaCl is held in the reactor cell 1 at a temperature not more than 600° C. TiCl4 which is of a Ti raw material is introduced into the reactor cell 1 while Na is introduced into the reactor cell 1. Na introduced into the reactor cell 1 is replaced by Ca, Ca is dissolved in the molten salt, Ca reduces TiCl4 introduced into the reactor cell 1, and thereby Ti particles are generated. The generated Ti particles are introduced to a separation cell 2 along with the molten salt, and the Ti particles and Na are separated from the molten salt. The residual molten salt is introduced to an electrolytic cell 3 to generate Na by high-temperature electrolysis at the temperature more than 600° C. The generated Na is returned to the reactor cell 1 to replenish Na consumed in the reactor cell 1. The highly reactive Ca is not directly handled, and Na which is easy to handle is used in a circulating manner. Therefore, the Ti or Ti alloy can economically be produced by Ca reduction.
摘要翻译：将含有CaCl 2 N 2和NaCl的混合熔融盐在不高于600℃的温度下保持在反应器电池1中。Ti原料的TiCl 4为引入反应器电池1中，同时将Na引入反应器电池1中。引入反应器电池1的Na被Ca替代，Ca溶解在熔融盐中，Ca使引入反应器电池1的TiCl 4导致，从而产生Ti颗粒。所产生的Ti颗粒与熔融盐一起被引入分离池2中，并将Ti颗粒和Na与熔融盐分离。将残留的熔融盐引入电解槽3中，通过在600℃以上的高温下进行高温电解而生成Na。将所生成的Na返回到反应器电池1，补充反应器电池1中消耗的Na。高反应性Ca不能直接处理，易于处理的Na以循环方式使用。因此，Ti或Ti合金可经济地通过Ca还原产生。

5. 发明申请

US20090152122A1 Method for electrolyzing molten salt, electrolytic cell, and process for producing ti using said method 审中-公开
标题翻译：使用所述方法电解熔融盐，电解池和制造方法的方法
公开(公告)号：US20090152122A1
公开(公告)日：2009-06-18
申请号：US11991072
申请日：2006-08-22
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Toru Uenishi , Masahiko Hori , Kazuo Takemura , Katsunori Dakeshita
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Toru Uenishi , Masahiko Hori , Kazuo Takemura , Katsunori Dakeshita
IPC分类号： C25B1/26 , C25B9/00 , C25C3/28
CPC分类号： C22B34/129 , C22B5/04 , C22B34/1268 , C25C3/02 , C25C7/005
摘要： The present invention provides a method for electrolyzing molten salt that can enhance the concentration of metal-fog forming metal in the molten salt by carrying out the electrolysis under conditions that the molten salt containing the chloride of metal-fog forming metal is supplied from one end of an electrolytic cell to a space between an anode and a cathode in a continuous or intermittent manner to provide a flow rate in one direction to the molten salt in the vicinity of the surface of the cathode and thus to allow the molten salt to flow in one direction in the vicinity of the surface of the cathode. According to the present invention, while high current efficiency is maintained, only the molten salt enriched with metal-fog forming metal such as Ca can be effectively taken out. Further, this method can easily be carried out by using the electrolytic cell according to the present invention. Furthermore, the application of the method for electrolyzing molten salt according to the present invention to the production of Ti by Ca reduction can realize the production of metallic Ti with high efficiency. Thus, the method for electrolyzing molten salt, the electrolytic cell, and the process for producing Ti, each according to the present invention, can be effectively utilized in the production of Ti by Ca reduction.
摘要翻译：本发明提供了一种电解熔融盐的方法，该方法可以通过在从一端供给含有金属雾形成金属的氯化物的熔融盐的条件下进行电解，从而提高熔融盐中金属雾形成金属的浓度的电解池以连续或间歇的方式连接到阳极和阴极之间的空间，以在阴极表面附近向熔融盐提供沿一个方向的流速，从而允许熔融盐流入在阴极表面附近的一个方向。根据本发明，在保持高电流效率的同时，仅有效地除去富含金属雾形成金属如Ca的熔盐。此外，该方法可以通过使用根据本发明的电解槽容易地进行。另外，通过将本发明的熔盐电解方法应用于通过Ca还原生产Ti，可以实现高效率地生产金属Ti。因此，根据本发明的电解熔融盐，电解槽和制造Ti的方法的方法可以有效地用于通过Ca还原生产Ti。

