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1. 发明授权

US4434308A Manufacture of synthetic lubricant additives from internal olefins using boron trifluoride catalysis 失效
标题翻译：使用三氟化硼催化从内部烯烃制造合成润滑剂添加剂
公开(公告)号：US4434308A
公开(公告)日：1984-02-28
申请号：US372492
申请日：1982-04-28
申请人： John M. Larkin , Lewis W. Watts, Jr. , Edward T. Marquis
发明人： John M. Larkin , Lewis W. Watts, Jr. , Edward T. Marquis
IPC分类号： C07C2/20 , C10G50/02 , C07C1/16 , C07C5/00
CPC分类号： C07C2/20 , C10G50/02 , C07C2527/1213 , C07C2531/02
摘要： An improved process for the manufacture of synthetic lubricant additives from internal olefins is described. The process utilizes boron trifluoride catalysis with a promoter to produce oligomer mixtures that have surprisingly low viscosities at low temperatures and surprisingly high viscosity indexes as compared with the oligomers found in other methods. It is important that internal olefins be used almost exclusively in the method of this invention.
摘要翻译：描述了从内烯烃制造合成润滑剂添加剂的改进方法。该方法利用三氟化硼催化促进剂产生低聚物混合物，其在低温下具有惊人的低粘度，并且与其它方法中发现的低聚物相比，具有令人惊奇的高粘度指数。重要的是内部烯烃几乎完全用于本发明的方法中。

2. 发明授权

US4420647A Semi-synthetic lubricating oil composition 失效
标题翻译：半合成润滑油组成
公开(公告)号：US4420647A
公开(公告)日：1983-12-13
申请号：US371859
申请日：1982-04-26
申请人： Kenneth G. Hammond , Joseph C. Sendra , Lewis W. Watts, Jr. , Edward T. Marquis , John M. Larkin
发明人： Kenneth G. Hammond , Joseph C. Sendra , Lewis W. Watts, Jr. , Edward T. Marquis , John M. Larkin
IPC分类号： C10M107/02 , C10M111/02 , C10M169/04 , C10M1/18 , C07C1/16 , C07C3/18
CPC分类号： C10M169/04 , C10M107/02 , C10M111/02 , C10M2203/1006 , C10M2203/1025 , C10M2203/1045 , C10M2203/1065 , C10M2203/1085 , C10M2205/00 , C10M2205/0206 , C10M2205/024 , C10M2205/0285 , C10M2207/023 , C10M2207/024 , C10M2207/026 , C10M2207/027 , C10M2209/084 , C10M2209/104 , C10M2209/108 , C10M2215/04 , C10M2215/06 , C10M2215/064 , C10M2215/065 , C10M2215/066 , C10M2215/067 , C10M2215/068 , C10M2215/26 , C10M2215/28 , C10M2217/046 , C10M2217/06 , C10M2219/046 , C10M2223/045 , C10M2223/12 , C10M2223/121 , C10M2225/04 , C10M2225/041 , C10M2229/02 , C10M2229/04 , C10M2229/041 , C10M2229/042 , C10M2229/043 , C10M2229/044 , C10M2229/045 , C10M2229/046 , C10M2229/047 , C10M2229/048 , C10M2229/05 , C10M2229/051 , C10M2229/052 , C10M2229/053 , C10M2229/054 , C10N2210/02 , C10N2220/02
摘要： A synthetic lubricating oil composition comprising a major portion of a synthetic lubricant component or a mixture of a synthetic lubricant component and a hydrocarbon mineral base oil and a minor portion of various additive components is described. The synthetic lubricant component is manufactured from internal olefins.The process for making the synthetic lubricant component utilizes boron trifluoride catalysis with a promoter to produce oligomer mixtures that have surprisingly low viscosities at low temperatures and surprisingly high viscosity indexes as compared with the oligomers found in other methods. It is important that internal olefins be used predominantly to make the oligomers. Alpha olefins make up the balance of the olefins.
摘要翻译：描述了合成润滑油组合物，其包含主要部分的合成润滑剂组分或合成润滑剂组分和烃类矿物基础油的混合物和少量各种添加剂组分。合成润滑剂组分由内烯烃制成。制造合成润滑剂组分的方法利用三氟化硼催化促进剂来制备低聚物混合物，其低温粘度令人惊奇，与其它方法中发现的低聚物相比，具有惊人的高粘度指数。重要的是内部烯烃主要用于制备低聚物。 α-烯烃构成了烯烃的平衡。

