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1. 发明授权

US07648560B2 Method for producing Ti or Ti alloy through reduction by Ca 失效
标题翻译：通过Ca还原生产Ti或Ti合金的方法
公开(公告)号：US07648560B2
公开(公告)日：2010-01-19
申请号：US10575225
申请日：2004-10-06
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Katsunori Dakeshita
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Katsunori Dakeshita
IPC分类号： C22B34/12 , C25C1/02
CPC分类号： C25C3/02 , C22B34/1268 , C22B34/1272 , C22B34/1295
摘要： The present invention is a method for producing Ti or a Ti alloy through reduction of TiCl4 by Ca, which can produce the high-purity metallic Ti or high-purity Ti alloy. A molten salt containing CaCl2 and having Ca dissolved therein is held in a reactor vessel, and a metallic chloride containing TiCl4 is reacted with Ca in the molten salt to generate Ti particles or Ti alloy particles in a molten CaCl2 solution, which allows enhancement of a feed rate of TiCl4 which is of a raw material of Ti, and also allows a continuous operation. Therefore, the high-purity metallic Ti or the high-purity Ti alloy can economically be produced with high efficiency. Further, the method by the present invention eliminates the need of replenishment of expensive metallic Ca and of the operation for separately handling Ca which is highly reactive and difficult to handle.
摘要翻译：本发明是通过还原TiCl 4来生产Ti或Ti合金的方法，其可以生产高纯度金属Ti或高纯Ti合金。将含有CaCl 2并将Ca溶解在其中的熔融盐保持在反应容器中，含有TiCl 4的金属氯化物与熔融盐中的Ca反应，生成熔融CaCl 2溶液中的Ti粒子或Ti合金粒子，作为原料Ti的TiCl4的进料速度，并且还允许连续操作。因此，可以高效率地经济地制造高纯度金属Ti或高纯Ti合金。此外，本发明的方法消除了对昂贵的金属Ca的补充的需要和用于单独处理高反应性和难以处理的Ca的操作。

2. 发明申请

US20090101517A1 Method for Producing Ti or Ti Alloy, and Pulling Electrolysis Method Applicable Thereto 审中-公开
标题翻译：生产Ti或Ti合金的方法，以及拉拔电解方法
公开(公告)号：US20090101517A1
公开(公告)日：2009-04-23
申请号：US11887511
申请日：2006-03-16
申请人： Kazuo Takemura , Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori
发明人： Kazuo Takemura , Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori
IPC分类号： C25C1/24 , C25C1/06
CPC分类号： C25C3/28 , C22B5/04 , C22B34/1268 , C22B34/129 , C25C3/02 , C25C3/26 , C25C5/04 , C25C7/00
摘要： In producing Ti or a Ti alloy through reduction by Ca, an electrolytic-bath salt taken out from a reduction process is electrolyzed to recover Ca and the electrolytic-bath salt as a solid substance, and the recovered Ca and electrolytic-bath salt are delivered to the reduction process. Therefore, heat generation is suppressed in the reduction process by utilizing latent heat of fusion possessed by the solid substance, thereby largely improving production efficiency and thermal efficiency. Additionally, a reaction temperature is easily controlled, and a raw-material loading rate can be enhanced to efficiently produce Ti or the Ti alloy. At this point, using a pulling electrolysis method of the invention, the solid-state Ca and electrolytic-bath salt can be obtained at a low voltage and high current efficiency, i.e., with the relatively small power consumption. When the solid-state Ca and electrolytic-bath salt is used as a Ca source in producing Ti or the Ti alloy through reduction by Ca, the Ti or Ti alloy can efficiently be produced.
摘要翻译：在通过Ca还原生产Ti或Ti合金时，从还原过程中取出的电解浴盐被电解以回收Ca和作为固体物质的电解浴盐，并且回收的Ca和电解浴盐被输送到减少过程。因此，通过利用固体物质所具有的熔解潜热，在还原过程中抑制发热，从而大大提高生产效率和热效率。另外，可以容易地控制反应温度，并且可以提高原料负载率，以有效地生产Ti或Ti合金。此时，使用本发明的拉电解法，可以以低电压和高电流效率即功耗相对较小获得固态Ca和电解浴盐。当使用固态Ca和电解浴盐作为通过Ca还原生产Ti或Ti合金的Ca源时，可以有效地制备Ti或Ti合金。

