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1. 发明授权

US4069828A Flavored tobacco article 失效
标题翻译：调味烟草制品
公开(公告)号：US4069828A
公开(公告)日：1978-01-24
申请号：US683302
申请日：1976-05-05
申请人： John B. Hall , Denis E. Hruza , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
发明人： John B. Hall , Denis E. Hruza , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
IPC分类号： A24B15/32 , C07C17/16 , C07C57/03 , C11B9/00 , A24B3/12
CPC分类号： C11B9/0019 , A24B15/32 , C07C17/16 , C07C57/03
摘要： A tobacco article comprising tobacco Tobacco and C.sub.1 -C.sub.6 alkyl-2-methyl-3,4-pentadienoates as a flavor adjuvant.
摘要翻译：一种烟草制品，其包含烟草烟草和C1-C6烷基-2-甲基-3,4-戊二烯酸酯作为风味佐剂。

2. 发明授权

US3987803A Novel process for altering the organoleptic properties of tobacco using 2-methyl-4-pentenoic acid and the ethyl esters thereof 失效
标题翻译：改善使用2-甲基-4-戊酸的烟草的有机性的新方法及其乙酯
公开(公告)号：US3987803A
公开(公告)日：1976-10-26
申请号：US569854
申请日：1975-04-21
申请人： John B. Hall , Ching Y. Tseng , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
发明人： John B. Hall , Ching Y. Tseng , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
IPC分类号： C07C17/16 , C07C57/03 , C11B9/00 , A24B3/12
CPC分类号： C11B9/0019 , C07C17/16 , C07C57/03
摘要： Described is a process comprising adding to tobacco (for subsequent incorporation into smoking articles along with tobacco blend) an amount sufficient to alter the flavor or aroma of the tobacco of 2-methyl-4-pentenoic acid and/or ethyl-2-methyl-4-pentenoate.

3. 发明授权

US3978239A Foodstuff and flavoring containing C.sub.1 -C.sub.6 alkyl-2-methyl-3,4-pentadienoates 失效
标题翻译：含有C 1'-C 6'亚烷基-2-甲基-3,4-二戊酸酯的食品和香料
公开(公告)号：US3978239A
公开(公告)日：1976-08-31
申请号：US566118
申请日：1975-04-08
申请人： John B. Hall , Denis E. Hruza , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
发明人： John B. Hall , Denis E. Hruza , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
IPC分类号： C07C17/16 , C07C57/03 , C11B9/00 , A23L1/235
CPC分类号： C11B9/0019 , C07C17/16 , C07C57/03
摘要： Described are methods for preparing foodstuffs, flavoring compositions for foodstuffs, tobacco compositions, flavoring compositions for tobacco, perfume compositions, ingredients for perfume compositions, perfumed articles and ingredients for perfumed articles by including therein one or more C.sub.1 -C.sub.6 alkyl-2-methyl-3,4-pentadienoates in order to produce:A. In food flavorings, sweet, fruity, strawberry, tagette oil-like, pear and/or apple-like aromas and sweet, fruity, winey, creamy, strawberry, tagette oil-like, pear and/or apple tastes;B. In perfumes, berry, chamomile, wormwood, apple and/or pineapple notes; andC. In tobaccos, sweet, woody and/or fruity notes;As well as the novel compounds, isobutyl-2-methyl-3,4-pentadienoate and n-hexyl-2-methyl-3,4-pentadienoate.

4. 发明授权

US3966799A Alkyl esters of 2-methyl-4-pentenoic acid 失效
标题翻译： 2-甲基-4-戊烯酸的烷基酯
公开(公告)号：US3966799A
公开(公告)日：1976-06-29
申请号：US579567
申请日：1975-05-21
申请人： John B. Hall , Ching Y. Tseng , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
发明人： John B. Hall , Ching Y. Tseng , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
IPC分类号： C07C17/16 , C07C57/03 , C07C69/533 , C11B9/00 , C07C69/52
CPC分类号： C11B9/0019 , C07C17/16 , C07C57/03 , C07C69/533
摘要： Methods are described for adding the novel compounds, isobutyl and n-hexyl esters of 2-methyl-4-pentenoic acid to foodstuffs, chewing gums or medicinal products in order to impart sweet, fruity, strawberry, pineapple-like, pear and/or green aromas and tastes.
摘要翻译：描述了将2-甲基-4-戊烯酸的新型化合物，异丁基和正己基酯添加到食品，口香糖或药用产品中的方法，以赋予甜味，水果，草莓，菠萝样，梨和/或绿色的香气和口味。