3. 发明授权

US4287364A Molybdenum catalyst for aniline-formaldehyde condensation 失效
标题翻译：用于苯胺 - 甲醛缩合的钼催化剂
公开(公告)号：US4287364A
公开(公告)日：1981-09-01
申请号：US190531
申请日：1980-09-24
申请人： Edward T. Marquis , Robert M. Gipson , Lewis W. Watts, Jr.
发明人： Edward T. Marquis , Robert M. Gipson , Lewis W. Watts, Jr.
IPC分类号： B01J23/28 , C07C85/145
CPC分类号： B01J23/28
摘要： Covers a method of preparing diaminodiphenylmethanes and higher homologues thereof which comprises the step of condensing aniline and formaldehyde in the presence of a molybdenum aluminide catalyst.
摘要翻译：包括制备二氨基二苯基甲烷及其高级同系物的方法，其包括在钼铝化物催化剂存在下使苯胺和甲醛缩合的步骤。

4. 发明授权

US4284815A Tungsten catalyzed aniline-formaldehyde condensation 失效
标题翻译：钨催化苯胺 - 甲醛缩合
公开(公告)号：US4284815A
公开(公告)日：1981-08-18
申请号：US189474
申请日：1980-09-22
申请人： Edward T. Marquis , Lewis W. Watts, Jr. , Robert M. Gipson
发明人： Edward T. Marquis , Lewis W. Watts, Jr. , Robert M. Gipson
IPC分类号： B01J23/30 , B01J27/047 , C07C85/18
CPC分类号： B01J27/047 , B01J23/30
摘要： Covers a method of preparing diaminodiphenylmethanes and higher homologues thereof which comprises the step of condensing aniline and formaldehyde in the presence of a tungsten boride or sulfide catalyst.
摘要翻译：包括制备二氨基二苯基甲烷及其高级同系物的方法，其包括在硼化钨或硫化物催化剂存在下使苯胺和甲醛缩合的步骤。

5. 发明授权

US4148819A Aliphatic diisocyanates 失效
标题翻译：脂肪族二异氰酸酯
公开(公告)号：US4148819A
公开(公告)日：1979-04-10
申请号：US892523
申请日：1978-04-03
申请人： Lewis W. Watts, Jr. , Clifford L. Lambert, Jr. , Edward T. Marquis
发明人： Lewis W. Watts, Jr. , Clifford L. Lambert, Jr. , Edward T. Marquis
IPC分类号： C07C265/04 , C08G18/77 , C08G65/26 , C08G65/322 , C08G65/324 , C08G65/325 , C07C119/042
CPC分类号： C07C265/00 , C08G18/771 , C08G65/2609 , C08G65/322 , C08G65/324 , C08G65/3255
摘要： Covers a diisocyanate having the following structural formula: ##STR1## WHERE X IS AN AVERAGE NUMBER RANGING FROM ABOUT 6 TO 50, AND Y AND Z ARE AVERAGE NUMBERS RANGING FROM ABOUT 1 TO ABOUT 20, WITH THE SUM OF Y AND Z BEING FROM ABOUT 6 TO ABOUT 40. Also covers a method of preparing said diisocyanate.
摘要翻译：涵盖具有以下结构式的二异氰酸酯： + tr X是从约6到50的平均值范围，Y和Z是从约1到约20的平均数字，以Y的大小并且从约6到约40。还涉及制备所述二异氰酸酯的方法。

6. 发明授权

US4036880A Method of preparing polyaminopolyphenylmethanes 失效
标题翻译：聚氨基多苯基甲烷的制备方法
公开(公告)号：US4036880A
公开(公告)日：1977-07-19
申请号：US723422
申请日：1976-09-15
申请人： Edward T. Marquis , Robert M. Gipson , Lewis W. Watts, Jr.
发明人： Edward T. Marquis , Robert M. Gipson , Lewis W. Watts, Jr.
IPC分类号： C07C85/24
CPC分类号： B01J23/30
摘要： Covers a method of preparing diaminodiphenylmethanes and higher homologues thereof which comprises the step of condensing aniline and formaldehyde in the presence of a molybdenum boride catalyst.
摘要翻译：包括制备二氨基二苯基甲烷及其高级同系物的方法，其包括在硼化钼催化剂存在下使苯胺和甲醛缩合的步骤。

7. 发明授权

US4661272A Thioether diester lubricating oil composition 失效
标题翻译：硫醚二酯润滑油组成
公开(公告)号：US4661272A
公开(公告)日：1987-04-28
申请号：US506733
申请日：1983-06-22
申请人： Edward T. Marquis , Lewis W. Watts, Jr. , Ernest L. Yeakey
发明人： Edward T. Marquis , Lewis W. Watts, Jr. , Ernest L. Yeakey
IPC分类号： C10M105/72 , C10M135/24 , C10M157/06
CPC分类号： C10M135/24 , C07C323/00 , C10M105/72 , C10M2219/084 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/105 , C10N2240/106 , C10N2240/14
摘要： Provided is a novel thioether diester synthetic lubricating oil composition represented by the formula: ##STR1## in which R and R.sub.1 each represent alkyl radicals having from 1 to 6 carbon atoms, with the total number of carbon atoms in R, R, R.sub.1, and R.sub.1 ranging from about 6 to 20, and n is an integer from 2 to 5.
摘要翻译：提供了一种由下式表示的新型硫醚二酯合成润滑油组合物：其中R和R 1各自表示具有1至6个碳原子的烷基，R，R，R 1和R 3中的碳原子总数 R1为约6至20，n为2至5的整数。

