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1. 发明授权

US06486365B1 Production and purification of phenol: hydroxyacetone removal by hydrotalcite 有权
标题翻译：苯酚的生产和纯化：通过水滑石除去羟基丙酮
公开(公告)号：US06486365B1
公开(公告)日：2002-11-26
申请号：US10063258
申请日：2002-04-04
申请人： John W. Fulmer , Bharat Singh , Pramod Kumbhar , Prashant Anil Tatake , Umesh Hasyagar
发明人： John W. Fulmer , Bharat Singh , Pramod Kumbhar , Prashant Anil Tatake , Umesh Hasyagar
IPC分类号： C07C3708
CPC分类号： C07C37/86 , C07C2521/10 , C07C39/04
摘要： A process for converting carbonyl-type impurities contained in a phenolic solvent to high-boiling derivatives is provided by contacting the phenolic solvent with a hydrotalcite-type material (HTM). The phenol can be separated from the high-boiling derivatives using conventional separation techniques, such as distillation, so the invention also provides a process for separating carbonyl-type impurities, such as hydroxyacetone (HA), from a phenolic solvent. The process can be applied in the conventional industrial process for converting cumene to phenol to remove carbonyl-type impurities from the phenol product. A process and a facility for producing purified phenol by converting cumene to phenol are provided. In the conversion of cumene to phenol, the phenol often contains carbonyl-type impurities. The phenol and carbonyl-type impurities are reacted in the presence of an HTM to produce phenol and high-boiling derivatives. The phenol may be further purified using conventional separation techniques, such as distillation, to remove the high-boiling derivatives.
摘要翻译：通过使酚类溶剂与水滑石类材料（HTM）接触来提供将酚类溶剂中所含的羰基型杂质转化成高沸点衍生物的方法。苯酚可以使用常规的分离技术如蒸馏从高沸点衍生物中分离，因此本发明还提供了从酚类溶剂中分离羰基型杂质如羟基丙酮（HA）的方法。该方法可用于将异丙基苯转化为苯酚以从苯酚产物中除去羰基型杂质的常规工业方法。提供了通过将异丙基苯转化成苯酚来生产纯化苯酚的方法和设备。在异丙苯转化为苯酚时，苯酚常含有羰基型杂质。苯酚和羰基型杂质在HTM存在下反应生成苯酚和高沸点衍生物。可以使用常规分离技术如蒸馏进一步纯化苯酚，以除去高沸点衍生物。

2. 发明授权

US07491855B2 Integrated process for the production of bisphenol A from cumene hydroperoxide 有权
标题翻译：由氢过氧化枯烯生产双酚A的综合工艺
公开(公告)号：US07491855B2
公开(公告)日：2009-02-17
申请号：US10250114
申请日：2003-06-04
申请人： Pramod Shankar Kumbhar , Jegadeesh Thampi , Bharat Singh , John W. Fulmer , Prashant Anil Tatake
发明人： Pramod Shankar Kumbhar , Jegadeesh Thampi , Bharat Singh , John W. Fulmer , Prashant Anil Tatake
IPC分类号： C07C39/16
CPC分类号： C07C37/20 , C07C37/08 , Y02P20/125 , Y02P20/52 , C07C39/04 , C07C39/16
摘要： Use of a specific combination of catalysts for the first and second steps of the process for the conversion of CHP to BPA provides high yields of BPA and low impurity yields, without a requirement for the intermediate purification steps. In the first step, CHP is cleaved in the presence of an acid treated clay such as acid treated Montmorillonite clay to produce phenol and acetone. In the second step, the phenol and acetone produced is reacted, preferably without intermediate purification, in the presence of a cation exchange resin catalyst that includes a cation exchange resin and a mercaptan or mercaptoalkanoic acid promoter to produce BPA.
摘要翻译：用于将CHP转化为BPA的方法的第一和第二步骤的特定的催化剂组合的使用提供了高产率的BPA和低杂质产率，而不需要中间纯化步骤。在第一步中，CHP在酸处理的粘土如酸处理的蒙脱石粘土存在下裂解，以产生苯酚和丙酮。在第二步中，所生产的苯酚和丙酮优选不经中间纯化，在包含阳离子交换树脂和硫醇或巯基链烷酸促进剂以产生BPA的阳离子交换树脂催化剂的存在下反应。