5. 发明授权

US3931306A Process for producing isomer mixtures containing high proportions of cis-2-methyl-3-pentenoic acid 失效
标题翻译：制备含高比例顺式-2-甲基-3-戊烯酸的异构体混合物的方法
公开(公告)号：US3931306A
公开(公告)日：1976-01-06
申请号：US490717
申请日：1974-07-22
申请人： John B. Hall , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
发明人： John B. Hall , Manfred Hugo Vock , Joaquin Vinals , Edward J. Shuster
IPC分类号： A23L27/20 , A24B3/12 , A61K8/36 , A61Q13/00 , C07C17/08 , C07C51/00 , C07C51/36 , C07C57/03 , C07C57/18 , C07C67/00 , C11B9/00 , C11D9/44 , C07C57/02
CPC分类号： C11B9/0019 , A23L27/2028 , C07C17/08 , C07C51/36 , C07C57/18
摘要： A method for producing mixtures containing greater than 50% cis 2-methyl-3-pentenoic acid comprising first reacting methyl acetylene with a methyl magnesium halide to form a methylacetylene magnesium halide Grignard reagent; then reacting the methyl acetylene magnesium halide Grignard reagent with acetaldehyde to form a 3-pentyn-2-ol magnesium halide salt; then hydrolyzing the magnesium halide salt to form 3-pentyn-2-ol; then halogenating the 3-pentyn-2-ol to form a 4-halo-2-pentyne; then reacting magnesium with the 4-halo-2-pentyne to produce a 4-magnesium halo-2-pentyne Grignard reagent; then reacting the 4-magnesium halo-2-pentyne Grignard reagent with carbon dioxide to form a magnesium halo-carboxylate salt mixture of compounds having the structures: ##EQU1## (wherein X is halogen); then hydrolyzing the magnesium halo-carboxylate salt mixture to form a mixture of carboxylic acids having the structures: ##EQU2## then hydrogenating the aforementioned mixture of carboxylic acids to form a mixture containing 80% cis-2-methyl-3-pentenoic acid and 20% of 2-methyl-2-pentenoic acid.
摘要翻译：包括含有大于50％的顺式2-甲基-3-戊烯酸的混合物的方法，其包括首先使甲基乙炔与甲基卤化镁反应以形成甲基乙炔卤化物格氏试剂; 然后使甲基乙炔卤化物格氏试剂与乙醛反应，形成3-戊炔-2-醇卤化镁盐; 然后水解卤化镁盐形成3-戊炔-2-醇; 然后将3-戊炔-2-醇卤化以形成4-卤代-2-戊炔; 然后使镁与4-卤代-2-戊炔反应，生成4-镁卤-2-戊炔格氏试剂; 然后使4-镁卤-2-戊炔格氏试剂与二氧化碳反应，形成具有以下结构的化合物的镁卤代羧酸盐盐混合物：CH3O | CH3-C3BOC CCC ANGLE HOMGX和CH3OH CH3-C = C = CC ANGLE OMgX（其中X为卤素）; 然后水解镁卤代羧酸盐盐混合物以形成具有以下结构的羧酸的混合物：CH 3 O | CH 3 -C 3 O C C C H ANHLE HOH和CH 3 O | CH 3 -C = C = CC ANGLE HOH，然后将上述羧酸混合物氢化成形成含有80％顺式-2-甲基-3-戊烯酸和20％2-甲基-2-戊烯酸的混合物。