6. 发明申请

US20130071752A1 NEGATIVE-ELECTRODE MATERIAL POWDER FOR LITHIUM-ION SECONDARY BATTERY AND METHOD FOR PRODUCING SAME 审中-公开
标题翻译：用于锂离子二次电池的负极电极材料粉末及其制造方法
公开(公告)号：US20130071752A1
公开(公告)日：2013-03-21
申请号：US13699793
申请日：2011-04-27
申请人： Hideaki Kanno , Shinji Shimosaki , Kazuo Takemura
发明人： Hideaki Kanno , Shinji Shimosaki , Kazuo Takemura
IPC分类号： H01M4/48 , H01M4/583
CPC分类号： H01M4/485 , C01B33/021 , C01B33/12 , C01B33/18 , C01P2004/60 , H01M4/134 , H01M4/1395 , H01M4/366 , H01M4/386 , H01M4/625 , H01M10/052 , H01M2004/027
摘要： Provided is a negative-electrode material powder for lithium-ion secondary battery including a silicon-rich layer on the surface of a lower silicon oxide powder, and a negative-electrode material powder for said battery comprising a silicon oxide powder, characterized by satisfying c/d
摘要翻译：本发明提供一种锂二次电池用负极材料粉末，其包含在下部氧化硅粉末的表面上的富硅层，以及包含氧化硅粉末的所述电池用负极材料粉末，其特征在于，满足c / d <1，其中c是氧化硅粉末表面上的氧与硅的摩尔比，d是其整个部分的摩尔比。优选满足c <1和0.8

7. 发明授权

US06770312B1 Frozen foods and process for producing the same 失效
标题翻译：冷冻食品和生产过程
公开(公告)号：US06770312B1
公开(公告)日：2004-08-03
申请号：US09806157
申请日：2001-03-28
申请人： Tatsuya Yamamoto , Katsumi Matsuzaki , Kensuke Furuyama , Toshifumi Andou , Kazuo Takemura , Akira Tamegai
发明人： Tatsuya Yamamoto , Katsumi Matsuzaki , Kensuke Furuyama , Toshifumi Andou , Kazuo Takemura , Akira Tamegai
IPC分类号： A23B410
CPC分类号： A23B9/14 , A23B9/10 , A23L3/36 , A23L7/111 , A23L7/1963 , A23P20/11 , A23P20/12 , A23P20/17
摘要： The frozen food product according to the present invention contains as a major ingredient boiled rice grains or boiled pasta pieces; a water migration-preventing layer formed on the surface of each rice grain or boiled pasta; and a sauce layer formed on the surface of the water migration-preventing layer, and the product is frozen in such a state. In the frozen food product described above, rice grains or pasta pieces contained as the major ingredient are mixed homogeneously with a sauce, and if the frozen food is packaged portionwise, the resulting packaged products can give stable quality where the major ingredient and the sauce are blended at a constant rate. This frozen food product can be manufactured by carrying out a step of admixing a primary sauce to the major ingredient so as to form a water migration-preventing layer; a step of freezing the thus treated major ingredient; a step of admixing a secondary sauce to the resulting major ingredient; and a step of freezing the resulting major ingredient.
摘要翻译：根据本发明的冷冻食品包含煮米饭或煮熟的面食片的主要成分; 在每个米粒或煮熟的面食的表面上形成防水层; 以及形成在防水层的表面上的酱汁层，并且在这种状态下将产品冷冻。在上述冷冻食品中，作为主要成分的米粒或面食片与酱料均匀混合，如果冷冻食品分批包装，则所得到的包装产品可以提供稳定的质量，其中主要成分和酱料为以恒定速率混合。该冷冻食品可以通过对主要成分进行混合以形成防水层的步骤来制造。冻结如此处理的主要成分的步骤; 将二次酱料与所得主要成分混合的步骤; 和冷冻所得主要成分的步骤。