3. 发明授权

US07154010B2 Integrated process for the production of bisphenol A from cumene hydroperoxide 有权
标题翻译：由氢过氧化枯烯生产双酚A的综合工艺
公开(公告)号：US07154010B2
公开(公告)日：2006-12-26
申请号：US10250107
申请日：2003-06-04
申请人： Pramod Shankar Kumbhar , Jegadeesh Thampi , Bharat Singh , John W. Fulmer , Prashant Anil Tatake
发明人： Pramod Shankar Kumbhar , Jegadeesh Thampi , Bharat Singh , John W. Fulmer , Prashant Anil Tatake
IPC分类号： C07C36/16
CPC分类号： C07C37/20 , C07C37/08 , C07C45/53 , Y02P20/125 , Y02P20/52 , C07C39/04 , C07C39/16 , C07C49/08
摘要： Use of a specific combination of catalysts for the first and second steps of the process for the conversion of CHP to BPA provides high yields of BPA and low impurity yields, without a requirement for the intermediate purification steps. In the first step, CHP is cleaved in the presence of a sulfated metal oxide catalyst such as sulfated Zirconia to produce phenol and acetone. In the second step, the phenol and acetone produced is reacted, preferably without intermediate purification, in the presence of a cation exchange resin catalyst that includes a cation exchange resin and a mercaptan or mercaptoalkanoic acid promoter to produce BPA.
摘要翻译：用于将CHP转化为BPA的方法的第一和第二步骤的特定的催化剂组合的使用提供了高产率的BPA和低杂质产率，而不需要中间纯化步骤。在第一步中，CHP在硫酸化金属氧化物催化剂如硫酸化氧化锆存在下裂解，生成苯酚和丙酮。在第二步中，所生产的苯酚和丙酮优选不经中间纯化，在包含阳离子交换树脂和硫醇或巯基链烷酸促进剂以产生BPA的阳离子交换树脂催化剂的存在下反应。

4. 发明授权

US07109385B2 Process for producing phenol 有权
标题翻译：苯酚生产工艺
公开(公告)号：US07109385B2
公开(公告)日：2006-09-19
申请号：US11092078
申请日：2005-03-29
申请人： Prashant Anil Tatake , Pramod Shankar Kumbhar , Bharat Singh , John William Fulmer , Sabyasachi Mandal , Arun N. Kumar , Rupesh Pawar
发明人： Prashant Anil Tatake , Pramod Shankar Kumbhar , Bharat Singh , John William Fulmer , Sabyasachi Mandal , Arun N. Kumar , Rupesh Pawar
IPC分类号： C07C37/08
CPC分类号： C07C37/08 , C07C39/04
摘要： A process for producing a phenol product generally comprises a first step comprising reacting in a first reactor a feed stream comprising cumene hydroperoxide and water with an acid catalyst to produce an effluent comprising the phenol product, acetone, and at least 1% by weight residual cumene hydroperoxide, and a second step comprising passing the effluent into a second reactor and decomposing the residual cumene hydroperoxide, wherein during said process the ratio of phenol to acetone is maintained at a molar ratio of greater than 1:1, and wherein the water in each of the first and second steps is present in an amount more than 0 and less than or equal to 5 weight percent based on the total weight of the feed stream or effluent, and wherein the process is continuous.
摘要翻译：一种生产酚产物的方法通常包括第一步骤，包括在第一反应器中使含有氢过氧化枯烯和水的进料流与酸催化剂反应以产生包含苯酚产物，丙酮和至少1重量％的残余枯烯的流出物氢过氧化物，第二步骤包括使流出物流入第二反应器并分解残留的氢过氧化枯烯，其中在所述方法期间，苯酚与丙酮的比例保持在大于1:1的摩尔比，并且其中每个基于进料流或流出物的总重量，第一步和第二步的存在量大于0且小于或等于5重量％，并且其中该方法是连续的。