3. 发明申请

US20080095930A1 Method For Producing Negative Electrode For Lithium Secondary Battery 审中-公开
标题翻译：锂二次电池负极生产方法
公开(公告)号：US20080095930A1
公开(公告)日：2008-04-24
申请号：US11575466
申请日：2005-09-05
申请人： Yoshitake Natsume , Tadashi Ogasawara , Kazuomi Azuma
发明人： Yoshitake Natsume , Tadashi Ogasawara , Kazuomi Azuma
IPC分类号： B05D5/12
CPC分类号： H01M4/0426 , H01M4/1391 , H01M4/485 , H01M4/525 , H01M4/661 , H01M10/0525 , H01M2004/021 , H01M2004/027 , Y10T29/49115
摘要： The lowness of the initial efficiency which is a drawback of lithium secondary batteries wherein a SiO negative electrode is used is largely made better without hindering a large initial charge capacity peculiar to the lithium secondary batteries. A fall in the cycle characteristic when the thickness of the SiO layer is made large is prevented. To realize these matters, a thin film of SiO is formed, as a negative electrode active material layer, on the surface of a current collector by vacuum evaporation or sputtering. The film is preferably formed by an ion plating process. The thickness of the SiO thin film is set to 5 μm or more. The surface roughness of the current collector is set to follows: the maximum height roughness Rz=5.0 or more. After the formation of the thin film, the film is thermally treated in a nonoxidative atmosphere.
摘要翻译：作为使用了SiO负极的锂二次电池的缺点的初始效率的低度大大地变得更好，而不会妨碍锂二次电池特有的大的初始充电能力。防止了当SiO层的厚度变大时的循环特性的下降。为了实现这些目的，通过真空蒸发或溅射在集电体的表面上形成SiO的薄膜作为负极活性物质层。该膜优选通过离子镀工艺形成。 SiO薄膜的厚度设定为5μm以上。集电体的表面粗糙度设定为：最大高度粗糙度Rz = 5.0以上。薄膜形成后，在非氧化气氛中进行热处理。

4. 发明申请

US20080078679A1 Method and Apparatus for Producing Metal by Molten-Salt Electrolysis 审中-公开
标题翻译：通过熔盐电解生产金属的方法和装置
公开(公告)号：US20080078679A1
公开(公告)日：2008-04-03
申请号：US11576887
申请日：2005-10-05
申请人： Masanori Yamaguchi , Yuichi Ono , Susumu Kosemura , Eiji Nishimura , Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi
发明人： Masanori Yamaguchi , Yuichi Ono , Susumu Kosemura , Eiji Nishimura , Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi
IPC分类号： C25C3/02 , C25C3/28 , C25C7/00
CPC分类号： C22B34/129 , C25C3/02 , C25C3/28 , C25C7/025
摘要： A method for production of metal by molten-salt electrolysis of the present invention is a method for production of metal by molten-salt electrolysis which is performed by filling a molten salt of calcium chloride in an electrolysis vessel having a anode and a cathode, one of the anode or cathode is arranged surrounding the other electrode, the cathode has at least one hole communicating the inner area surrounded by the cathode with the outer area, and the molten salt flows through the communicating holes from one area including the anode (the inner area or outer area) to the other area.
摘要翻译：本发明的通过熔盐电解生产金属的方法是通过熔融盐电解生产金属的方法，其通过在具有阳极和阴极的电解容器中填充氯化钙的熔融盐，一种阳极或阴极被布置为围绕另一电极，阴极具有至少一个孔，其将由阴极包围的内部区域与外部区域连通，并且熔融盐从包括阳极的一个区域（内部）流过连通孔区域或外部区域）到另一个区域。