6. 发明授权

US4081483A 1-(2-Methyl-2-propenyl)-3-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde and 1-(2-methyl-2-propenyl)-4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde 失效
标题翻译： 1-（2-甲基-2-丙烯基）-3-（4-甲基-3-戊烯基） - {66 {hu 3 {b-环己烯-1-甲醛和1-（2-甲基-2-丙烯基） - 4-（4-甲基-3-戊烯基） - {66 {hu 3 {b-环己烯-1-甲醛
公开(公告)号：US4081483A
公开(公告)日：1978-03-28
申请号：US811620
申请日：1977-06-30
申请人： John B. Hall , Mark A. Sprecker , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , Robert M. Novak
发明人： John B. Hall , Mark A. Sprecker , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , Robert M. Novak
IPC分类号： A23G3/00 , A23G3/36 , A23G4/00 , A23G4/06 , A23G4/12 , A23L27/20 , A24B15/30 , A24B15/34 , C07C45/62 , C07C45/68 , C07C47/21 , C07C47/232 , C07C47/38 , C07C49/303 , C07C49/557 , C07C49/647 , C11B9/00
CPC分类号： A23G3/36 , A23G4/06 , A23G4/126 , A24B15/30 , A24B15/34 , C07C403/02 , C07C45/62 , C07C45/68 , C07C47/21 , C07C47/232 , C07C49/303 , C07C49/557 , C07C49/647 , C11B9/0015 , C11B9/0034 , C11D3/0084 , C07C2101/16
摘要： Described are the compounds 1-(2-methyl-2-propenyl)-3-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde and 1-(2-methyl-2-propenyl)-4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde; and a process for preparing same by means of reacting a methallylic halide with a mixture of 3 and 4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde using a phase transfer agent in a two phase system according to the reaction: ##STR1## wherein the carboxaldehyde moiety is bonded to the alpha-carbon atom or the beta-carbon atom, X is chloro or bromo and M is alkali metal, processes for adding such 1-(2-methyl-2-propenyl)-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehydes to consumable materials whereby:I. In foodstuffs and medicinal products, floral, muguet, coriander, fatty, green and creamy aroma and flavor characteristics are augmented or enhanced;Ii. In perfumes and perfumed articles, citrus, floral and fatty nuances are imparted, augmented and/or enhanced; andIii. In tobaccos and tobacco flavor and aroma imparting or enhancing compositions, sweet, spicey, coriander-like, citrus/fruity notes are imparted, prior to, and, on smokingAnd tobacco, foodstuff, flavor and perfume compositions containing the 1-(2-methyl-2-propenyl)-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehydes.
摘要翻译：描述了化合物1-（2-甲基-2-丙烯基）-3-（4-甲基-3-戊烯基）-TTA3-环己烯-1-甲醛和1-（2-甲基-2-丙烯基）-4 - （4-甲基-3-戊烯基） - DELTA 3-环己烯-1-甲醛; 和其制备方法，其通过使用相间转移剂在2-相系统中使甲基卤化物与3和4-（4-甲基-3-戊烯基）-TA 3 -3-环己烯-1-甲醛的混合物反应，反应：其中羧甲醛部分键合到α-碳原子或β-碳原子上，X是氯或溴，M是碱金属，加入这样的1-（2 - 甲基-2-丙烯基） - （4-甲基-3-戊烯基） - DELTA 3-环己烯-1-甲醛，由此可以得到：

7. 发明授权

US4120308A Substituted norbornane derivatives used in the process of flavoring tobacco and the product thereof 失效
标题翻译：用于调味烟草及其制品过程中的取代的降冰片烷衍生物
公开(公告)号：US4120308A
公开(公告)日：1978-10-17
申请号：US860134
申请日：1977-12-13
申请人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44 , A24B3/12
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： The use of substituted norbornane derivatives used in the process of flavoring tobacco and the product thereof.
摘要翻译：在烟草调味过程中使用的取代的降冰片烷衍生物及其产物的用途。

8. 发明授权

US4119577A Substituted-norbornane perfumes compositions 失效
标题翻译：取代的降冰片烷香料组合物
公开(公告)号：US4119577A
公开(公告)日：1978-10-10
申请号：US860125
申请日：1977-12-13
申请人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： Substituted-norbornane derivatives are described for use as perfumes, colognes and in perfume aroma augmenting, modifying, enhancing, and imparting compositions. The substituted norbornane derivatives having the following structure: ##STR1## wherein R is C.sub.3 or C.sub.4 alkenyl.
摘要翻译：描述了取代的降冰片烷衍生物用作香料，古龙水和香料香气增强，改性，增强和赋予组合物。具有以下结构的取代的降冰片烷衍生物：其中R是C 3或C 4链烯基。