5. 发明申请

US20050137429A1 Methods for purification of phenol 审中-公开
标题翻译：苯酚纯化方法
公开(公告)号：US20050137429A1
公开(公告)日：2005-06-23
申请号：US10758373
申请日：2004-01-15
申请人： Prashant Tatake , Umesh Hasyagar , Pramond Kumbhar , Bharat Singh , John Fulmer
发明人： Prashant Tatake , Umesh Hasyagar , Pramond Kumbhar , Bharat Singh , John Fulmer
IPC分类号： C07C37/82 , C07C37/86 , C07C37/68 , C07C29/74
CPC分类号： C07C37/82 , C07C39/04
摘要： A process for producing a purified phenol stream generally includes contacting a phenol stream containing an initial concentration of hydroxyacetone and methylbenzofuran with an acidic ion exchange resin at a temperature of 50° C. to 100° C. to concurrently reduce the initial concentration of the hydroxyacetone and the methylbenzofuran in the phenol stream to produce the purified phenol stream.
摘要翻译：纯化苯酚流的制备方法通常包括在50℃至100℃的温度下使含有初始浓度的羟基丙酮和甲基苯并呋喃的苯酚流与酸性离子交换树脂接触，同时降低羟基丙酮的初始浓度和苯酚流中的甲基苯并呋喃以产生纯化的苯酚流。

6. 发明申请

US20050222466A1 Process for producing phenol 有权
标题翻译：苯酚生产工艺
公开(公告)号：US20050222466A1
公开(公告)日：2005-10-06
申请号：US11092078
申请日：2005-03-29
申请人： Prashant Tatake , Pramod Kumbhar , Bharat Singh , John Fulmer , Sabyasachi Mandal , Arun Kumar , Rupesh Pawar
发明人： Prashant Tatake , Pramod Kumbhar , Bharat Singh , John Fulmer , Sabyasachi Mandal , Arun Kumar , Rupesh Pawar
IPC分类号： C07C37/08 , C07C39/04
CPC分类号： C07C37/08 , C07C39/04
摘要： A process for producing a phenol product generally comprises a first step comprising reacting in a first reactor a feed stream comprising cumene hydroperoxide and water with an acid catalyst to produce an effluent comprising the phenol product, acetone, and at least 1% by weight residual cumene hydroperoxide, and a second step comprising passing the effluent into a second reactor and decomposing the residual cumene hydroperoxide, wherein during said process the ratio of phenol to acetone is maintained at a molar ratio of greater than 1:1, and wherein the water in each of the first and second steps is present in an amount more than 0 and less than or equal to 5 weight percent based on the total weight of the feed stream or effluent, and wherein the process is continuous.
摘要翻译：一种生产酚产物的方法通常包括第一步骤，包括在第一反应器中使含有氢过氧化枯烯和水的进料流与酸催化剂反应以产生包含苯酚产物，丙酮和至少1重量％的残余枯烯的流出物氢过氧化物，第二步骤包括使流出物流入第二反应器并分解残留的氢过氧化枯烯，其中在所述方法期间，苯酚与丙酮的比例保持在大于1:1的摩尔比，并且其中每个基于进料流或流出物的总重量，第一步和第二步的存在量大于0且小于或等于5重量％，并且其中该方法是连续的。

7. 发明授权

US06573408B1 System and method for purifying cumene hydroperoxide cleavage products 有权
标题翻译：枯烯氢过氧化物裂解产物的系统和方法
公开(公告)号：US06573408B1
公开(公告)日：2003-06-03
申请号：US09683190
申请日：2001-11-29
申请人： John William Fulmer , Pramod S. Kumbhar , Marakani Venkata Ramani , Bharat Singh
发明人： John William Fulmer , Pramod S. Kumbhar , Marakani Venkata Ramani , Bharat Singh
IPC分类号： C07C4500
CPC分类号： C07C37/86 , B01J19/0086 , B01J2219/00006 , C07C45/85 , C07C39/04
摘要： A system for purifying a cumene hydroperoxide cleavage product mixture comprises a cumene hydroperoxide cleavage product mixture feed containing impurities in fluid communication with an aqueous alkaline solution feed; the cumene hydroperoxide cleavage product mixture and aqueous alkaline solution feeds are in fluid communication with a neutralization drum having an aqueous salt phase outlet; an aqueous salt phase feed containing impurities in fluid communication with a heat treatment vessel having a heat-treated aqueous salt phase outlet; and a heat-treated aqueous salt phase feed containing water-soluble derivatives of the impurities in fluid communication with the cumene hydroperoxide cleavage product mixture prior to the neutralization drum.
摘要翻译：用于纯化氢过氧化枯烯裂解产物混合物的系统包括含有与碱性水溶液进料流体连通的杂质的枯烯氢过氧化物裂解产物混合物进料; 氢过氧化枯烯裂解产物混合物和碱性水溶液进料与具有盐水相出口的中和鼓流体连通; 含有与具有热处理的盐水相出口的热处理容器流体连通的杂质的含水盐相进料; 和热处理的含水盐相进料，其含有在中和鼓之前与氢过氧化枯烯裂解产物混合物流体连通的杂质的水溶性衍生物。