5. 发明申请

US20070187255A1 Method for producing ti or ti alloy through reduction by ca 审中-公开
标题翻译：通过还原制备钛或钛合金的方法
公开(公告)号：US20070187255A1
公开(公告)日：2007-08-16
申请号：US10589879
申请日：2005-02-16
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Katsunori Dakeshita
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Katsunori Dakeshita
IPC分类号： C25C3/28
CPC分类号： C22B34/1272 , C22B34/129 , C25C5/04
摘要： The invention is a method for producing Ti or Ti alloys through reduction of TiCl4 by Ca, which can produce high-purity Ti metals or Ti alloys. A molten salt containing CaCl2 and having Ca dissolved therein is held in a reactor cell, electrolysis is performed in the molten salt in the reactor cell, and particulate Ti or Ti alloys are generated in the molten salt by supplying a metallic chloride containing TiCl4 to the molten salt so as to react with Ca generated on a cathode electrode side by the electrolysis, allowing enhancement of a feed rate of TiCl4 as a raw material of Ti, and also a continuous operation. Further, the method by the invention eliminates the need of the separate handling of Ca, because a reducing reaction and an electrolytic reaction can simultaneously proceed in the reactor cell to replenish Ca, consumed in the reducing reaction, by the electrolytic reaction. Accordingly, the production method by the invention can be used as means for efficiently and economically producing high-purity Ti metals or Ti alloys.
摘要翻译：本发明是通过Ca还原TiCl 4制备Ti或Ti合金的方法，其可以生产高纯Ti金属或Ti合金。将含有CaCl 2 Ca的Ca盐溶解在其中的熔融盐保持在反应器电池中，在反应器电池中的熔融盐中进行电解，并且在熔融盐中产生颗粒状的Ti或Ti合金，将含有TiCl 4的金属氯化物供给熔融盐，以便通过电解与在阴极电极侧产生的Ca反应，从而提高TiCl 4的进料速率，作为Ti的原料，也是连续操作。此外，本发明的方法消除了对Ca的单独处理的需要，因为还原反应和电解反应可以在反应器电池中同时进行以补充通过电解反应在还原反应中消耗的Ca。因此，本发明的制造方法可以用作高效且经济地制造高纯度Ti金属或Ti合金的手段。

6. 发明申请

US20070131057A1 Method for producing ti or ti alloy through reduction by ca 审中-公开
标题翻译：通过还原制备钛或钛合金的方法
公开(公告)号：US20070131057A1
公开(公告)日：2007-06-14
申请号：US10575224
申请日：2004-10-06
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Yuko Urasaki , Kazuo Takemura
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi , Yuko Urasaki , Kazuo Takemura
IPC分类号： B22F9/24
CPC分类号： C25C3/28 , C22B34/1272 , C22B34/1295 , C25C3/02
摘要： A method for producing Ti or Ti alloys through reduction by Ca, including: a reduction step of holding a molten salt, containing CaCl2 and having Ca dissolved therein, in a reactor vessel 1, and reacting a metallic chloride containing TiCl4 with Ca in said salt to generate particles of Ti or Ti alloys in said salt; and a separation step of separating particles of Ti or Ti alloys, generated in said salt, from said salt. An electrolysis step 8, in which CaCl2 discharged outside the reactor vessel 1 is electrolyzed into Ca and Cl2, and the generated Ca is used for the generation reaction of Ti or Ti alloys in the reactor vessel 1, is preferably added. In the electrolysis step 8, an alloy electrode made of a molten Ca alloy, if applied for a cathode, is effective in enhancing the electricity efficiency, and also can be effectively utilized as a carrier medium of Ca for raising a Ca concentration of molten salt. By this method, high-purity Ti metals can be efficiently and economically produced.
摘要翻译：一种通过Ca还原制造Ti或Ti合金的方法，包括：将含有CaCl 2·Ca和Ca的溶解在其中的熔融盐保持在反应容器1中的还原步骤，并使金属在所述盐中含有TiCl 4 Si与Ca的氯化物，以在所述盐中产生Ti或Ti合金颗粒; 以及分离步骤，从所述盐分离在所述盐中产生的Ti或Ti合金的颗粒。电解步骤8，其中排放到反应容器1外部的CaCl 2电解为Ca和Cl 2，并且所产生的Ca用于Ti或优选添加反应器容器1中的Ti合金。在电解工序8中，如果用于阴极，则由熔融的Ca合金构成的合金电极，对于提高电效率是有效的，也可以有效地利用Ca作为提高熔融盐的Ca浓度的载体介质。通过这种方法，可以高效且经济地生产高纯度Ti金属。