8. 发明授权

US4367352A Oligomerized olefins for lubricant stock 失效
标题翻译：用于润滑剂原料的低聚烯烃
公开(公告)号：US4367352A
公开(公告)日：1983-01-04
申请号：US219119
申请日：1980-12-22
申请人： Lewis W. Watts, Jr. , Edward T. Marquis
发明人： Lewis W. Watts, Jr. , Edward T. Marquis
IPC分类号： C07C2/28 , C07C9/22 , C07C2/74
CPC分类号： C07C9/22 , C07C2/28 , C07C2531/10 , C10G2400/10 , Y02P20/52
摘要： A process is disclosed for the production of high quality synthetic lubricants which comprises transforming ethylene into a mix of alpha olefins, separating from this mix of alpha olefins the alpha olefins in the range from about 14 to 20 carbon atoms, oligomerizing the alpha olefins in the range from about 14 to 20 atoms with a perfluorosulfonic acid resin catalyst and hydrogenating these oligomerized olefins. The olefins from the original mix of alpha olefins which are lighter and heavier than the 14 to 20 carbon atom alpha olefins processed above are combined and subjected to an isomerization/disproportionation process and the resulting olefins in the range of about 14 to 20 carbon atoms are oligomerized with perfluorosulfonic acid resin catalyst as above. Optionally, these olefins in the range of 14 to 20 carbon atoms may be combined with the olefins prepared directly from ethylene before oligomerization takes place. The resulting oligomers are hydrogenated. The olefins from the isomerization/disproportionation process which are less than 14 carbon atoms or greater than 20 carbon atoms are once again subjected to the isomerization/disproportionation process as above, the 14 to 20 carbon atom cut is oligomerized, and the process is repeated. The resulting hydrogenated oligomerized olefins are useful in internal combustion engines as crankcase lubricants.
摘要翻译：公开了用于生产高质量合成润滑剂的方法，其包括将乙烯转化为α-烯烃的混合物，从该α-烯烃混合物中分离出约14至20个碳原子的α-烯烃，使α-烯烃在范围从约14至20个原子与全氟磺酸树脂催化剂和氢化这些低聚烯烃。将来自比上述加工的14至20个碳原子α-烯烃更轻和更重的α-烯烃的原始混合物的烯烃合并并进行异构化/歧化过程，所得的约14至20个碳原子范围的烯烃为如上所述用全氟磺酸树脂催化剂低聚。任选地，在低聚发生之前，可将这些在14至20个碳原子范围内的烯烃与直接由乙烯制备的烯烃组合。所得的低聚物被氢化。来自异构化/歧化过程的低于14个碳原子或大于20个碳原子的烯烃再次进行如上所述的异构化/歧化过程，14至20个碳原子切割被低聚，并重复该过程。所得氢化低聚烯烃可用作内燃机作为曲轴箱润滑剂。

9. 发明授权

US4286107A Silver catalysts used to prepare polyaminopolyphenylmethanes 失效
标题翻译：用于制备聚氨基多苯基甲烷的银催化剂
公开(公告)号：US4286107A
公开(公告)日：1981-08-25
申请号：US193325
申请日：1980-10-02
申请人： Edward T. Marquis , Lewis W. Watts, Jr.
发明人： Edward T. Marquis , Lewis W. Watts, Jr.
IPC分类号： B01J23/68 , C07C85/18
CPC分类号： B01J23/687
摘要： Covers a method of preparing diaminodiphenylmethanes and higher homologues thereof which comprises the step of condensing aniline and formaldehyde in the presence of a silver tungstate catalyst.
摘要翻译：包括制备二氨基二苯基甲烷及其高级同系物的方法，其包括在钨酸银催化剂存在下使苯胺和甲醛缩合的步骤。

10. 发明授权

US4052456A Method of preparing polyaminopolyphenylmethanes 失效
标题翻译：制备聚酰胺基苯乙烯的方法
公开(公告)号：US4052456A
公开(公告)日：1977-10-04
申请号：US763967
申请日：1977-01-31
申请人： Edward T. Marquis , Lewis W. Watts, Jr.
发明人： Edward T. Marquis , Lewis W. Watts, Jr.
IPC分类号： C07C85/08
CPC分类号： B01J23/30
摘要： Covers a method of preparing diaminodiphenylmethanes and higher homologues thereof which comprises the step of condensing aniline and formaldehyde in the presence of an aluminum silicide catalyst.

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