8. 发明申请

US20100258745A1 OPTICAL ARTICLE HAVING ANTI-THEFT FEATURE AND A SYSTEM AND METHOD FOR INHIBITING THEFT OF SAME 有权
标题翻译：具有防伪特征的光学文章和用于抑制它们的系统和方法
公开(公告)号：US20100258745A1
公开(公告)日：2010-10-14
申请号：US12704578
申请日：2010-02-12
申请人： Marc Brian Wisnudel , Terry Michael Topka , Pingfan Peter Wu , Radislav Alexandrovich Potyrailo , David Gilles Gascoyne , William David Smith , Adil Minoo Dhalla , Yogendrasinh Bharatsinh Chauhan , Rupesh Bhikaji Pawar , Bharat Singh , Sriramakrishna Maruvada , Vandita Pai-Paranjape , Kenneth Brakeley Welles, II , Philippe Schottland , Eugene George Olczak , Ashok Menon
发明人： Marc Brian Wisnudel , Terry Michael Topka , Pingfan Peter Wu , Radislav Alexandrovich Potyrailo , David Gilles Gascoyne , William David Smith , Adil Minoo Dhalla , Yogendrasinh Bharatsinh Chauhan , Rupesh Bhikaji Pawar , Bharat Singh , Sriramakrishna Maruvada , Vandita Pai-Paranjape , Kenneth Brakeley Welles, II , Philippe Schottland , Eugene George Olczak , Ashok Menon
IPC分类号： G21K5/00
CPC分类号： G11B23/286 , G11B11/10584 , G11B20/00086 , G11B23/0042 , G11B23/282 , Y10S428/913 , Y10S428/916 , Y10T428/24917
摘要： A system for altering a functionality of an optical article from a pre-activated state to an activated state, comprising an optical article comprising an optical data layer for storing data, an external radiation source for generating an external stimulus adapted to interact with the optical article, such interaction causing a change in optical accessibility of optically stored data, a directing material, wherein said directing material is for directing the external stimulus to selective portions of the optical article, thereby altering the functionality of the optical article from a pre-activated state to an activated state; a convertible element capable of responding to the external stimulus to irreversibly alter the optical article from the pre-activated state of functionality to the activated state of functionality, wherein said convertible element comprises a color-shift dye, a magnetic material, a thermo-chromic material, a magneto-optical material, a light scattering material, a phase-change material, dye aggregates, or combinations thereof.
摘要翻译：一种用于将光学制品的功能从预激活状态改变为激活状态的系统，包括包括用于存储数据的光学数据层的光学制品，用于产生适于与光学制品相互作用的外部刺激的外部辐射源，这种相互作用导致光学存储数据的光学可访问性的改变，导向材料，其中所述引导材料用于将外部刺激引导到光学制品的选择性部分，从而将光学制品的功能性从预激活状态到激活状态; 能够响应外部刺激的可转换元件，以将光学物品从预激活的功能状态改变为激活的功能状态，其中所述可转换元件包括色移染料，磁性材料，热铬材料，磁光材料，光散射材料，相变材料，染料聚集体或其组合。