7. 发明申请

US20060266698A1 Titanium powder sintered compact 失效
标题翻译：钛粉烧结体
公开(公告)号：US20060266698A1
公开(公告)日：2006-11-30
申请号：US11501733
申请日：2006-08-10
申请人： Takashi Onishi , Tadashi Ogasawara , Munetoshi Watanabe , Masamichi Kato
发明人： Takashi Onishi , Tadashi Ogasawara , Munetoshi Watanabe , Masamichi Kato
IPC分类号： B01D29/00
CPC分类号： H01M8/0232 , B01D39/2034 , B01D39/2079 , B01D2201/188 , B22F1/0048 , B22F3/004 , B22F3/10 , B22F3/11 , B22F3/1103 , B22F3/1109 , B22F2998/00 , B22F2998/10 , B22F2999/00 , H01M8/0247 , Y10T428/12014 , Y10T428/12021 , B22F9/082 , B22F2207/11 , B22F3/02
摘要： Provided are a porous sintered compact suitable for a filter, a power feeder in a polymer electrolyte membrane type water electrolyzer, a current collector in a solid polymer fuel cell and in addition a liquid dispersion plate, especially an ink dispersion plate for an ink jet printer ink and the like. A titanium powder sintered compact made of a plate-like porous compact is obtained by sintering spherical powder made of titanium or a titanium alloy produced by means of a gas atomization method. A void ratio in the range of from 35 to 55% is realized by filling without applying a pressure and sintering without applying a pressure.
摘要翻译：提供一种适用于过滤器的多孔烧结体，聚合物电解质膜型水电解槽中的动力给料机，固体高分子型燃料电池中的集电体，以及液体分散板，特别是喷墨打印机用油墨分散板油墨等。通过烧结通过气体雾化法制造的由钛或钛合金制成的球形粉末，获得由板状多孔压块制成的钛粉末烧结体。通过在不施加压力的情况下施加压力和烧结而填充而实现35至55％范围内的空隙率。

8. 发明申请

US20050085095A1 Sintered object of silicon monoxide and method for producing the same 失效
标题翻译：一氧化硅的烧结体及其制造方法
公开(公告)号：US20050085095A1
公开(公告)日：2005-04-21
申请号：US10501996
申请日：2002-11-29
申请人： Yoshitake Natsume , Tadashi Ogasawara , Munetoshi Watanabe , Kazuomi Azuma , Toshiharu Iwase
发明人： Yoshitake Natsume , Tadashi Ogasawara , Munetoshi Watanabe , Kazuomi Azuma , Toshiharu Iwase
IPC分类号： C04B35/14 , C04B35/645 , C23C14/24 , C23C14/34 , H01L21/31 , H01L21/469
CPC分类号： C04B35/645 , C04B35/14 , C04B2235/3418 , C04B2235/5427 , C04B2235/604 , C04B2235/658 , C04B2235/6581 , C04B2235/79
摘要： A sintered object of silicon monoxide for use as a material for forming silicon oxide thin films is provided of which the evaporation residue as determined by subjecting a sample thereof to thermogravimetry at a heating temperature of 1,300° C. and in a vacuum atmosphere, namely at a pressure of not higher than 10 Pa, is not more than 4% by mass relative to the sample before measurement. This sintered object can be produced by sintering SiO particles having a particle diameter of not smaller than 250 μm, either after press forming thereof or during press forming thereof, in a non-oxygen atmosphere. This sintered object is high in evaporation rate and, when it is used as a material for film formation, an improvement in productivity in producing silicon oxide thin films can be expected. Thus, it can be widely applied in forming silicon oxide thin films useful as electric insulating films, mechanical protection films, optical films, barrier films of food packaging materials, etc.
摘要翻译：提供用作形成氧化硅薄膜的材料的一氧化硅的烧结体，其中通过将样品在1,300℃的加热温度和真空气氛中，即在 10Pa以下的压力相对于测定前的样品不超过4质量％。该烧结体可以通过在非氧气氛中烧结粒径不小于250μm的SiO粒子，或者在其压制成型之后或在其压制成形期间来制造。该烧结体的蒸发速度高，并且当其用作成膜材料时，可以预期提高生产氧化硅薄膜的生产率。因此，可以广泛地应用于形成用作电绝缘膜，机械保护膜，光学膜，食品包装材料的阻隔膜等的氧化硅薄膜等。