9. 发明授权

US4076853A Flavoring with substituted norbornane derivatives 失效
标题翻译：用取代的降冰片烷衍生物调味
公开(公告)号：US4076853A
公开(公告)日：1978-02-28
申请号：US765847
申请日：1977-02-04
申请人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44 , A23L1/226
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： Norbornane derivatives are used in foodstuffs and flavorings. Specifically, alpha-allyl-3, 3-dimethyl-2-norbornanemethanol, alpha-methallyl-3,3-dimethyl-2-norbornanemethanol, and alpha-allyl-alpha-3,3-trimethyl-2-norbornanemethanol are used.
摘要翻译：降冰片烷衍生物用于食品和调味品。具体地，使用α-烯丙基-3,3-二甲基-2-降冰片烷甲醇，α-甲代烯丙基-3,3-二甲基-2-降冰片烷甲醇和α-烯丙基-α3,3-三甲基-2-降冰片烷甲醇。

10. 发明授权

US4122122A Mixture of 1-(2-propenyl)-3-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde and 1-(2-propenyl)-4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde and process for producing same 失效
标题翻译： 1-（2-丙烯基）-3-（4-甲基-3-戊烯基） - {66 {hu 3 {b-环己烯-1-甲醛和1-（2-丙烯基）-4-（4-甲基） -3-戊烯基） - {66 {hu 3 {b-环己烯-1-甲醛及其制备方法
公开(公告)号：US4122122A
公开(公告)日：1978-10-24
申请号：US827202
申请日：1977-08-24
申请人： John B. Hall , Mark A. Sprecker , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , Robert M. Novak
发明人： John B. Hall , Mark A. Sprecker , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , Robert M. Novak
IPC分类号： A23G3/00 , A23G3/36 , A23G4/00 , A23G4/06 , A23G4/12 , A23L27/20 , A24B15/30 , A24B15/34 , C07C45/62 , C07C45/68 , C07C47/21 , C07C47/232 , C07C47/38 , C07C49/303 , C07C49/557 , C07C49/647 , C11B9/00
CPC分类号： A23G3/36 , A23G4/06 , A23G4/126 , A24B15/30 , A24B15/34 , C07C403/02 , C07C45/62 , C07C45/68 , C07C47/21 , C07C47/232 , C07C49/303 , C07C49/557 , C07C49/647 , C11B9/0015 , C11B9/0034 , C11D3/0084 , C07C2101/16
摘要： Described are the compounds 1-(2-propenyl-3-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde and 1-(2-propenyl)-4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde; and a process for preparing same by means of reacting an allylic halide with a mixture of 3 and 4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde using a phase transfer agent in a two phase system according to the reaction: ##STR1## wherein the carboxaldehyde moiety is bonded to the alpha-carbon atom or the beta-carbon atom, X is chloro or bromo and M is alkali metal, processes for adding such 1-(2-propenyl)-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehydes to consumable materials whereby:(i) In foodstuffs and medicinal products, sweet, fatty, cocoa butter-like, green/grassy, dairy, diacetyl-like, apricot-like and carrot-like aroma characteristics and fatty, cocoa butter-like, green/grassy, dairy-like, diacetyl-like, peach and coconut flavor characteristics are augmented or enhanced;(ii( In perfumes and perfumed articles, sweet, fruity, lavender notes with citrus, floral and balsam nuances are imparted, augmented and/or enhanced; and(iii) In tobaccos and tobacco flavor and aroma imparting or enhancing compositions, cocoa liquor-like, sweet-rich and creamy oily notes are imparted, prior to, and, on smoking and flavor compositions and perfume compositions containing the 1-(2-propenyl)-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehydes.
摘要翻译：描述了化合物1-（2-丙烯基-3-（4-甲基-3-戊烯基）-TATA-环己烯-1-甲醛和1-（2-丙烯基）-4-（4-甲基-3-戊烯基） - DELTA 3-环己烯-1-甲醛;及其制备方法，通过使烯丙基卤与3-和4-（4-甲基-3-戊烯基）-TATA-环己烯-1-甲醛的混合物根据以下反应在两相体系中使用相转移剂：其中甲醛部分键合到α-碳原子或β-碳原子上，X是氯或溴，M是碱金属，将这种1-（2-丙烯基） - （4-甲基-3-戊烯基）-TATA-环己烯-1-甲醛加入到可消耗材料中的方法，由此：

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