9. 发明授权

US5309092A Token ring test simulation method and device 失效
标题翻译：令牌环测试模拟方法及装置
公开(公告)号：US5309092A
公开(公告)日：1994-05-03
申请号：US9523
申请日：1993-01-27
申请人： David Kuntz , Bharat Singh , Kittur Nagesh , Ronald McBride
发明人： David Kuntz , Bharat Singh , Kittur Nagesh , Ronald McBride
IPC分类号： G01R31/28 , G01R31/317 , G01R31/02
CPC分类号： H04L12/2697 , H04L12/433 , H04L43/50
摘要： A loopback connector system for testing token ring components such as routers or interface assemblies with requiring that the component to be tested be connected into the local area network (LAN). The connector permits the component to be tested to be isolated from the LAN, permitting the integrity of the component to be tested without regard to the integrity of lobe cables or other devices on the ring, and without degrading network performance. The connector system includes two different multi-pin connector types, a DB9 and an RJ45 connector, used to connect into the network, separated by a short two-pair cable. Resistors used to simulate the network loading on the component are connected between appropriate pins, with the resistors being shared between the two types of connectors.
摘要翻译：用于测试令牌环组件（如路由器或接口组件）的环回连接器系统，要求将要测试的组件连接到局域网（LAN）。连接器允许组件被测试与LAN隔离，允许测试组件的完整性，而不考虑环上的波形电缆或其他设备的完整性，并且不会降低网络性能。连接器系统包括两个不同的多针连接器类型，一个DB9和一个RJ45连接器，用于连接到网络中，由两根短路电缆分开。用于模拟组件上网络负载的电阻器连接在适当的引脚之间，电阻在两种类型的连接器之间共享。

10. 发明授权

US08057886B2 Optical article having anti-theft feature and a system and method for inhibiting theft of same 有权
标题翻译：具有防盗功能的光学制品以及用于防止盗窃的系统和方法
公开(公告)号：US08057886B2
公开(公告)日：2011-11-15
申请号：US12704578
申请日：2010-02-12
申请人： Marc Brian Wisnudel , Terry Michael Topka , Pingfan Peter Wu , Radislav Alexandrovich Potyrailo , David Gilles Gascoyne , William David Smith , Adil Minoo Dhalla , Yogendrasinh Bharatsinh Chauhan , Rupesh Bhikaji Pawar , Bharat Singh , Sriramakrishna Maruvada , Vandita Pai-Paranjape , Kenneth Brakeley Welles, II , Philippe Schottland , Eugene George Olczak , Ashok Menon
发明人： Marc Brian Wisnudel , Terry Michael Topka , Pingfan Peter Wu , Radislav Alexandrovich Potyrailo , David Gilles Gascoyne , William David Smith , Adil Minoo Dhalla , Yogendrasinh Bharatsinh Chauhan , Rupesh Bhikaji Pawar , Bharat Singh , Sriramakrishna Maruvada , Vandita Pai-Paranjape , Kenneth Brakeley Welles, II , Philippe Schottland , Eugene George Olczak , Ashok Menon
IPC分类号： B32B3/00
CPC分类号： G11B23/286 , G11B11/10584 , G11B20/00086 , G11B23/0042 , G11B23/282 , Y10S428/913 , Y10S428/916 , Y10T428/24917
摘要： A system for altering a functionality of an optical article from a pre-activated state to an activated state, comprising an optical article comprising an optical data layer for storing data, an external radiation source for generating an external stimulus adapted to interact with the optical article, such interaction causing a change in optical accessibility of optically stored data, a directing material, wherein said directing material is for directing the external stimulus to selective portions of the optical article, thereby altering the functionality of the optical article from a pre-activated state to an activated state; a convertible element capable of responding to the external stimulus to irreversibly alter the optical article from the pre-activated state of functionality to the activated state of functionality, wherein said convertible element comprises a color-shift dye, a magnetic material, a thermo-chromic material, a magneto-optical material, a light scattering material, a phase-change material, dye aggregates, or combinations thereof.
摘要翻译：一种用于将光学制品的功能从预激活状态改变为激活状态的系统，包括包括用于存储数据的光学数据层的光学制品，用于产生适于与光学制品相互作用的外部刺激的外部辐射源，这种相互作用导致光学存储数据的光学可访问性的改变，导向材料，其中所述引导材料用于将外部刺激引导到光学制品的选择性部分，从而将光学制品的功能性从预激活状态到激活状态; 能够响应外部刺激的可转换元件，以将光学物品从预激活的功能状态改变为激活的功能状态，其中所述可转换元件包括色移染料，磁性材料，热铬材料，磁光材料，光散射材料，相变材料，染料聚集体或其组合。

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