9. 发明授权

US4709509A Numerically controlled grinding machine 失效
标题翻译：数控磨床
公开(公告)号：US4709509A
公开(公告)日：1987-12-01
申请号：US920192
申请日：1986-10-17
申请人： Takao Yoneda , Tadashi Ogasawara , Norio Ohta , Yasuji Sakakibara
发明人： Takao Yoneda , Tadashi Ogasawara , Norio Ohta , Yasuji Sakakibara
IPC分类号： B24B47/22 , B23Q15/14 , B24B5/01 , B24B49/02 , B24B51/00 , G05B19/401
CPC分类号： B24B5/01 , B23Q15/14 , B24B49/02 , G05B19/4015
摘要： A numerically controlled grinding machine equipped with two registers in which data concerning the positions of the cylindrical and shoulder grinding surfaces of a grinding wheel is stored. A reference point is established on the wheel spindle stock. A reference member having two reference surfaces is disposed on the worktable. The machine further includes a manual pulse generator for moving the grinding wheel head and the worktable, detectors for detecting the distances traveled by the wheel head and the worktable, a data entry device, an arithmetic processing unit, and a memory.
摘要翻译：一种数控磨床，配有两个寄存器，其中存储有关砂轮的圆柱和肩磨削面的位置的数据。在主轴轴上设置参考点。具有两个参考表面的参考构件设置在工作台上。该机器还包括用于移动砂轮头和工作台的手动脉冲发生器，用于检测由轮头和工作台行进的距离的检测器，数据输入装置，运算处理单元和存储器。

10. 发明授权

US07951284B2 Electrolysis apparatus, electrochemical reaction membrane apparatus, porous electrical conductor, and production method thereof 有权
标题翻译：电解装置，电化学反应膜装置，多孔电导体及其制造方法
公开(公告)号：US07951284B2
公开(公告)日：2011-05-31
申请号：US11361722
申请日：2006-02-24
申请人： Koji Nakazawa , Masanori Okabe , Masato Kita , Kenji Taruya , Tadashi Ogasawara , Kazuomi Azuma , Takashi Onishi
发明人： Koji Nakazawa , Masanori Okabe , Masato Kita , Kenji Taruya , Tadashi Ogasawara , Kazuomi Azuma , Takashi Onishi
IPC分类号： B23H3/00
CPC分类号： B22F3/1146 , B22F2003/241 , B22F2003/247 , C25B9/04
摘要： A water electrolysis apparatus includes a plurality of unit cells. A membrane electrode assembly of the unit cell includes an anode side power feeding element and a cathode side power feeding element stacked on an anode catalyst layer and a cathode catalyst layer on both surfaces of a solid polymer electrolyte membrane. A surface of the anode side power feeding element is subjected to a grinding process, and then, subjected to an etching process to form a smooth surface.
摘要翻译：水电解装置包括多个单电池。单元电池的膜电极组件包括堆叠在固体聚合物电解质膜的两个表面的阳极催化剂层和阴极催化剂层上的阳极侧供电元件和阴极侧供电元件。对阳极侧供电元件的表面进行研磨处理，然后进行蚀刻处理以形成光滑表面。

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