8. 发明授权

US5114760A Method for manufacturing layer-built material with silicon dioxide film containing organic colorant and the layer-built material manufactured thereby 失效
标题翻译：包含有机颜料的二氧化硅膜和制造的层状材料制备层状材料的方法
公开(公告)号：US5114760A
公开(公告)日：1992-05-19
申请号：US500987
申请日：1990-03-29
申请人： Kazuo Takemura , Juichi Ino , Hideo Kawahara , Masaki Kitaoka
发明人： Kazuo Takemura , Juichi Ino , Hideo Kawahara , Masaki Kitaoka
IPC分类号： C03C17/00 , C03C17/25 , C03C17/36 , C09D1/00 , C09D183/02 , G02F1/1335
CPC分类号： C03C17/3607 , C03C17/009 , C03C17/25 , C03C17/36 , C03C17/3642 , C03C17/3663 , C09D1/00 , C09D183/02 , G02F1/133516 , C03C2217/213 , C03C2217/45 , C03C2217/485 , C03C2217/78 , C03C2218/11 , Y10T428/31 , Y10T428/31507
摘要： A method for forming a silicon dioxide film according to the present invention comprises steps of: (i) contacting a substrate with processing solution containing silicofluoric acid solution supersaturated with silicon dioxide, and (ii) forming the silicon dioxide film on the substrate; wherein organic colorant(s) is/are introduced into the silicon dioxide film by adding organic colorant(s) to the processing solution. According to the present invention, a silicon dioxide film containing organic colorant without defect such as air bubbles, or undecomposed raw material.
摘要翻译：根据本发明的形成二氧化硅膜的方法包括以下步骤：（i）使基底与含有二氧化硅过饱和的硅氟酸溶液的处理溶液接触，和（ii）在基底上形成二氧化硅膜; 其中通过向处理溶液中加入有机着色剂将有机着色剂引入二氧化硅膜中。根据本发明，含有无缺陷的有机着色剂如气泡或未分解的原料的二氧化硅膜。

9. 发明授权

US5232781A Method for manufacturing layer-built material with silicon dioxide film containing organic colorant and the layer-built material manufactured thereby 失效
标题翻译：使用含有有机着色剂的二氧化硅膜制造层状材料的方法和由其制造的层叠材料
公开(公告)号：US5232781A
公开(公告)日：1993-08-03
申请号：US834455
申请日：1992-02-12
申请人： Kazuo Takemura , Juichi Ino , Hideo Kawahara , Masaki Kitaoka
发明人： Kazuo Takemura , Juichi Ino , Hideo Kawahara , Masaki Kitaoka
IPC分类号： C03C17/00 , C03C17/25 , C03C17/36 , C09D1/00 , C09D183/02 , G02F1/1335
CPC分类号： C03C17/3607 , C03C17/009 , C03C17/25 , C03C17/36 , C03C17/3642 , C03C17/3657 , C09D1/00 , C09D183/02 , G02F1/133516 , C03C2217/213 , C03C2217/45 , C03C2217/485 , C03C2218/11 , Y10T428/2993 , Y10T428/2996 , Y10T428/2998 , Y10T428/31 , Y10T428/315
摘要： A method for forming a silicon dioxide film according to the present invention comprises steps of: (i) contacting a substrate with processing solution containing silicofluoric acid solution supersaturated with silicon dioxide, and (ii) forming the silicon dioxide film on the substrate; wherein organic colorant(s) is/are introduced into the silicon dioxide film by adding organic colorant(s) to the processing solution. According to the present invention, a silicon dioxide film containing organic colorant without defect such as air bubbles, or undecomposed raw material.
摘要翻译：根据本发明的形成二氧化硅膜的方法包括以下步骤：（i）使基底与含有二氧化硅过饱和的硅氟酸溶液的处理溶液接触，和（ii）在基底上形成二氧化硅膜; 其中通过向处理溶液中加入有机着色剂将有机着色剂引入二氧化硅膜中。根据本发明，含有无缺陷的有机着色剂如气泡或未分解的原料的二氧化硅膜。

10. 发明授权

US5220482A Thin film capacitor 失效
标题翻译：薄膜电容器
公开(公告)号：US5220482A
公开(公告)日：1993-06-15
申请号：US826468
申请日：1992-01-27
申请人： Kazuo Takemura , Harunobu Yoshida , Hideo Kawahara , Eiji Mizushima , Masanaga Kikuzawa
发明人： Kazuo Takemura , Harunobu Yoshida , Hideo Kawahara , Eiji Mizushima , Masanaga Kikuzawa
IPC分类号： H01L21/316 , H01L21/02 , H01L21/822 , H01L27/04 , H01L29/94
CPC分类号： H01L28/40 , H01L29/94
摘要： A thin film capacitor having high performances, e.g. high frequency characteristics, heat resistance and dielectric strength, and capable of meeting demands for high integration and miniaturization of electronic devices, which comprises an electrically conductive substrate, a silica thin film formed on the substrate by bringing the substrate into contact with an aqueous solution of hydrosilicofluoric acid supersaturated with silica, and an electrically conductive film formed as an electrode on the silica thin film.

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